data_230k_smz-f1_a _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ' 4-amino-N-(4-methylpyrimidin-2-yl) ' _chemical_name_common ' Sulfamerazine ' _chemical_melting_point ? _chemical_formula_moiety 'C11 H12 N4 O2 S' _chemical_formula_sum 'C11 H12 N4 O2 S' _chemical_formula_weight 264.31 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_H-M_alt 'P n a 21' _space_group_name_Hall 'P 2c -2n' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' _cell_length_a 14.48140(10) _cell_length_b 8.19930(10) _cell_length_c 21.8844(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 2598.50(5) _cell_formula_units_Z 8 _cell_measurement_temperature 230 _cell_measurement_reflns_used 10946 _cell_measurement_theta_min 2.5600 _cell_measurement_theta_max 29.4930 _exptl_crystal_description Parallelepiped _exptl_crystal_colour Colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.351 _exptl_crystal_F_000 1104 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.50 _exptl_crystal_size_mid 0.40 _exptl_crystal_size_min 0.20 _exptl_absorpt_coefficient_mu 0.249 _shelx_estimated_absorpt_T_min 0.886 _shelx_estimated_absorpt_T_max 0.952 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.97876 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _diffrn_ambient_temperature 230 _diffrn_radiation_wavelength 0.68890 _diffrn_radiation_type 'Synchrotron' _diffrn_radiation_source 'Diamond Light Source Beamline I19' _diffrn_radiation_monochromator 'double crystal Silicon 111' _diffrn_measurement_specimen_support 'MiTeGen loop' _diffrn_measurement_device 'CrystalLogic Kappa (3 circle)' _diffrn_measurement_device_type 'Rigaku Saturn724+ (2x2 bin mode)' _diffrn_measurement_method ; omega rotation with 1 degree frames ; _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 23484 _diffrn_reflns_av_unetI/netI 0.0444 _diffrn_reflns_av_R_equivalents 0.0455 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_theta_min 1.804 _diffrn_reflns_theta_max 29.466 _diffrn_reflns_theta_full 24.415 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.968 _diffrn_reflns_point_group_measured_fraction_full 0.988 _reflns_number_total 7671 _reflns_number_gt 6063 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.895 _reflns_Friedel_fraction_max 0.937 _reflns_Friedel_fraction_full 0.977 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_structure_solution 'SHELXT' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'OSCAIL' _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0541P)^2^+0.3587P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 2307 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.02(5) _chemical_absolute_configuration ad _refine_ls_number_reflns 7671 _refine_ls_number_parameters 344 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0620 _refine_ls_R_factor_gt 0.0463 _refine_ls_wR_factor_ref 0.1215 _refine_ls_wR_factor_gt 0.1094 _refine_ls_goodness_of_fit_ref 1.023 _refine_ls_restrained_S_all 1.022 _refine_ls_shift/su_max 0.164 _refine_ls_shift/su_mean 0.004 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.64563(5) 0.49528(9) 0.34413(5) 0.03062(18) Uani 1 1 d . . . . . S2 S 0.57779(5) 0.49624(9) 0.65274(5) 0.03005(18) Uani 1 1 d . . . . . O1 O 0.68883(18) 0.3709(3) 0.30836(13) 0.0400(6) Uani 1 1 d . . . . . O2 O 0.54833(17) 0.5223(3) 0.33745(14) 0.0398(6) Uani 1 1 d . . . . . O3 O 0.67555(16) 0.4689(3) 0.65913(13) 0.0385(6) Uani 1 1 d . . . . . O4 O 0.53552(17) 0.6233(3) 0.68759(12) 0.0386(6) Uani 1 1 d . . . . . N1 N 0.8423(2) 1.1169(4) 0.31214(18) 0.0468(8) Uani 1 1 d . . . . . N2 N 0.6549(2) 0.4487(4) 0.41717(15) 0.0348(6) Uani 1 1 d . . . . . N3 N 0.81439(19) 0.4095(3) 0.41717(15) 0.0356(6) Uani 1 1 d . . . . . N4 N 0.7281(2) 0.4296(5) 0.50952(16) 0.0493(8) Uani 1 1 d . . . . . N5 N 0.3802(2) -0.1201(4) 0.69541(19) 0.0571(10) Uani 1 1 d . . . . . H5A H 0.3238 -0.1186 0.7077 0.074 Uiso 1 1 calc R U . . . H5B H 0.4075 -0.2116 0.6890 0.074 Uiso 1 1 calc R U . . . N6 N 0.5683(2) 0.5383(4) 0.57937(15) 0.0366(7) Uani 1 1 d . . . . . N7 N 0.4095(2) 0.5866(4) 0.58006(15) 0.0377(7) Uani 1 1 d . . . . . N8 N 0.4961(2) 0.5658(5) 0.48751(16) 0.0497(8) Uani 1 1 d . . . . . C1 C 0.7046(2) 0.6773(4) 0.33386(18) 0.0291(7) Uani 1 1 d . . . . . C2 C 0.7942(2) 0.6793(4) 0.31053(16) 0.0298(7) Uani 1 1 d . . . . . H2 H 0.8231 0.5822 0.2998 0.039 Uiso 1 1 calc R U . . . C3 C 0.8396(2) 0.8252(4) 0.30340(17) 0.0302(7) Uani 1 1 d . . . . . H3 H 0.8996 0.8260 0.2882 0.039 Uiso 1 1 calc R U . . . C4 C 0.7967(2) 0.9724(4) 0.31880(16) 0.0323(7) Uani 1 1 d . . . . . C5 C 0.7062(2) 0.9696(4) 0.3424(2) 0.0355(7) Uani 1 1 d . . . . . H5 H 0.6769 1.0666 0.3528 0.046 Uiso 1 1 calc R U . . . C6 C 0.6612(2) 0.8231(4) 0.35001(19) 0.0347(7) Uani 1 1 d . . . . . H6 H 0.6017 0.8213 0.3660 0.045 Uiso 1 1 calc R U . . . C7 C 0.7370(2) 0.4286(4) 0.44910(16) 0.0333(7) Uani 1 1 d . . . . . C8 C 0.8065(3) 0.4047(8) 0.5404(2) 0.0687(15) Uani 1 1 d . . . . . H8 H 0.8040 0.4019 0.5829 0.089 Uiso 1 1 calc R U . . . C9 C 0.8898(3) 0.3833(7) 0.5125(2) 0.0630(13) Uani 1 1 d . . . . . H9 H 0.9432 0.3660 0.5352 0.082 Uiso 1 1 calc R U . . . C10 C 0.8920(2) 0.3880(5) 0.4499(2) 0.0436(9) Uani 1 1 d . . . . . C11 C 0.9787(3) 0.3698(6) 0.4142(2) 0.0600(12) Uani 1 1 d . . . . . H11A H 0.9802 0.2638 0.3956 0.078 Uiso 1 1 calc R U . . . H11B H 1.0308 0.3820 0.4409 0.078 Uiso 1 1 calc R U . . . H11C H 0.9810 0.4520 0.3830 0.078 Uiso 1 1 calc R U . . . C12 C 0.5191(2) 0.3159(4) 0.66590(16) 0.0290(6) Uani 1 1 d . . . . . C13 C 0.5636(2) 0.1684(4) 0.6556(2) 0.0395(8) Uani 1 1 d . . . . . H13 H 0.6244 0.1674 0.6419 0.051 Uiso 1 1 calc R U . . . C14 C 0.5178(3) 0.0237(4) 0.6656(2) 0.0442(10) Uani 1 1 d . . . . . H14 H 0.5481 -0.0746 0.6585 0.057 Uiso 1 1 calc R U . . . C15 C 0.4263(3) 0.0226(4) 0.68613(18) 0.0379(8) Uani 1 1 d . . . . . C16 C 0.3823(2) 0.1721(4) 0.69650(17) 0.0342(7) Uani 1 1 d . . . . . H16 H 0.3216 0.1734 0.7102 0.044 Uiso 1 1 calc R U . . . C17 C 0.4279(2) 0.3173(4) 0.68660(18) 0.0313(7) Uani 1 1 d . . . . . H17 H 0.3980 0.4159 0.6937 0.041 Uiso 1 1 calc R U . . . C18 C 0.4866(2) 0.5653(4) 0.54835(17) 0.0344(7) Uani 1 1 d . . . . . C19 C 0.4183(3) 0.5982(8) 0.4565(2) 0.0672(15) Uani 1 1 d . . . . . H19 H 0.4206 0.6027 0.4141 0.087 Uiso 1 1 calc R U . . . C20 C 0.3353(3) 0.6250(7) 0.4851(2) 0.0673(14) Uani 1 1 d . . . . . H20 H 0.2825 0.6491 0.4627 0.088 Uiso 1 1 calc R U . . . C21 C 0.3323(3) 0.6151(5) 0.5481(2) 0.0446(9) Uani 1 1 d . . . . . C22 C 0.2455(3) 0.6357(7) 0.5843(3) 0.0637(13) Uani 1 1 d . . . . . H22A H 0.2450 0.7417 0.6029 0.083 Uiso 1 1 calc R U . . . H22B H 0.2427 0.5535 0.6155 0.083 Uiso 1 1 calc R U . . . H22C H 0.1931 0.6251 0.5577 0.083 Uiso 1 1 calc R U . . . H1N1 H 0.895(3) 1.121(6) 0.293(2) 0.065(14) Uiso 1 1 d . . . . . H2N1 H 0.812(3) 1.202(6) 0.316(2) 0.053(12) Uiso 1 1 d . . . . . H1N2 H 0.614(3) 0.484(5) 0.438(2) 0.043(12) Uiso 1 1 d . . . . . H1N6 H 0.622(3) 0.498(5) 0.559(2) 0.060(15) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0286(3) 0.0327(4) 0.0305(4) 0.0024(3) -0.0015(3) -0.0020(3) S2 0.0278(3) 0.0326(4) 0.0298(5) 0.0036(3) -0.0014(3) -0.0019(3) O1 0.0473(14) 0.0334(11) 0.0394(15) -0.0056(11) 0.0003(12) -0.0016(10) O2 0.0304(11) 0.0487(13) 0.0403(16) 0.0076(12) -0.0057(12) -0.0057(10) O3 0.0279(11) 0.0510(14) 0.0367(15) 0.0078(12) -0.0062(11) -0.0034(9) O4 0.0436(14) 0.0316(11) 0.0407(15) -0.0032(10) -0.0012(12) -0.0017(10) N1 0.0400(17) 0.0345(15) 0.066(2) -0.0074(15) 0.0187(17) -0.0055(13) N2 0.0254(13) 0.0456(16) 0.0333(18) 0.0072(14) 0.0011(12) 0.0011(11) N3 0.0289(13) 0.0389(14) 0.0390(18) 0.0039(13) 0.0018(12) 0.0016(11) N4 0.0347(16) 0.080(2) 0.0334(19) 0.0057(17) 0.0002(14) 0.0122(16) N5 0.051(2) 0.0325(15) 0.088(3) -0.0053(17) 0.017(2) -0.0086(13) N6 0.0279(13) 0.0514(17) 0.0304(18) 0.0098(14) 0.0018(12) 0.0027(12) N7 0.0298(14) 0.0423(15) 0.0410(19) 0.0018(13) 0.0014(12) 0.0048(11) N8 0.0352(16) 0.078(2) 0.036(2) 0.0066(17) -0.0028(14) 0.0134(16) C1 0.0270(14) 0.0308(14) 0.0294(18) 0.0030(13) 0.0021(13) -0.0003(11) C2 0.0281(14) 0.0327(14) 0.0285(18) -0.0011(12) 0.0003(13) 0.0035(11) C3 0.0263(15) 0.0374(16) 0.0270(19) -0.0019(13) 0.0047(13) -0.0002(12) C4 0.0354(17) 0.0331(15) 0.0285(18) -0.0019(12) 0.0009(14) -0.0013(12) C5 0.0353(17) 0.0319(14) 0.039(2) -0.0028(15) 0.0063(17) 0.0034(12) C6 0.0293(14) 0.0356(15) 0.039(2) -0.0001(15) 0.0074(15) 0.0014(11) C7 0.0301(16) 0.0351(16) 0.035(2) 0.0048(14) 0.0004(14) 0.0029(12) C8 0.051(3) 0.118(4) 0.037(3) 0.000(3) -0.010(2) 0.026(3) C9 0.035(2) 0.105(4) 0.049(3) -0.004(3) -0.012(2) 0.019(2) C10 0.0315(17) 0.048(2) 0.051(3) -0.0017(18) 0.0001(17) 0.0075(15) C11 0.034(2) 0.077(3) 0.069(3) -0.003(3) 0.003(2) 0.0110(19) C12 0.0287(14) 0.0300(13) 0.0282(17) 0.0003(12) 0.0015(13) 0.0015(11) C13 0.0316(16) 0.0367(16) 0.050(2) 0.0010(17) 0.0090(18) 0.0045(12) C14 0.0382(18) 0.0314(16) 0.063(3) -0.0030(16) 0.0060(18) 0.0042(13) C15 0.0394(19) 0.0339(16) 0.040(2) -0.0004(14) 0.0009(16) -0.0017(13) C16 0.0337(16) 0.0344(15) 0.035(2) -0.0037(14) 0.0037(14) -0.0023(12) C17 0.0311(16) 0.0311(15) 0.032(2) -0.0021(13) 0.0028(14) 0.0015(12) C18 0.0317(16) 0.0379(16) 0.034(2) 0.0051(14) -0.0018(14) 0.0021(13) C19 0.044(2) 0.122(5) 0.035(3) 0.002(3) -0.0068(19) 0.024(3) C20 0.043(2) 0.107(4) 0.052(3) -0.004(3) -0.010(2) 0.029(2) C21 0.0326(17) 0.052(2) 0.050(3) -0.0003(18) -0.0017(17) 0.0075(15) C22 0.034(2) 0.084(3) 0.073(3) -0.006(3) 0.006(2) 0.009(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 O1 1.430(3) . ? S1 O2 1.434(2) . ? S1 N2 1.649(3) . ? S1 C1 1.734(3) . ? S2 O4 1.429(3) . ? S2 O3 1.440(2) . ? S2 N6 1.648(3) . ? S2 C12 1.730(3) . ? N1 C4 1.364(4) . ? N1 H1N1 0.87(5) . ? N1 H2N1 0.83(4) . ? N2 C7 1.389(4) . ? N2 H1N2 0.80(5) . ? N3 C7 1.330(4) . ? N3 C10 1.345(5) . ? N4 C7 1.328(5) . ? N4 C8 1.336(5) . ? N5 C15 1.362(4) . ? N5 H5A 0.8600 . ? N5 H5B 0.8600 . ? N6 C18 1.382(4) . ? N6 H1N6 0.95(5) . ? N7 C18 1.325(4) . ? N7 C21 1.340(5) . ? N8 C18 1.339(5) . ? N8 C19 1.342(5) . ? C1 C2 1.394(4) . ? C1 C6 1.396(4) . ? C2 C3 1.374(5) . ? C2 H2 0.9300 . ? C3 C4 1.399(5) . ? C3 H3 0.9300 . ? C4 C5 1.409(5) . ? C5 C6 1.376(5) . ? C5 H5 0.9300 . ? C6 H6 0.9300 . ? C8 C9 1.364(6) . ? C8 H8 0.9300 . ? C9 C10 1.371(6) . ? C9 H9 0.9300 . ? C10 C11 1.486(5) . ? C11 H11A 0.9600 . ? C11 H11B 0.9600 . ? C11 H11C 0.9600 . ? C12 C13 1.389(4) . ? C12 C17 1.396(4) . ? C13 C14 1.377(5) . ? C13 H13 0.9300 . ? C14 C15 1.400(5) . ? C14 H14 0.9300 . ? C15 C16 1.400(5) . ? C16 C17 1.378(5) . ? C16 H16 0.9300 . ? C17 H17 0.9300 . ? C19 C20 1.373(6) . ? C19 H19 0.9300 . ? C20 C21 1.380(7) . ? C20 H20 0.9300 . ? C21 C22 1.495(6) . ? C22 H22A 0.9600 . ? C22 H22B 0.9600 . ? C22 H22C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 S1 O2 118.96(16) . . ? O1 S1 N2 109.25(17) . . ? O2 S1 N2 102.40(16) . . ? O1 S1 C1 109.10(17) . . ? O2 S1 C1 109.77(15) . . ? N2 S1 C1 106.56(18) . . ? O4 S2 O3 118.88(17) . . ? O4 S2 N6 109.36(16) . . ? O3 S2 N6 102.07(16) . . ? O4 S2 C12 108.91(16) . . ? O3 S2 C12 109.50(15) . . ? N6 S2 C12 107.46(17) . . ? C4 N1 H1N1 120(3) . . ? C4 N1 H2N1 118(3) . . ? H1N1 N1 H2N1 119(4) . . ? C7 N2 S1 125.8(3) . . ? C7 N2 H1N2 113(4) . . ? S1 N2 H1N2 114(3) . . ? C7 N3 C10 116.1(3) . . ? C7 N4 C8 114.9(4) . . ? C15 N5 H5A 120.0 . . ? C15 N5 H5B 120.0 . . ? H5A N5 H5B 120.0 . . ? C18 N6 S2 125.7(3) . . ? C18 N6 H1N6 121(3) . . ? S2 N6 H1N6 109(3) . . ? C18 N7 C21 116.9(3) . . ? C18 N8 C19 114.6(4) . . ? C2 C1 C6 120.1(3) . . ? C2 C1 S1 121.1(2) . . ? C6 C1 S1 118.8(2) . . ? C3 C2 C1 119.9(3) . . ? C3 C2 H2 120.1 . . ? C1 C2 H2 120.1 . . ? C2 C3 C4 120.7(3) . . ? C2 C3 H3 119.6 . . ? C4 C3 H3 119.6 . . ? N1 C4 C3 120.6(3) . . ? N1 C4 C5 120.3(3) . . ? C3 C4 C5 119.2(3) . . ? C6 C5 C4 120.0(3) . . ? C6 C5 H5 120.0 . . ? C4 C5 H5 120.0 . . ? C5 C6 C1 120.2(3) . . ? C5 C6 H6 119.9 . . ? C1 C6 H6 119.9 . . ? N4 C7 N3 127.2(3) . . ? N4 C7 N2 114.7(3) . . ? N3 C7 N2 118.1(3) . . ? N4 C8 C9 123.0(4) . . ? N4 C8 H8 118.5 . . ? C9 C8 H8 118.5 . . ? C8 C9 C10 117.7(4) . . ? C8 C9 H9 121.2 . . ? C10 C9 H9 121.2 . . ? N3 C10 C9 121.1(4) . . ? N3 C10 C11 116.0(4) . . ? C9 C10 C11 122.9(4) . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C13 C12 C17 119.9(3) . . ? C13 C12 S2 119.3(2) . . ? C17 C12 S2 120.8(2) . . ? C14 C13 C12 120.1(3) . . ? C14 C13 H13 120.0 . . ? C12 C13 H13 120.0 . . ? C13 C14 C15 120.8(3) . . ? C13 C14 H14 119.6 . . ? C15 C14 H14 119.6 . . ? N5 C15 C16 120.3(3) . . ? N5 C15 C14 121.2(3) . . ? C16 C15 C14 118.5(3) . . ? C17 C16 C15 120.9(3) . . ? C17 C16 H16 119.6 . . ? C15 C16 H16 119.6 . . ? C16 C17 C12 119.8(3) . . ? C16 C17 H17 120.1 . . ? C12 C17 H17 120.1 . . ? N7 C18 N8 127.4(3) . . ? N7 C18 N6 119.0(3) . . ? N8 C18 N6 113.6(3) . . ? N8 C19 C20 122.5(4) . . ? N8 C19 H19 118.8 . . ? C20 C19 H19 118.8 . . ? C19 C20 C21 118.2(4) . . ? C19 C20 H20 120.9 . . ? C21 C20 H20 120.9 . . ? N7 C21 C20 120.4(4) . . ? N7 C21 C22 116.4(4) . . ? C20 C21 C22 123.2(4) . . ? C21 C22 H22A 109.5 . . ? C21 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C21 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 S1 N2 C7 60.5(3) . . . . ? O2 S1 N2 C7 -172.4(3) . . . . ? C1 S1 N2 C7 -57.2(3) . . . . ? O4 S2 N6 C18 -57.2(3) . . . . ? O3 S2 N6 C18 176.0(3) . . . . ? C12 S2 N6 C18 60.9(3) . . . . ? O1 S1 C1 C2 -18.4(4) . . . . ? O2 S1 C1 C2 -150.4(3) . . . . ? N2 S1 C1 C2 99.5(3) . . . . ? O1 S1 C1 C6 162.3(3) . . . . ? O2 S1 C1 C6 30.3(4) . . . . ? N2 S1 C1 C6 -79.9(3) . . . . ? C6 C1 C2 C3 -0.1(5) . . . . ? S1 C1 C2 C3 -179.4(3) . . . . ? C1 C2 C3 C4 -0.6(5) . . . . ? C2 C3 C4 N1 179.4(3) . . . . ? C2 C3 C4 C5 0.6(5) . . . . ? N1 C4 C5 C6 -178.8(4) . . . . ? C3 C4 C5 C6 0.0(6) . . . . ? C4 C5 C6 C1 -0.6(6) . . . . ? C2 C1 C6 C5 0.7(6) . . . . ? S1 C1 C6 C5 -180.0(3) . . . . ? C8 N4 C7 N3 -1.6(6) . . . . ? C8 N4 C7 N2 177.8(4) . . . . ? C10 N3 C7 N4 0.4(5) . . . . ? C10 N3 C7 N2 -179.0(3) . . . . ? S1 N2 C7 N4 164.8(3) . . . . ? S1 N2 C7 N3 -15.7(5) . . . . ? C7 N4 C8 C9 1.3(8) . . . . ? N4 C8 C9 C10 0.1(9) . . . . ? C7 N3 C10 C9 1.2(6) . . . . ? C7 N3 C10 C11 -178.9(4) . . . . ? C8 C9 C10 N3 -1.4(7) . . . . ? C8 C9 C10 C11 178.7(5) . . . . ? O4 S2 C12 C13 -157.4(3) . . . . ? O3 S2 C12 C13 -25.9(3) . . . . ? N6 S2 C12 C13 84.2(3) . . . . ? O4 S2 C12 C17 22.6(3) . . . . ? O3 S2 C12 C17 154.1(3) . . . . ? N6 S2 C12 C17 -95.7(3) . . . . ? C17 C12 C13 C14 0.2(6) . . . . ? S2 C12 C13 C14 -179.7(4) . . . . ? C12 C13 C14 C15 0.0(7) . . . . ? C13 C14 C15 N5 179.2(4) . . . . ? C13 C14 C15 C16 -0.1(6) . . . . ? N5 C15 C16 C17 -179.2(4) . . . . ? C14 C15 C16 C17 0.1(6) . . . . ? C15 C16 C17 C12 0.1(6) . . . . ? C13 C12 C17 C16 -0.2(5) . . . . ? S2 C12 C17 C16 179.7(3) . . . . ? C21 N7 C18 N8 -1.4(6) . . . . ? C21 N7 C18 N6 178.9(3) . . . . ? C19 N8 C18 N7 2.8(6) . . . . ? C19 N8 C18 N6 -177.5(4) . . . . ? S2 N6 C18 N7 11.9(5) . . . . ? S2 N6 C18 N8 -167.8(3) . . . . ? C18 N8 C19 C20 -1.4(8) . . . . ? N8 C19 C20 C21 -1.1(9) . . . . ? C18 N7 C21 C20 -1.5(6) . . . . ? C18 N7 C21 C22 178.8(4) . . . . ? C19 C20 C21 N7 2.7(8) . . . . ? C19 C20 C21 C22 -177.7(5) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N5 H5B O4 0.86 2.30 3.085(4) 152.6 1_545 N1 H1N1 O4 0.87(5) 2.51(5) 3.250(4) 143(4) 4_654 N1 H2N1 O1 0.83(4) 2.27(4) 3.047(4) 157(4) 1_565 N2 H1N2 N8 0.80(5) 2.14(5) 2.929(5) 174(5) . N6 H1N6 N4 0.95(5) 1.96(5) 2.914(5) 175(5) . _refine_diff_density_max 0.244 _refine_diff_density_min -0.313 _refine_diff_density_rms 0.047 _shelx_res_file ; 230k_smz-f1_a.res created by SHELXL-2014/7 TITL 230k_smz-f1_a.res in Pna2(1) REM Old TITL 009_230K_SulfamerazineF1_ in Pna2(1) REM SHELXT solution in Pna2(1) REM R1 0.100, Rweak 0.041, Alpha 0.003, Orientation as input REM Flack x = 0.092 ( 0.040 ) from Parsons' quotients REM Formula found by SHELXT: C26 N4 O4 S2 CELL 0.68890 14.4814 8.1993 21.8844 90.000 90.000 90.000 ZERR 8.000 0.0001 0.0001 0.0003 0.000 0.000 0.000 REM SG 33 4 4 Pna21 PGmm2 Orthorhombic LATT -1 REM SG ASUN 1 .5 .5 1. REM SG ORGN on 2(1) SYMM -X,-Y,0.5+Z SYMM 0.5+X,0.5-Y,Z SYMM 0.5-X,0.5+Y,0.5+Z SFAC C H N O S UNIT 88.00 96.00 32.00 16.00 8.00 L.S. 10 SIZE 0.50 0.40 0.20 BOND $H FMAP 2 PLAN 20 ACTA CONF EQIV $1 x, y-1, z HTAB N5 O4_$1 EQIV $2 -x+3/2, y+1/2, z-1/2 HTAB N1 O4_$2 EQIV $3 x, y+1, z HTAB N1 O1_$3 HTAB N2 N8 HTAB N6 N4 LIST 4 WGHT 0.054100 0.358700 FVAR 0.52336 0.35344 S1 5 0.645632 0.495278 0.344131 11.00000 0.02862 0.03270 = 0.03055 0.00243 -0.00148 -0.00202 S2 5 0.577793 0.496243 0.652744 11.00000 0.02780 0.03258 = 0.02978 0.00361 -0.00143 -0.00186 O1 4 0.688829 0.370880 0.308365 11.00000 0.04733 0.03340 = 0.03941 -0.00561 0.00028 -0.00158 O2 4 0.548329 0.522268 0.337450 11.00000 0.03042 0.04866 = 0.04034 0.00756 -0.00567 -0.00568 O3 4 0.675552 0.468902 0.659128 11.00000 0.02795 0.05099 = 0.03671 0.00777 -0.00620 -0.00336 O4 4 0.535515 0.623319 0.687587 11.00000 0.04365 0.03161 = 0.04066 -0.00319 -0.00119 -0.00171 N1 3 0.842317 1.116934 0.312144 11.00000 0.03995 0.03445 = 0.06605 -0.00744 0.01868 -0.00554 N2 3 0.654909 0.448675 0.417167 11.00000 0.02543 0.04564 = 0.03335 0.00718 0.00107 0.00105 N3 3 0.814393 0.409542 0.417174 11.00000 0.02890 0.03895 = 0.03904 0.00394 0.00176 0.00161 N4 3 0.728144 0.429550 0.509518 11.00000 0.03470 0.07981 = 0.03337 0.00569 0.00018 0.01221 N5 3 0.380188 -0.120079 0.695406 11.00000 0.05119 0.03249 = 0.08756 -0.00535 0.01672 -0.00857 AFIX 93 H5A 2 0.323782 -0.118597 0.707688 11.00000 -1.30000 H5B 2 0.407483 -0.211637 0.688979 11.00000 -1.30000 AFIX 0 N6 3 0.568290 0.538320 0.579374 11.00000 0.02787 0.05143 = 0.03038 0.00983 0.00184 0.00272 N7 3 0.409542 0.586631 0.580064 11.00000 0.02982 0.04229 = 0.04098 0.00185 0.00137 0.00476 N8 3 0.496101 0.565844 0.487514 11.00000 0.03518 0.07842 = 0.03562 0.00664 -0.00276 0.01336 C1 1 0.704634 0.677265 0.333857 11.00000 0.02702 0.03085 = 0.02938 0.00302 0.00211 -0.00029 C2 1 0.794205 0.679339 0.310533 11.00000 0.02808 0.03272 = 0.02847 -0.00108 0.00029 0.00347 AFIX 43 H2 2 0.823137 0.582196 0.299823 11.00000 -1.30000 AFIX 0 C3 1 0.839646 0.825166 0.303402 11.00000 0.02632 0.03743 = 0.02696 -0.00188 0.00470 -0.00023 AFIX 43 H3 2 0.899600 0.826029 0.288175 11.00000 -1.30000 AFIX 0 C4 1 0.796708 0.972432 0.318800 11.00000 0.03540 0.03305 = 0.02848 -0.00190 0.00093 -0.00133 C5 1 0.706227 0.969557 0.342392 11.00000 0.03531 0.03194 = 0.03919 -0.00284 0.00629 0.00345 AFIX 43 H5 2 0.676911 1.066562 0.352817 11.00000 -1.30000 AFIX 0 C6 1 0.661220 0.823097 0.350009 11.00000 0.02928 0.03557 = 0.03935 -0.00007 0.00739 0.00140 AFIX 43 H6 2 0.601706 0.821261 0.365964 11.00000 -1.30000 AFIX 0 C7 1 0.737000 0.428588 0.449105 11.00000 0.03010 0.03513 = 0.03472 0.00481 0.00044 0.00290 C8 1 0.806457 0.404697 0.540408 11.00000 0.05068 0.11840 = 0.03716 -0.00007 -0.00987 0.02638 AFIX 43 H8 2 0.804040 0.401893 0.582861 11.00000 -1.30000 AFIX 0 C9 1 0.889788 0.383252 0.512511 11.00000 0.03516 0.10464 = 0.04929 -0.00422 -0.01228 0.01911 AFIX 43 H9 2 0.943240 0.365988 0.535161 11.00000 -1.30000 AFIX 0 C10 1 0.892001 0.388033 0.449928 11.00000 0.03152 0.04777 = 0.05143 -0.00171 0.00011 0.00746 C11 1 0.978675 0.369835 0.414186 11.00000 0.03449 0.07671 = 0.06869 -0.00305 0.00285 0.01104 AFIX 137 H11A 2 0.980226 0.263785 0.395625 11.00000 -1.30000 H11B 2 1.030813 0.382006 0.440892 11.00000 -1.30000 H11C 2 0.980962 0.451963 0.382958 11.00000 -1.30000 AFIX 0 C12 1 0.519091 0.315883 0.665896 11.00000 0.02867 0.03004 = 0.02816 0.00029 0.00152 0.00155 C13 1 0.563607 0.168402 0.655577 11.00000 0.03163 0.03671 = 0.05006 0.00096 0.00904 0.00447 AFIX 43 H13 2 0.624414 0.167402 0.641912 11.00000 -1.30000 AFIX 0 C14 1 0.517817 0.023686 0.665554 11.00000 0.03817 0.03136 = 0.06309 -0.00296 0.00601 0.00415 AFIX 43 H14 2 0.548068 -0.074596 0.658533 11.00000 -1.30000 AFIX 0 C15 1 0.426305 0.022622 0.686133 11.00000 0.03943 0.03390 = 0.04046 -0.00040 0.00091 -0.00174 C16 1 0.382334 0.172086 0.696498 11.00000 0.03366 0.03440 = 0.03452 -0.00372 0.00373 -0.00230 AFIX 43 H16 2 0.321572 0.173449 0.710246 11.00000 -1.30000 AFIX 0 C17 1 0.427904 0.317305 0.686597 11.00000 0.03112 0.03108 = 0.03164 -0.00212 0.00285 0.00145 AFIX 43 H17 2 0.398007 0.415890 0.693683 11.00000 -1.30000 AFIX 0 C18 1 0.486556 0.565317 0.548353 11.00000 0.03173 0.03792 = 0.03353 0.00512 -0.00177 0.00212 C19 1 0.418273 0.598225 0.456542 11.00000 0.04441 0.12183 = 0.03532 0.00247 -0.00681 0.02421 AFIX 43 H19 2 0.420644 0.602706 0.414108 11.00000 -1.30000 AFIX 0 C20 1 0.335266 0.624992 0.485142 11.00000 0.04291 0.10656 = 0.05250 -0.00392 -0.01012 0.02905 AFIX 43 H20 2 0.282453 0.649139 0.462721 11.00000 -1.30000 AFIX 0 C21 1 0.332321 0.615092 0.548083 11.00000 0.03260 0.05151 = 0.04963 -0.00025 -0.00171 0.00753 C22 1 0.245515 0.635660 0.584269 11.00000 0.03399 0.08363 = 0.07334 -0.00594 0.00591 0.00936 AFIX 137 H22A 2 0.245019 0.741654 0.602900 11.00000 -1.30000 H22B 2 0.242672 0.553461 0.615451 11.00000 -1.30000 H22C 2 0.193121 0.625070 0.557688 11.00000 -1.30000 AFIX 0 H1N1 2 0.894604 1.120749 0.292587 11.00000 0.06469 H2N1 2 0.812353 1.202356 0.316374 11.00000 0.05299 H1N2 2 0.614309 0.483533 0.437928 11.00000 0.04289 H1N6 2 0.621525 0.498437 0.558591 11.00000 0.05974 HKLF 4 REM 230k_smz-f1_a.res in Pna2(1) REM R1 = 0.0463 for 6063 Fo > 4sig(Fo) and 0.0620 for all 7671 data REM 344 parameters refined using 1 restraints END WGHT 0.0532 0.2362 REM Highest difference peak 0.244, deepest hole -0.313, 1-sigma level 0.047 Q1 1 0.8091 0.7607 0.3090 11.00000 0.05 0.24 Q2 1 0.6801 0.6004 0.3402 11.00000 0.05 0.23 Q3 1 0.5468 0.3927 0.6581 11.00000 0.05 0.23 Q4 1 0.5485 0.2550 0.6570 11.00000 0.05 0.21 Q5 1 0.6362 0.4707 0.6585 11.00000 0.05 0.21 Q6 1 0.1966 0.5313 0.6816 11.00000 0.05 0.20 Q7 1 0.5885 0.5526 0.3490 11.00000 0.05 0.20 Q8 1 0.4081 0.1022 0.6901 11.00000 0.05 0.20 Q9 1 0.5352 0.0956 0.6580 11.00000 0.05 0.19 Q10 1 0.5315 0.5958 0.5698 11.00000 0.05 0.19 Q11 1 0.5321 0.4172 0.6664 11.00000 0.05 0.19 Q12 1 0.7460 0.9596 0.3203 11.00000 0.05 0.18 Q13 1 0.8231 0.9002 0.3172 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180.91 14.03 4 -6 9 177.74 12.51 4 6 9 146.67 12.86 4 -6 9 194.16 14.06 4 6 10 96.16 10.26 4 6 10 116.89 11.43 -4 6 10 97.45 10.52 4 -6 10 101.43 10.13 4 -6 10 92.20 9.18 4 6 11 470.94 22.78 -4 6 11 403.29 21.25 4 6 11 425.01 22.09 4 -6 11 414.67 19.60 4 -6 11 443.70 21.34 4 -6 12 32.64 5.66 4 6 12 32.34 6.89 4 6 12 43.51 7.26 -4 6 12 30.76 6.19 4 -6 12 28.62 5.91 4 6 13 20.48 4.89 4 6 13 36.33 6.83 4 -6 13 23.03 4.52 -4 6 13 28.14 5.12 4 6 14 108.12 11.16 4 6 14 129.97 12.80 4 -6 14 105.19 10.55 -4 6 14 97.46 11.36 4 6 15 446.81 23.27 -4 6 15 429.83 22.70 4 6 15 414.75 22.67 4 6 16 32.42 6.50 -4 6 16 26.71 6.91 4 6 16 29.16 6.48 4 6 17 94.09 10.74 4 6 17 77.92 10.30 -4 6 17 87.87 10.84 -4 6 18 12.76 4.82 4 6 18 10.34 4.44 4 6 18 7.16 4.68 4 6 19 15.06 4.94 4 6 19 8.22 3.82 -4 6 19 8.29 4.22 4 6 20 149.05 14.31 -4 6 20 148.03 14.41 4 6 21 54.55 9.08 -4 6 21 72.39 10.65 -4 6 22 32.33 7.52 4 6 22 20.31 6.04 -4 6 22 27.97 6.62 4 6 23 32.16 7.52 -4 6 23 24.98 6.88 -4 6 23 43.28 8.31 -4 6 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4.94 4 -8 -12 8.08 2.18 4 -8 -12 1.68 2.23 4 8 -12 8.93 4.55 -4 -8 -12 1.99 2.03 -4 -8 -11 10.45 4.27 4 8 -11 7.51 3.92 4 -8 -11 11.00 4.17 4 -8 -11 5.93 2.56 4 8 -10 120.00 12.73 -4 8 -10 128.60 12.98 -4 -8 -10 131.97 12.67 4 -8 -10 142.88 14.06 4 -8 -10 133.87 12.94 -4 -8 -9 27.29 6.10 4 8 -9 26.36 6.67 4 -8 -9 13.37 4.21 4 -8 -9 24.64 5.55 -4 8 -9 13.14 4.37 4 8 -8 11.81 3.48 4 -8 -8 12.06 4.62 -4 8 -8 13.16 4.63 4 -8 -8 16.16 4.83 4 8 -7 103.68 11.72 4 -8 -7 75.53 10.30 -4 8 -7 78.14 10.21 4 -8 -7 94.79 10.80 4 -8 -6 136.00 13.81 4 8 -6 127.09 12.45 -4 8 -6 135.09 13.13 4 -8 -6 133.58 12.73 4 8 -5 41.23 7.50 -4 8 -5 42.52 7.75 4 -8 -5 42.03 6.80 4 -8 -5 38.52 8.13 4 8 -5 49.97 7.48 4 8 -4 18.00 5.38 -4 8 -4 24.49 5.99 4 -8 -4 16.18 4.66 4 8 -4 30.86 6.25 4 -8 -4 13.08 3.70 4 -8 -3 8.43 2.60 4 8 -3 5.16 3.64 4 -8 -3 11.56 5.18 4 8 -3 12.47 3.49 -4 8 -3 12.24 4.65 -4 8 -2 18.52 4.87 4 8 -2 15.25 4.75 4 -8 -2 12.80 4.30 4 -8 -2 12.66 4.75 4 8 -2 17.31 5.74 4 -8 -1 112.70 10.82 4 -8 -1 134.03 13.35 4 8 -1 122.02 12.51 -4 8 -1 132.04 13.02 4 8 -1 128.23 12.48 4 8 0 197.86 15.58 4 8 0 183.76 14.65 -4 8 0 159.76 14.02 4 -8 0 158.46 14.68 4 -8 0 162.40 12.58 4 8 1 136.67 13.37 4 8 1 150.54 13.30 -4 8 1 141.04 13.62 4 -8 1 123.42 11.15 4 -8 1 105.43 11.49 4 -8 2 15.16 5.35 4 8 2 13.40 4.38 -4 8 2 12.87 4.10 4 8 2 2.37 2.85 4 -8 3 12.13 3.85 4 8 3 10.07 3.79 4 8 3 5.44 3.41 -4 8 3 20.47 5.87 4 8 4 27.37 6.13 -4 8 4 8.58 3.81 4 8 4 22.61 4.83 4 -8 4 12.42 4.63 -4 8 5 33.32 6.73 4 8 5 44.79 7.09 4 8 5 30.96 7.18 4 -8 5 31.76 6.03 4 8 6 136.06 13.05 4 8 6 133.23 13.57 4 -8 6 103.22 11.73 -4 8 6 122.67 12.55 4 8 7 80.32 9.98 -4 8 7 97.12 11.30 4 -8 7 96.15 11.02 4 8 7 91.24 11.15 4 8 8 8.34 4.05 -4 8 8 10.56 4.78 4 8 8 2.46 2.45 4 -8 8 0.85 1.71 4 8 9 37.24 7.64 4 8 9 22.68 5.70 4 -8 9 22.37 6.29 -4 8 9 23.92 6.06 4 -8 10 124.32 13.10 4 8 10 158.69 14.76 -4 8 10 137.34 13.61 4 8 10 140.16 13.63 4 8 11 7.57 2.28 4 8 11 4.95 3.08 -4 8 11 5.99 3.24 4 -8 11 4.52 3.75 -4 8 12 4.82 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131.31 11.05 5 3 14 114.81 9.10 5 -3 15 619.52 23.14 5 3 15 567.87 20.46 5 3 15 557.10 23.75 5 3 16 166.97 11.27 5 3 16 176.71 13.75 5 -3 16 190.21 12.98 5 3 17 21.26 4.70 5 3 17 26.52 4.92 5 -3 17 19.47 4.54 5 3 18 18.54 4.52 5 -3 18 25.09 5.49 5 3 19 138.85 12.96 5 3 20 85.10 10.65 5 3 21 143.92 13.49 5 3 22 142.50 13.81 5 3 23 4.50 3.05 5 3 24 14.16 5.41 5 3 25 150.22 14.95 5 -4 -28 2.23 3.25 5 -4 -27 -0.33 2.11 5 -4 -26 1.69 2.48 5 -4 -25 12.03 4.78 5 -4 -24 61.31 9.62 5 -4 -23 29.33 7.07 5 -4 -22 11.57 4.53 5 -4 -21 25.17 5.23 5 -4 -20 67.88 9.45 5 -4 -20 69.67 9.59 5 -4 -19 2.09 1.73 5 -4 -19 6.27 2.93 5 -4 -18 7.35 3.18 -5 -4 -18 5.86 3.50 5 -4 -18 11.80 4.22 -5 -4 -17 304.50 18.43 5 -4 -17 312.59 19.21 5 -4 -17 261.57 17.74 -5 -4 -16 96.41 10.36 5 -4 -16 112.17 10.80 5 4 -16 109.61 10.08 5 -4 -16 101.37 10.76 -5 -4 -15 39.26 7.01 5 -4 -15 42.40 6.91 5 4 -15 44.29 6.66 5 -4 -15 41.08 7.25 5 4 -14 27.63 5.28 5 -4 -14 18.67 4.90 5 -4 -14 19.02 4.78 -5 -4 -14 20.40 4.79 5 -4 -13 111.55 10.80 -5 -4 -13 99.85 9.83 5 -4 -13 112.62 10.71 5 4 -13 115.02 10.16 -5 -4 -12 182.03 12.98 5 -4 -12 187.40 13.84 5 -4 -12 156.85 12.73 5 4 -12 165.75 12.19 5 -4 -11 38.16 6.28 5 -4 -11 34.94 6.11 -5 4 -11 33.69 4.47 5 4 -11 43.98 6.01 5 4 -10 14.95 3.96 -5 4 -10 13.66 2.89 5 -4 -10 12.11 3.82 5 -4 -10 16.60 4.46 5 4 -9 129.01 10.34 5 4 -9 136.10 7.45 5 -4 -9 142.91 11.77 5 -4 -9 117.78 10.47 -5 4 -8 22.04 3.90 5 -4 -8 22.19 4.43 5 4 -8 26.87 4.64 5 4 -8 25.53 3.42 5 -4 -8 22.77 4.59 5 4 -7 55.46 7.18 -5 4 -7 94.71 7.72 5 -4 -7 77.04 8.22 5 -4 -7 80.22 8.35 5 4 -7 66.67 5.77 5 -4 -6 242.81 14.46 5 4 -6 224.19 10.75 5 4 -6 229.51 13.57 5 -4 -6 234.78 14.65 5 4 -5 66.89 7.38 5 -4 -5 95.78 9.02 5 4 -5 65.32 3.03 5 4 -5 76.82 6.35 5 -4 -5 85.48 8.64 5 4 -4 101.88 4.55 5 4 -4 128.76 9.94 5 4 -4 107.84 7.83 5 -4 -4 124.66 10.29 5 -4 -4 127.00 10.25 5 4 -3 6.81 1.31 5 4 -3 7.16 2.23 5 4 -3 7.15 2.68 5 -4 -3 6.90 2.93 5 -4 -3 8.20 2.82 5 4 -2 38.13 4.86 5 4 -2 31.77 4.66 5 -4 -2 34.56 5.25 5 -4 -2 26.96 4.62 5 -4 -1 3.02 2.20 5 4 -1 3.33 1.90 5 4 -1 6.83 2.31 5 -4 -1 4.82 1.65 5 4 0 127.60 9.33 5 4 0 111.70 9.19 5 -4 0 131.29 9.85 5 -4 0 126.10 10.05 5 -4 1 6.87 2.81 5 4 1 4.63 1.80 5 4 1 8.38 2.68 5 -4 1 5.71 2.24 5 -4 2 29.22 4.81 5 4 2 36.22 5.43 5 4 2 34.65 5.11 5 -4 2 26.22 4.41 5 -4 3 11.87 3.42 5 4 3 10.41 3.80 5 4 3 1.63 1.05 5 -4 3 11.87 3.19 5 -4 4 114.72 9.66 5 4 4 113.89 9.43 5 4 4 116.67 9.37 5 -4 4 110.99 9.09 5 -4 5 81.39 8.19 5 4 5 58.56 6.84 5 4 5 76.84 7.77 5 -4 5 78.60 7.59 5 -4 6 234.51 13.79 5 4 6 227.42 13.89 5 4 6 242.71 13.81 5 4 7 66.21 7.17 5 -4 7 70.52 7.91 5 4 7 84.04 8.27 5 -4 8 23.42 4.80 5 4 8 31.49 4.79 5 4 8 21.90 4.38 5 4 9 146.46 11.49 5 -4 9 133.60 10.57 5 4 9 128.29 10.23 5 -4 10 16.06 4.10 5 4 10 14.29 3.71 5 4 10 12.88 3.54 5 -4 11 45.51 6.27 5 4 11 50.61 6.56 5 4 11 47.68 6.61 5 -4 12 168.50 12.13 5 4 12 179.88 12.54 5 4 12 162.20 12.86 5 -4 13 115.26 10.05 5 4 13 126.77 10.67 5 4 13 118.31 10.81 5 4 14 27.30 5.79 5 4 14 15.09 3.72 5 -4 14 25.98 4.90 5 -4 15 40.59 6.17 5 4 15 47.14 6.76 5 4 15 49.19 7.44 5 -4 16 102.24 9.96 5 4 16 101.16 9.72 5 4 16 117.84 11.37 5 -4 17 262.49 15.89 5 4 17 293.38 16.85 5 4 17 282.13 17.65 5 4 18 9.95 4.07 5 4 19 8.69 3.51 5 4 20 71.86 9.68 5 4 21 22.50 5.43 5 4 22 6.46 2.91 5 4 23 26.88 6.99 5 4 24 46.43 8.42 5 4 25 3.83 2.53 5 4 26 2.03 3.25 5 -5 -27 2.55 2.07 5 -5 -26 17.78 5.64 5 -5 -25 13.82 4.32 5 -5 -24 58.04 9.39 5 -5 -23 14.97 5.93 5 -5 -22 6.28 3.31 5 -5 -21 40.82 7.80 -5 -5 -20 106.29 12.19 5 -5 -20 95.59 10.95 5 -5 -20 124.87 13.18 -5 -5 -19 8.50 3.16 5 -5 -19 13.35 3.57 5 -5 -19 7.03 3.14 5 -5 -18 12.32 4.15 5 -5 -18 2.00 1.66 -5 -5 -18 8.73 4.01 5 -5 -17 76.05 10.07 -5 -5 -17 62.35 8.87 5 -5 -17 74.03 10.05 5 5 -16 3.53 2.52 5 -5 -16 1.08 3.96 -5 -5 -16 4.19 2.55 5 -5 -16 -0.05 2.80 -5 -5 -15 147.21 12.66 5 -5 -15 173.80 14.46 5 -5 -15 161.27 13.93 5 -5 -14 75.09 9.63 -5 -5 -14 58.88 7.85 5 5 -14 56.13 7.70 5 -5 -14 48.94 7.83 5 5 -13 0.93 1.32 -5 -5 -13 3.27 1.60 5 -5 -13 -1.44 1.98 5 -5 -13 6.10 3.25 5 5 -12 26.77 5.45 -5 -5 -12 34.67 5.59 5 -5 -12 25.99 5.69 5 -5 -12 20.33 4.64 -5 5 -11 172.14 11.46 -5 -5 -11 172.75 12.96 5 -5 -11 172.89 13.65 5 -5 -11 184.42 14.39 5 5 -11 178.44 13.69 5 5 -10 47.23 7.10 5 -5 -10 55.60 7.75 -5 5 -10 48.99 6.29 5 -5 -10 58.78 8.05 -5 -5 -10 67.27 7.99 5 5 -9 100.41 10.32 -5 5 -9 101.43 9.12 5 -5 -9 119.19 11.07 5 -5 -9 107.36 10.98 5 5 -8 24.46 4.98 5 5 -8 22.30 3.54 5 -5 -8 30.15 5.94 5 -5 -8 25.82 5.45 -5 5 -8 20.72 4.23 5 5 -7 28.69 5.67 5 -5 -7 21.62 5.05 -5 5 -7 23.66 4.25 5 5 -7 32.19 4.64 5 -5 -7 16.80 4.52 5 5 -6 356.74 18.09 5 -5 -6 297.47 16.80 -5 5 -6 356.30 16.97 5 5 -6 338.81 14.91 5 -5 -6 339.39 18.55 5 -5 -5 191.02 13.15 5 5 -5 189.00 11.84 5 5 -5 191.25 13.25 -5 5 -5 204.61 12.70 5 -5 -5 201.31 14.30 5 5 -4 11.62 4.15 -5 5 -4 14.08 3.38 5 -5 -4 10.49 3.29 5 5 -4 9.44 2.81 5 -5 -4 11.93 3.78 5 5 -3 38.51 5.43 5 5 -3 48.59 6.22 -5 5 -3 57.94 6.68 5 -5 -3 37.50 5.91 5 -5 -3 34.32 5.94 5 5 -2 39.95 5.81 5 5 -2 32.44 4.81 5 -5 -2 39.58 6.13 5 -5 -2 33.75 5.65 5 5 -1 55.33 7.09 5 5 -1 84.37 8.11 5 -5 -1 63.59 7.35 5 -5 -1 81.34 8.82 5 5 0 235.76 14.42 5 5 0 211.07 13.11 5 -5 0 219.91 14.36 5 -5 0 218.86 13.59 5 5 1 65.91 7.49 5 5 1 66.86 7.46 5 -5 1 69.31 7.43 5 -5 1 63.27 7.58 5 5 2 39.94 6.20 5 5 2 32.73 5.11 5 -5 2 30.36 5.14 5 -5 2 41.84 6.00 5 5 3 41.07 5.61 5 5 3 46.85 6.57 5 -5 3 51.40 6.19 5 -5 3 41.24 6.23 5 -5 4 17.08 4.08 5 5 4 8.08 1.80 5 -5 4 13.95 3.41 5 5 4 15.81 3.66 5 5 5 157.25 11.89 5 5 5 188.07 13.02 5 -5 5 173.32 11.82 5 -5 5 166.61 12.31 5 5 6 371.40 18.47 5 5 6 353.59 18.17 5 -5 6 354.56 17.27 5 -5 6 357.21 18.11 5 5 7 30.82 5.93 5 -5 7 35.53 5.46 5 5 7 33.02 5.98 5 -5 7 26.97 5.10 5 -5 8 20.15 4.43 5 5 8 33.85 5.99 5 5 8 31.59 5.57 5 -5 8 16.85 4.01 5 -5 9 100.76 9.61 5 5 9 133.62 11.20 5 5 9 99.11 10.17 5 -5 9 113.28 10.22 5 5 10 48.90 6.62 5 5 10 41.85 6.47 5 -5 10 62.65 7.60 5 -5 11 171.59 12.98 5 5 11 191.97 13.64 5 5 11 190.52 14.32 5 -5 12 18.55 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7.17 -5 -6 -15 45.99 7.81 5 -6 -15 46.93 8.36 5 6 -14 10.57 3.69 -5 -6 -14 15.47 4.41 5 -6 -14 11.64 4.36 5 -6 -14 10.00 4.30 5 -6 -13 20.14 5.70 5 6 -13 16.38 4.83 -5 -6 -13 17.87 5.06 5 -6 -13 12.45 4.21 5 6 -12 85.51 9.75 -5 -6 -12 86.19 9.64 5 -6 -12 80.60 9.79 5 -6 -12 56.49 8.36 5 6 -11 8.81 3.61 -5 -6 -11 14.53 4.05 5 -6 -11 10.95 3.96 5 -6 -11 13.04 4.98 5 6 -10 6.17 2.77 -5 -6 -10 4.30 2.61 5 -6 -10 2.30 1.72 -5 6 -10 9.82 3.68 5 -6 -10 4.00 1.47 5 -6 -9 53.95 8.08 5 -6 -9 46.09 7.01 -5 6 -9 40.99 6.36 5 6 -9 45.21 7.15 5 -6 -8 38.51 6.62 5 6 -8 29.72 5.93 -5 6 -8 32.58 5.82 5 -6 -8 45.34 7.57 5 6 -7 86.25 8.18 -5 6 -7 91.12 9.19 5 -6 -7 99.65 10.41 5 -6 -7 80.06 9.73 5 6 -7 103.03 10.74 5 6 -6 2.57 2.42 5 6 -6 12.43 3.45 -5 6 -6 5.99 2.72 5 -6 -6 7.29 2.68 5 -6 -6 5.94 3.66 5 -6 -5 8.17 3.36 5 6 -5 12.65 4.39 -5 6 -5 15.30 3.81 5 6 -5 12.87 3.68 5 6 -4 128.79 11.54 5 -6 -4 117.70 10.57 5 6 -4 138.43 10.82 -5 6 -4 125.33 10.88 5 -6 -4 131.44 12.27 5 -6 -3 26.34 4.99 5 6 -3 31.26 6.01 5 6 -3 29.52 5.12 -5 6 -3 20.65 5.13 5 -6 -3 41.14 6.70 5 6 -2 69.38 8.41 5 6 -2 72.40 8.06 -5 6 -2 83.75 8.74 5 -6 -2 57.68 7.70 5 -6 -2 68.27 9.13 5 6 -1 74.06 8.71 5 -6 -1 70.65 7.67 5 6 -1 66.62 7.82 -5 6 -1 64.89 8.14 5 -6 -1 87.80 9.72 5 6 0 84.78 9.43 5 -6 0 65.39 7.48 5 6 0 73.74 8.21 -5 6 0 75.38 8.54 5 -6 0 88.94 9.52 5 6 1 69.34 8.67 5 -6 1 80.08 8.85 5 6 1 84.62 8.80 -5 6 1 77.93 9.08 5 -6 1 72.44 8.88 5 -6 2 64.19 8.63 5 6 2 69.67 8.21 5 6 2 71.68 8.25 -5 6 2 67.43 8.09 5 -6 2 78.42 8.61 5 -6 3 28.85 5.94 5 -6 3 36.90 5.65 5 6 3 32.13 6.26 5 6 3 34.10 5.73 -5 6 3 35.23 6.39 5 -6 4 117.65 10.62 5 6 4 127.10 11.53 5 6 4 135.75 11.74 5 -6 4 137.66 12.09 -5 6 4 139.08 11.84 5 -6 5 10.46 3.50 5 6 5 16.41 4.53 5 6 5 13.28 4.34 5 -6 5 10.31 2.92 5 6 6 3.70 3.00 5 -6 6 3.34 1.49 5 6 6 8.69 3.53 5 -6 6 7.49 2.00 5 6 7 114.42 11.01 5 6 7 103.10 10.37 5 -6 7 96.22 9.95 5 -6 7 95.65 9.83 5 -6 8 34.27 6.03 5 6 8 44.89 6.63 5 -6 8 30.99 5.37 5 6 8 29.02 5.76 5 -6 9 46.25 7.07 5 6 9 48.52 7.69 5 6 9 40.76 6.32 5 -6 9 33.48 5.92 5 6 10 3.26 1.73 5 -6 10 4.22 2.11 5 -6 11 8.96 3.71 5 6 11 15.36 4.45 5 6 11 11.08 3.49 5 -6 11 6.87 2.95 5 6 12 70.14 9.27 5 -6 12 72.24 9.27 5 6 12 91.52 10.63 5 -6 12 61.02 8.92 5 6 13 22.81 5.18 5 6 13 9.86 3.45 5 -6 13 15.02 4.80 -5 6 13 16.85 4.58 5 -6 13 12.85 4.51 5 6 14 8.69 2.78 5 6 14 7.85 2.83 -5 6 14 9.52 3.45 5 -6 14 18.46 5.11 5 6 15 46.73 7.43 5 6 15 39.11 7.02 -5 6 15 25.43 5.87 5 6 16 22.38 5.38 5 6 16 32.58 6.92 -5 6 16 31.01 6.51 5 6 17 6.89 2.29 5 6 17 14.25 5.12 -5 6 17 6.31 4.88 5 6 18 4.68 2.87 5 6 18 9.78 3.33 -5 6 18 10.42 4.92 5 6 19 2.73 3.48 -5 6 19 5.66 3.96 -5 6 20 2.50 3.50 5 6 20 2.87 2.44 -5 6 21 4.50 4.40 5 6 21 -0.51 2.28 -5 6 22 18.70 6.24 5 6 22 10.83 3.70 -5 6 23 -6.34 3.91 5 6 23 0.43 3.25 5 6 24 10.48 4.65 5 6 25 -0.38 2.06 5 -7 -23 -1.29 3.77 5 -7 -22 6.19 3.24 5 -7 -21 48.34 9.10 5 -7 -20 21.65 5.44 -5 -7 -19 29.49 6.97 5 -7 -19 41.85 8.03 5 -7 -19 35.93 8.18 -5 -7 -18 37.35 7.02 5 -7 -18 60.04 9.24 5 -7 -18 41.52 8.24 -5 -7 -17 40.44 7.37 5 -7 -17 62.46 9.10 5 -7 -17 45.82 8.72 5 -7 -16 62.47 10.01 -5 -7 -16 47.93 8.16 5 -7 -16 69.04 9.67 -5 -7 -15 3.11 2.40 5 -7 -15 6.54 1.93 5 -7 -15 7.03 3.91 5 7 -14 27.74 6.19 -5 -7 -14 16.08 4.47 5 -7 -14 18.85 5.87 5 -7 -14 34.67 7.44 5 7 -13 20.94 5.25 -5 -7 -13 28.47 5.69 5 -7 -13 33.42 6.95 5 7 -12 29.62 6.71 -5 -7 -12 25.46 6.33 5 -7 -12 32.22 6.79 5 -7 -12 29.31 6.69 5 7 -11 102.30 11.55 -5 -7 -11 121.68 11.73 5 -7 -11 95.48 11.06 5 -7 -11 97.88 11.51 5 7 -10 162.16 14.10 -5 7 -10 148.13 12.98 5 -7 -10 170.45 14.69 5 -7 -10 152.42 14.58 -5 -7 -10 166.03 14.17 5 7 -9 130.83 12.86 5 -7 -9 96.85 11.01 -5 7 -9 105.05 10.99 5 -7 -9 90.92 10.84 5 7 -8 96.31 10.86 5 -7 -8 106.44 11.41 -5 7 -8 101.88 10.81 5 -7 -8 99.66 11.17 5 7 -7 121.36 12.20 5 -7 -7 118.75 11.74 -5 7 -7 109.31 11.02 5 -7 -7 119.32 12.06 5 7 -6 62.00 8.82 -5 7 -6 46.07 6.96 5 -7 -6 45.48 8.14 5 7 -6 63.87 7.85 5 -7 -6 58.46 8.06 5 -7 -5 123.17 12.23 5 7 -5 119.50 11.79 5 7 -5 98.99 9.99 -5 7 -5 114.79 11.28 5 -7 -5 122.32 11.55 5 7 -4 24.27 6.07 5 7 -4 30.78 6.01 -5 7 -4 37.37 6.98 5 -7 -4 46.90 7.50 5 -7 -4 42.63 7.38 -5 7 -3 9.65 4.10 5 7 -3 5.50 2.24 5 -7 -3 3.10 2.66 5 7 -3 6.06 2.82 5 -7 -3 4.50 2.49 5 -7 -2 30.66 5.85 5 7 -2 31.46 5.79 5 7 -2 40.33 7.20 -5 7 -2 35.97 6.66 5 -7 -2 43.72 7.32 5 -7 -1 100.79 10.30 5 7 -1 107.75 10.96 -5 7 -1 108.04 11.21 5 7 -1 106.10 10.39 5 -7 -1 115.05 11.87 5 -7 0 24.86 5.54 5 7 0 9.36 3.41 5 7 0 14.70 4.33 5 -7 0 15.69 4.14 -5 7 0 14.79 4.27 5 7 1 86.60 9.99 5 7 1 98.22 10.29 5 -7 1 96.21 10.81 -5 7 1 103.61 10.64 5 -7 1 85.28 9.22 5 -7 2 35.09 6.25 5 7 2 22.74 4.97 5 7 2 43.50 6.75 -5 7 2 40.33 7.30 5 -7 2 29.78 5.84 5 -7 3 10.08 3.83 5 7 3 5.74 3.13 5 7 3 5.09 3.41 5 -7 3 2.50 1.84 -5 7 3 6.28 3.32 5 -7 4 26.85 5.62 5 7 4 23.72 5.05 5 7 4 44.22 6.97 -5 7 4 40.53 7.31 5 -7 4 39.70 6.65 -5 7 5 102.97 11.14 5 7 5 116.82 11.92 5 7 5 100.98 10.63 5 -7 5 137.30 11.97 5 -7 5 101.24 10.99 5 7 6 53.86 7.87 5 7 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9.42 6 -1 -4 147.73 9.93 6 1 -3 97.59 7.13 6 1 -3 96.87 6.75 6 1 -3 101.33 7.79 6 -1 -3 118.07 8.32 6 -1 -3 96.98 7.91 6 1 -2 2.72 1.48 6 1 -2 1.60 1.05 6 -1 -2 1.28 0.86 6 -1 -2 3.08 1.68 6 1 -2 4.35 1.97 6 1 -1 9.11 2.39 6 1 -1 14.56 2.96 6 -1 -1 16.44 3.01 6 -1 -1 21.35 3.74 6 1 0 3.63 1.51 6 1 0 4.09 2.05 6 -1 0 2.09 1.04 6 -1 0 1.76 0.80 6 1 1 16.16 2.96 6 -1 1 17.98 3.21 6 1 1 14.06 2.91 6 1 2 1.95 1.22 6 -1 2 1.62 1.75 6 1 2 2.41 1.53 6 1 3 98.83 7.58 6 -1 3 108.98 8.19 6 1 3 101.38 7.33 6 1 4 141.34 9.30 6 -1 4 139.91 9.29 6 1 4 143.30 8.58 6 1 5 725.84 21.71 6 1 5 721.11 19.08 6 -1 5 722.79 21.39 6 1 6 531.45 16.12 6 1 6 539.48 18.95 6 -1 6 508.71 18.27 6 1 7 352.93 13.00 6 1 7 337.22 15.18 6 -1 7 342.29 15.15 6 1 8 35.28 4.09 6 1 8 45.88 5.71 6 -1 8 43.38 5.70 6 1 9 61.81 5.34 6 1 9 50.69 6.16 6 -1 9 54.68 6.49 6 -1 10 6.01 1.88 6 1 10 5.29 1.55 6 1 10 7.20 2.64 6 -1 11 87.02 8.14 6 1 11 104.72 8.99 6 1 11 97.35 6.64 6 -1 12 97.29 8.64 6 1 12 77.38 8.12 6 1 12 88.77 6.38 6 1 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593.73 24.45 6 -2 -14 585.61 22.49 6 2 -14 611.76 22.70 6 2 -13 60.72 6.83 6 -2 -13 40.45 6.03 6 -2 -13 53.70 6.80 6 2 -13 55.63 6.62 6 2 -12 91.82 7.98 6 2 -12 112.13 9.25 6 -2 -12 111.95 9.53 6 -2 -12 91.41 9.44 6 2 -11 90.75 7.60 6 -2 -11 88.01 8.96 6 -2 -11 91.91 8.40 6 2 -11 91.83 8.38 6 2 -10 61.96 4.46 6 -2 -10 61.41 7.30 6 2 -10 57.60 6.05 6 -2 -10 53.30 6.57 6 2 -10 60.58 6.89 6 2 -9 3.90 1.83 6 -2 -9 7.01 2.53 6 -2 -9 5.99 2.62 6 2 -9 5.39 2.00 6 2 -9 5.00 1.24 6 2 -8 18.76 4.02 6 2 -8 18.17 2.64 6 2 -8 14.52 2.98 6 -2 -8 22.43 4.11 6 -2 -8 23.28 4.10 6 2 -7 9.45 2.03 6 -2 -7 13.77 3.31 6 2 -7 7.98 1.78 6 -2 -7 15.39 3.32 6 2 -7 10.79 2.31 6 -2 -6 252.26 13.30 6 2 -6 247.82 13.15 6 2 -6 235.31 10.73 6 -2 -6 239.79 13.65 6 2 -6 248.29 10.24 6 2 -5 65.29 6.64 6 -2 -5 62.44 6.62 6 2 -5 87.20 6.23 6 2 -5 63.42 5.49 6 -2 -5 74.70 7.64 6 2 -4 5.17 2.22 6 -2 -4 3.99 1.97 6 2 -4 3.64 1.04 6 -2 -4 5.16 2.27 6 2 -4 8.04 2.06 6 2 -3 51.14 5.94 6 2 -3 52.28 4.93 6 -2 -3 49.02 5.80 6 -2 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2 15 173.76 13.25 6 -2 15 147.64 11.50 6 2 16 220.65 15.53 6 -2 16 214.85 14.39 6 -2 17 0.55 1.18 6 2 17 3.47 1.76 6 2 18 33.87 5.83 6 -2 18 25.52 4.96 6 2 19 1.17 1.42 6 -2 19 1.47 1.79 6 -2 20 34.92 6.05 6 2 20 24.47 5.33 6 2 21 4.02 3.41 6 2 22 8.23 3.90 6 2 23 2.97 2.77 6 2 24 59.63 9.18 6 2 25 5.71 3.57 6 -3 -28 3.65 2.01 6 -3 -27 17.03 5.32 6 -3 -26 16.78 5.80 6 -3 -25 56.12 9.19 6 -3 -24 12.87 5.17 6 -3 -23 8.65 4.21 6 -3 -22 7.32 2.55 6 -3 -21 10.53 3.46 6 -3 -20 36.82 6.77 6 -3 -19 107.25 11.77 6 -3 -18 51.77 8.18 6 -3 -18 51.22 7.72 6 -3 -17 146.79 12.67 6 3 -17 141.40 11.99 6 -3 -17 119.33 11.76 6 -3 -16 65.66 8.97 6 -3 -16 49.18 7.55 6 3 -16 79.84 8.66 6 -3 -15 38.05 6.51 6 -3 -15 28.13 5.47 6 3 -15 27.93 5.21 6 -3 -14 185.28 14.23 6 3 -14 199.85 13.40 6 -3 -14 220.59 14.81 6 -3 -13 68.29 8.17 6 3 -13 52.77 5.57 6 -3 -13 65.49 8.29 6 3 -13 68.05 7.83 6 -3 -12 82.27 9.58 6 3 -12 80.50 6.81 6 -3 -12 78.92 8.77 6 3 -12 77.70 8.33 6 3 -11 180.77 9.73 -6 3 -11 158.18 8.46 6 -3 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101.95 11.21 6 3 20 43.90 7.82 6 3 21 4.42 3.52 6 3 22 -0.16 1.96 6 3 23 5.38 3.31 6 3 24 5.83 2.85 6 3 25 49.37 9.29 6 3 26 27.38 7.11 6 -4 -27 -0.33 2.76 6 -4 -26 10.30 2.98 6 -4 -25 5.03 2.35 6 -4 -24 72.52 11.11 6 -4 -23 24.52 5.49 6 -4 -22 26.24 6.12 6 -4 -21 39.31 7.76 6 -4 -20 36.59 7.66 6 -4 -20 28.34 6.02 6 -4 -19 3.80 3.69 6 -4 -19 0.69 2.51 6 -4 -18 222.98 16.65 6 -4 -18 217.39 16.57 6 -4 -17 59.64 8.70 6 -4 -17 72.55 9.31 6 4 -17 70.90 8.72 6 -4 -16 38.16 6.29 6 -4 -16 44.44 7.27 6 4 -16 50.73 7.56 6 -4 -15 50.98 7.69 6 4 -15 49.51 7.03 6 -4 -15 49.57 7.89 6 4 -14 12.12 3.18 6 -4 -14 8.13 3.24 6 -4 -14 12.51 4.44 6 -4 -13 81.79 9.56 6 -4 -13 90.34 10.20 6 4 -13 87.99 9.17 6 -4 -12 441.69 21.91 6 -4 -12 396.84 20.61 6 4 -12 378.19 18.77 -6 4 -11 143.65 9.72 6 -4 -11 174.02 13.39 6 -4 -11 135.40 12.23 6 4 -11 151.46 11.93 6 4 -10 36.53 6.02 -6 4 -10 34.02 4.52 6 -4 -10 49.04 7.26 6 -4 -10 38.87 6.30 6 4 -9 113.39 10.03 6 4 -9 117.35 7.41 6 -4 -9 125.03 11.18 -6 4 -9 112.82 8.54 6 -4 -9 105.22 10.28 6 4 -8 461.93 15.67 6 -4 -8 511.79 22.17 6 4 -8 511.45 21.25 6 -4 -8 487.30 22.18 6 4 -7 35.26 5.73 6 4 -7 31.45 4.22 6 -4 -7 36.53 5.96 6 -4 -7 37.22 6.03 6 4 -6 67.94 7.97 6 4 -6 72.88 4.49 6 4 -6 72.15 6.54 6 -4 -6 75.87 8.61 6 -4 -6 73.71 8.61 6 4 -5 521.20 21.30 6 -4 -5 523.63 21.68 6 4 -5 530.84 12.35 6 4 -5 523.77 17.72 6 -4 -5 547.28 22.44 6 -4 -4 1.82 1.86 6 4 -4 2.72 1.98 6 4 -4 0.88 1.21 6 4 -4 0.40 0.65 6 -4 -4 2.42 2.49 6 4 -3 192.29 12.98 6 -4 -3 201.18 13.33 6 4 -3 235.58 12.37 6 4 -3 232.30 8.92 6 -4 -3 216.63 13.75 6 4 -2 111.77 9.69 6 4 -2 100.19 8.48 6 -4 -2 118.52 10.38 6 -4 -2 104.61 9.56 6 4 -1 88.66 8.51 6 4 -1 93.20 7.82 6 -4 -1 73.75 8.07 6 -4 -1 85.95 8.71 6 -4 0 117.27 10.12 6 4 0 137.04 10.51 6 -4 0 139.58 10.66 6 4 0 140.18 9.91 6 -4 1 86.87 8.60 6 4 1 94.44 8.80 6 -4 1 91.12 8.85 6 4 1 74.88 7.53 6 -4 2 110.62 9.87 6 4 2 106.45 9.11 6 4 2 115.10 9.83 6 -4 2 88.03 8.58 6 -4 3 215.68 13.90 6 4 3 212.19 13.27 6 -4 3 231.75 13.84 6 4 3 227.13 13.55 6 4 4 3.02 1.47 6 4 4 2.28 1.60 6 -4 4 3.29 2.08 6 -4 4 3.30 1.60 6 -4 5 506.29 21.27 6 4 5 551.38 21.26 6 -4 5 489.98 20.35 6 4 5 522.84 20.97 6 -4 6 81.55 8.57 6 4 6 76.86 8.14 6 -4 6 70.79 7.63 6 4 6 83.85 8.56 6 -4 7 36.01 5.81 6 4 7 27.53 4.88 6 4 7 29.92 5.45 6 4 8 488.34 20.36 6 -4 8 463.18 20.40 6 4 8 504.83 21.48 6 4 9 128.58 10.48 6 -4 9 120.83 10.38 6 4 9 133.45 11.01 6 4 10 30.69 5.26 6 -4 10 36.45 5.59 6 4 10 42.21 6.83 6 4 11 161.84 11.69 6 -4 11 143.99 11.68 6 4 11 154.97 12.17 6 4 12 391.58 18.69 6 4 12 393.67 20.07 6 -4 12 387.76 19.36 6 4 13 67.30 7.90 6 -4 13 61.32 7.66 6 4 13 81.87 9.74 6 4 14 16.71 3.81 6 -4 14 16.42 3.99 6 4 14 5.67 3.63 6 4 15 56.18 7.03 6 -4 15 39.34 6.33 6 4 15 42.07 6.90 6 4 16 37.52 6.16 6 -4 16 50.00 7.59 6 4 16 45.24 7.68 6 4 17 69.42 8.55 6 -4 17 57.88 8.34 6 4 17 62.45 8.95 6 4 18 246.22 17.57 6 4 19 2.15 2.06 6 4 20 19.38 5.37 6 4 21 30.58 6.88 6 4 22 23.77 5.79 6 4 23 26.85 6.16 6 4 24 48.84 8.53 6 4 25 10.60 5.47 6 4 26 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8.32 3.12 6 5 -6 7.90 2.18 6 5 -6 13.04 2.99 6 -5 -6 12.63 4.39 6 5 -5 43.58 6.63 6 -5 -5 29.77 5.98 6 5 -5 39.37 5.36 6 -5 -5 43.21 6.83 6 5 -4 98.20 9.52 6 -5 -4 99.04 9.47 6 -5 -4 86.02 9.58 6 5 -4 94.28 8.29 6 5 -3 93.13 9.45 6 -5 -3 96.97 9.92 6 -5 -3 91.08 9.56 6 5 -3 90.79 8.29 6 5 -2 71.58 8.20 6 -5 -2 62.09 7.83 6 -5 -2 74.87 8.56 6 5 -2 73.93 7.67 6 -5 -1 22.81 5.32 6 5 -1 23.01 4.22 6 -5 -1 20.96 4.43 6 5 -1 33.65 5.48 6 5 0 22.62 4.79 6 -5 0 25.23 5.33 6 5 0 19.70 4.82 6 -5 0 25.26 4.92 6 5 1 19.48 4.23 6 5 1 22.51 4.34 6 -5 1 29.12 5.90 6 -5 1 24.87 5.44 6 5 2 82.78 8.50 6 5 2 74.07 8.30 6 -5 2 67.90 7.64 6 -5 2 65.78 8.18 6 5 3 98.93 9.60 6 -5 3 92.60 9.38 6 -5 3 73.65 8.33 6 5 4 83.97 8.73 6 5 4 82.33 8.83 6 -5 4 86.87 9.10 6 -5 4 91.59 9.25 6 5 5 38.75 6.36 6 -5 5 45.21 6.77 6 5 5 42.88 6.36 6 -5 5 27.84 5.09 6 -5 6 5.68 1.17 6 5 6 11.20 3.67 6 5 6 13.96 3.92 6 -5 6 8.01 3.13 6 -5 7 19.51 4.74 6 5 7 21.97 5.29 6 5 7 23.51 4.99 6 -5 7 19.21 4.41 6 5 8 33.41 5.62 6 -5 8 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344.60 17.97 6 6 -2 329.05 18.62 6 -6 -2 386.81 20.01 -6 6 -2 336.62 18.19 6 -6 -2 338.54 19.50 6 6 -1 65.35 7.81 6 6 -1 81.49 9.18 6 -6 -1 53.00 7.39 -6 6 -1 76.47 8.60 6 -6 -1 66.85 9.02 6 -6 0 5.60 3.63 6 6 0 5.29 1.88 6 6 0 4.26 2.30 6 -6 0 2.51 1.41 6 6 1 90.29 9.86 6 6 1 64.78 8.15 6 -6 1 79.10 8.79 6 -6 1 71.92 8.98 6 6 2 358.41 19.69 6 6 2 334.47 18.22 6 -6 2 341.82 18.45 6 -6 2 344.17 19.45 6 -6 3 2.20 2.38 6 6 3 3.25 2.97 6 6 3 7.57 2.91 6 -6 3 0.82 2.16 6 6 4 196.80 14.59 6 6 4 182.29 13.71 6 -6 4 179.97 13.66 6 -6 4 198.21 14.63 6 6 5 56.57 7.88 6 6 5 53.18 7.81 6 -6 5 62.97 8.02 6 -6 5 52.36 7.52 6 -6 6 1.72 2.40 6 6 6 -1.83 2.60 6 6 6 0.20 1.65 6 -6 6 -0.36 1.88 6 6 7 65.84 8.51 6 6 7 67.15 8.80 6 -6 7 63.80 8.27 6 -6 7 68.44 9.03 6 -6 8 389.21 21.03 6 6 8 387.19 20.92 6 -6 8 390.06 20.05 6 6 8 384.02 20.78 6 6 9 50.98 7.74 6 -6 9 32.70 6.22 6 6 9 43.02 7.12 6 -6 9 36.47 5.95 6 -6 10 5.29 3.57 6 6 10 6.00 3.46 6 6 10 1.95 1.40 6 -6 10 2.43 1.72 6 6 11 32.43 6.84 6 6 11 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49.79 7.05 7 5 -2 298.53 17.22 7 5 -2 326.72 16.39 7 -5 -2 308.40 18.04 7 -5 -1 9.49 3.85 7 5 -1 18.86 4.83 7 5 -1 12.70 3.24 7 -5 -1 12.52 3.34 7 -5 0 2.65 2.47 7 5 0 5.97 2.51 7 5 0 1.57 2.22 7 -5 0 1.80 1.54 7 -5 1 18.89 4.41 7 5 1 7.80 3.77 7 5 1 12.91 3.58 7 -5 1 16.28 4.45 7 5 2 319.08 17.53 7 -5 2 282.31 16.98 7 5 2 308.03 16.62 7 -5 2 296.67 17.41 7 -5 3 50.61 7.46 7 5 3 57.81 7.85 7 -5 3 69.03 8.09 7 5 3 69.13 8.28 7 5 4 60.80 7.49 7 -5 4 33.71 6.05 7 -5 4 58.82 7.82 7 5 4 54.54 6.98 7 -5 5 35.64 6.73 7 5 5 30.91 5.62 7 -5 5 35.19 6.11 7 5 5 42.43 6.36 7 5 6 14.25 3.80 7 -5 6 10.53 4.07 7 -5 6 8.57 3.55 7 5 6 18.10 4.27 7 -5 7 61.23 8.29 7 5 7 64.25 7.97 7 -5 7 66.15 8.23 7 5 7 65.07 8.07 7 -5 8 270.49 17.03 7 5 8 290.85 16.82 7 -5 8 241.15 15.78 7 5 8 269.89 16.81 7 5 9 13.07 4.02 7 -5 9 16.10 4.71 7 5 9 18.20 4.21 7 -5 9 18.38 4.18 7 5 10 12.91 4.01 7 -5 10 4.59 2.78 7 5 10 5.41 2.69 7 -5 10 7.20 3.52 7 -5 11 40.68 7.10 7 5 11 55.34 7.36 7 5 11 44.78 7.03 7 5 12 267.12 16.64 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11.82 3.64 7 6 3 3.02 2.70 7 -6 3 5.82 2.21 7 6 3 1.70 2.92 7 -6 3 5.05 4.08 7 6 4 13.13 4.59 7 -6 4 19.50 5.08 7 6 4 16.82 3.97 7 -6 4 17.08 5.20 7 6 5 38.64 6.55 7 -6 5 37.98 6.92 7 -6 5 44.34 7.45 7 6 5 39.83 6.74 7 6 6 -0.32 2.20 7 -6 6 3.13 2.79 7 6 6 7.10 3.73 7 -6 6 5.16 4.08 7 6 7 8.94 3.63 7 -6 7 12.78 4.63 7 6 7 8.17 2.59 7 -6 7 3.03 2.43 7 6 8 2.05 2.95 7 -6 8 -0.25 2.00 7 6 8 -0.12 2.43 7 -6 8 0.36 2.81 7 6 9 2.10 2.37 7 -6 9 0.92 1.53 7 6 9 7.64 4.02 7 -6 9 2.44 2.16 7 6 10 12.98 4.22 7 -6 10 12.03 4.08 7 6 10 12.14 4.24 7 -6 10 11.82 3.82 7 -6 11 10.51 4.77 7 6 11 22.60 5.35 7 -6 11 14.61 5.43 7 6 11 21.92 5.63 7 -6 12 7.58 3.58 7 6 12 16.95 4.99 7 -6 12 13.91 4.85 7 6 12 16.55 4.65 7 -6 13 27.43 5.87 7 6 13 41.84 7.32 7 -6 13 46.79 8.48 7 6 13 32.19 6.76 7 -6 14 10.79 3.64 7 6 14 12.69 4.02 7 6 14 8.25 3.48 7 -6 14 14.24 5.09 7 -6 15 6.93 3.52 7 6 15 0.99 2.20 7 6 15 5.11 2.38 7 6 16 2.92 2.30 7 6 16 0.85 1.97 7 6 17 1.82 2.07 7 6 17 -1.29 2.69 7 6 18 0.05 2.88 7 6 19 1.78 2.28 7 6 20 -1.81 3.21 -7 6 21 20.95 5.37 7 6 21 14.99 5.36 7 6 22 0.53 3.39 -7 6 22 3.79 3.90 7 6 23 1.91 2.79 -7 6 23 8.91 3.58 7 6 24 -4.10 3.91 -7 6 24 1.38 3.24 7 -7 -22 15.10 5.58 7 -7 -22 18.35 7.03 7 -7 -21 8.11 3.22 7 -7 -21 1.98 2.70 7 -7 -20 22.13 6.38 7 -7 -20 34.04 8.10 7 -7 -19 -1.12 3.20 7 -7 -19 5.38 4.40 7 -7 -18 128.45 14.36 7 -7 -18 102.71 12.63 7 -7 -17 19.42 6.61 7 -7 -17 22.65 5.35 7 -7 -16 -2.24 3.31 7 -7 -16 -0.17 2.06 7 7 -15 3.48 3.38 7 -7 -15 0.36 4.14 7 -7 -15 0.69 3.04 7 7 -14 28.30 6.42 7 -7 -14 42.95 7.36 7 -7 -14 45.26 8.24 7 7 -13 11.13 4.98 7 -7 -13 3.94 3.19 7 -7 -13 6.37 3.73 7 7 -12 179.54 14.97 7 -7 -12 169.74 15.41 7 -7 -12 160.01 15.20 7 7 -11 8.83 4.19 7 -7 -11 5.08 3.09 7 -7 -11 3.11 3.69 7 7 -10 0.06 2.07 7 -7 -10 1.97 2.53 7 -7 -10 2.70 4.20 -7 7 -9 5.42 2.33 7 -7 -9 4.61 3.51 7 -7 -9 6.22 3.43 7 7 -8 276.51 18.42 7 -7 -8 270.14 19.31 -7 7 -8 283.41 18.33 7 -7 -8 314.83 19.98 7 7 -7 7.88 3.27 -7 7 -7 10.96 3.55 7 -7 -7 12.87 5.35 7 -7 -7 13.49 4.23 7 7 -6 36.90 6.86 -7 7 -6 42.35 7.20 7 -7 -6 41.97 7.71 7 -7 -6 38.24 7.11 -7 7 -5 18.42 4.47 7 7 -5 17.74 5.67 7 -7 -5 14.28 5.04 7 7 -5 22.14 5.08 7 -7 -5 20.94 5.67 7 7 -4 88.65 10.16 -7 7 -4 94.99 10.48 7 -7 -4 97.94 11.05 7 -7 -4 94.04 11.25 7 7 -4 99.15 10.28 7 -7 -3 0.40 3.44 7 7 -3 -1.04 3.25 -7 7 -3 -2.44 2.74 7 -7 -3 -2.67 2.41 7 7 -3 2.45 3.32 7 -7 -2 147.17 13.47 7 7 -2 145.79 13.23 -7 7 -2 153.44 13.58 7 -7 -2 136.55 13.32 7 7 -2 142.01 12.54 7 -7 -1 14.62 4.84 7 7 -1 16.74 4.83 7 7 -1 17.06 4.42 -7 7 -1 23.04 5.20 7 -7 -1 16.54 4.71 7 -7 0 0.06 2.26 7 7 0 2.75 2.09 7 7 0 0.08 1.44 7 -7 0 6.64 4.95 -7 7 0 6.90 4.19 7 -7 1 23.86 5.80 7 7 1 17.34 5.20 7 7 1 22.01 5.44 -7 7 1 11.86 3.19 7 -7 1 27.26 5.63 7 7 2 146.42 12.76 7 7 2 168.64 14.23 -7 7 2 171.23 14.02 7 -7 2 131.44 13.11 7 -7 2 136.68 13.47 7 -7 3 6.64 3.67 7 7 3 -0.99 1.65 7 7 3 1.20 2.43 -7 7 3 1.47 2.19 7 -7 3 1.30 2.08 7 7 4 103.97 11.24 7 7 4 118.99 12.07 -7 7 4 105.97 10.96 7 -7 4 108.52 12.04 7 -7 4 106.43 12.06 7 -7 5 24.76 6.29 7 7 5 14.56 5.52 7 7 5 17.68 5.40 7 -7 5 15.85 5.56 7 7 6 41.47 6.95 7 7 6 44.79 7.33 7 -7 6 36.86 7.53 7 -7 6 46.77 8.39 7 -7 7 8.30 4.41 7 7 7 15.59 4.64 7 7 7 14.64 3.69 7 -7 7 3.82 1.97 7 7 8 290.86 18.92 7 7 8 278.26 18.45 7 -7 8 285.38 19.09 7 -7 8 266.80 18.98 7 -7 9 4.73 3.82 7 7 9 6.53 3.32 7 7 9 3.00 3.14 7 -7 9 13.73 5.53 7 -7 10 -0.86 2.19 7 7 10 -0.39 2.70 7 7 10 -0.89 2.57 7 -7 10 0.35 3.43 7 -7 11 14.07 4.30 7 7 11 7.87 4.37 7 7 11 10.04 4.18 7 7 12 158.31 14.26 7 -7 12 164.98 14.98 7 7 12 147.46 14.66 7 7 13 15.78 5.27 7 -7 13 17.05 5.02 7 7 13 7.28 2.48 -7 7 13 15.80 4.76 7 -7 14 45.76 8.08 7 7 14 36.91 7.17 -7 7 14 30.94 6.79 7 7 14 29.31 6.78 7 7 15 4.76 4.03 -7 7 15 1.50 2.09 7 7 15 0.03 1.84 7 7 16 0.40 3.40 -7 7 16 -0.84 3.74 7 7 16 0.93 2.06 7 7 17 16.25 4.77 7 7 17 22.55 6.09 -7 7 17 7.68 3.09 7 7 18 108.34 12.84 -7 7 18 115.86 13.45 7 7 18 137.85 14.22 7 7 19 -0.70 1.64 -7 7 19 5.27 3.21 7 7 20 42.08 8.53 -7 7 20 38.21 7.91 -7 7 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2.55 7 -8 -4 7.28 3.16 7 -8 -4 0.83 2.50 7 8 -3 -1.31 1.41 7 8 -3 3.17 2.74 -7 8 -3 3.09 2.78 7 -8 -3 1.77 2.72 7 -8 -3 4.15 3.32 7 8 -2 6.20 2.93 7 8 -2 8.59 2.32 -7 8 -2 7.00 3.29 7 -8 -2 8.64 3.20 7 -8 -2 10.63 4.29 7 -8 -1 5.66 3.73 7 8 -1 3.10 2.19 7 8 -1 5.54 3.21 -7 8 -1 1.21 3.28 7 -8 -1 1.06 3.45 7 8 0 0.86 2.24 7 8 0 0.25 1.90 -7 8 0 0.45 2.89 7 -8 0 2.11 3.33 7 -8 0 -1.15 2.41 7 8 1 3.78 2.78 7 -8 1 2.48 3.56 7 8 1 2.06 2.31 -7 8 1 3.98 2.30 7 -8 1 2.08 3.19 7 -8 2 3.13 2.02 7 8 2 1.01 1.65 7 8 2 7.23 2.78 7 -8 2 3.48 2.97 7 -8 3 2.26 3.60 7 8 3 2.33 4.18 7 8 3 0.22 2.41 -7 8 3 0.98 2.32 7 -8 3 4.88 4.44 7 -8 4 6.36 3.46 -7 8 4 3.36 3.56 7 8 4 2.28 2.18 7 -8 4 6.51 3.88 7 -8 5 8.49 3.73 -7 8 5 11.56 5.02 7 8 5 10.95 4.97 7 8 5 6.52 2.84 7 -8 6 12.47 4.95 7 8 6 15.85 4.94 7 8 6 9.67 4.39 -7 8 6 10.45 3.26 7 -8 7 1.62 3.26 7 8 7 1.49 2.34 7 8 7 2.62 2.63 -7 8 7 1.50 2.84 7 -8 8 1.53 2.95 -7 8 8 3.15 2.75 7 8 8 7.04 4.55 7 8 8 10.89 3.68 7 -8 9 10.70 3.48 7 8 9 7.15 3.48 7 8 9 13.18 4.30 -7 8 9 7.82 3.69 7 -8 10 3.45 3.24 7 8 10 2.80 3.25 7 8 10 -1.74 3.28 -7 8 10 -0.43 1.91 7 -8 11 5.77 2.73 7 8 11 4.92 2.66 7 8 11 3.07 2.85 -7 8 11 10.75 4.97 7 -8 12 -0.17 2.34 7 8 12 0.72 3.07 7 8 12 4.40 4.62 -7 8 12 -3.12 3.00 7 8 13 1.84 3.48 7 8 13 3.75 4.15 -7 8 13 14.53 6.13 7 8 14 11.65 4.90 7 8 14 5.54 2.27 -7 8 14 16.12 4.88 -7 8 15 3.41 4.22 7 8 15 3.54 2.73 7 8 15 -4.43 4.00 7 8 16 -5.66 5.17 -7 8 16 -2.71 2.88 7 8 16 1.44 3.21 7 8 17 5.21 3.45 -7 8 17 12.77 4.61 7 8 17 7.02 3.41 7 8 18 -0.41 3.45 -7 8 18 -1.91 2.19 7 8 18 -2.47 2.76 7 8 19 0.23 2.91 -7 8 19 -2.01 3.24 7 8 20 0.10 2.01 -7 8 20 6.09 4.33 7 -9 -16 2.95 4.17 7 -9 -16 3.98 2.44 7 -9 -15 13.16 5.54 7 -9 -15 17.04 5.81 7 9 -14 73.38 11.39 7 -9 -14 83.09 11.65 7 -9 -14 66.30 10.55 7 9 -13 8.86 3.58 7 -9 -13 4.09 2.69 7 -9 -13 -0.81 3.92 7 9 -12 108.71 13.61 7 -9 -12 126.27 14.85 7 -9 -12 107.43 13.01 7 9 -11 7.74 2.89 7 -9 -11 3.67 2.51 7 -9 -11 13.45 5.57 7 -9 -10 4.41 2.50 7 9 -10 -0.52 3.51 7 -9 -9 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49.55 6.22 8 -4 -3 61.92 8.25 8 4 -3 58.51 5.96 8 -4 -2 367.27 19.54 8 4 -2 356.64 18.31 8 4 -2 335.79 16.67 8 -4 -2 296.97 17.53 8 4 -2 310.21 14.42 8 -4 -1 589.01 24.07 8 4 -1 657.52 25.05 8 4 -1 619.83 22.92 8 -4 -1 609.98 24.89 8 4 0 58.96 7.53 8 -4 0 71.94 8.51 8 4 0 78.36 8.02 8 -4 0 67.28 8.16 8 4 1 624.90 24.22 8 -4 1 602.49 24.84 8 4 1 609.21 23.11 8 -4 1 615.75 25.00 8 4 2 337.95 17.94 8 -4 2 358.26 19.08 8 4 2 381.10 18.43 8 -4 2 331.71 18.43 8 4 3 55.57 7.40 8 -4 3 48.50 7.17 8 4 3 47.41 6.12 8 4 4 212.73 14.17 8 -4 4 213.96 14.95 8 4 4 222.53 14.34 8 -4 4 191.74 13.87 8 4 5 416.87 19.67 8 -4 5 412.76 20.62 8 4 5 379.57 18.99 8 -4 5 395.40 19.77 8 4 6 24.97 5.52 8 4 6 21.63 5.05 8 -4 6 24.51 5.53 8 -4 6 9.49 1.72 8 4 7 110.87 10.34 8 4 7 111.26 10.53 8 -4 7 106.25 10.57 8 -4 7 105.25 10.67 8 4 8 16.57 4.25 8 4 8 14.70 5.21 8 -4 8 13.59 4.25 8 4 9 26.77 5.40 8 4 9 22.08 4.55 8 -4 9 28.37 5.34 8 4 10 38.68 6.45 8 -4 10 32.09 6.02 8 4 10 34.17 6.02 8 4 11 130.80 11.51 8 -4 11 115.13 11.25 8 4 11 123.86 11.56 8 4 12 43.65 6.87 8 -4 12 46.91 7.47 8 4 12 53.62 7.77 8 4 13 47.22 7.00 8 -4 13 56.20 8.17 8 4 13 54.02 8.14 8 4 14 65.42 7.89 8 -4 14 62.24 8.62 8 4 14 51.65 7.84 8 4 15 190.90 14.04 8 -4 15 176.23 14.76 8 4 15 175.88 14.81 8 4 16 140.53 11.94 8 -4 16 123.70 13.01 8 4 16 119.12 12.28 8 4 17 7.11 3.28 8 -4 17 6.28 2.57 8 4 18 42.94 7.99 8 -4 18 33.01 6.48 8 4 19 28.85 6.82 8 4 20 0.16 2.64 8 4 21 38.98 7.80 8 4 22 36.62 7.11 8 4 23 -0.54 2.81 8 4 24 50.32 9.52 8 4 25 47.55 9.34 8 4 26 -2.07 2.03 8 -5 -25 4.93 3.69 8 -5 -24 -0.16 2.21 8 -5 -23 0.17 2.47 8 -5 -22 -1.41 2.12 8 -5 -21 3.61 2.20 8 -5 -20 -0.56 2.72 8 -5 -19 8.41 3.61 8 -5 -19 3.46 2.81 8 -5 -18 9.51 4.69 8 -5 -18 11.97 5.13 8 5 -17 18.24 5.58 8 -5 -17 17.56 5.80 8 -5 -17 19.47 5.51 8 -5 -16 41.17 8.08 8 -5 -16 43.88 8.12 8 5 -16 38.00 7.45 8 5 -15 44.61 7.29 8 -5 -15 36.22 7.43 8 -5 -15 32.65 6.84 8 5 -14 40.08 6.98 8 -5 -14 39.75 7.77 8 -5 -14 32.29 6.31 8 5 -13 13.00 4.35 8 -5 -13 15.78 5.79 8 -5 -13 13.63 5.28 8 5 -12 28.76 5.92 8 -5 -12 24.49 5.85 8 -5 -12 18.92 5.54 8 5 -11 23.53 5.35 8 -5 -11 13.62 3.98 8 -5 -11 17.05 5.10 8 -5 -10 0.66 2.63 8 5 -10 1.70 1.68 -8 5 -10 -2.26 1.50 8 -5 -10 -0.24 1.76 8 -5 -9 13.57 4.45 8 5 -9 5.73 2.92 8 -5 -9 9.37 3.54 8 -5 -8 23.07 5.66 8 5 -8 19.59 4.97 8 -5 -8 17.93 5.08 8 5 -7 73.60 8.78 8 5 -7 82.71 8.37 8 -5 -7 66.24 8.95 8 -5 -7 63.89 9.21 8 -5 -6 29.10 5.85 8 5 -6 28.35 5.73 8 -5 -6 27.68 6.26 8 5 -6 27.76 4.83 8 5 -5 17.50 4.24 8 -5 -5 18.11 4.68 8 5 -5 17.63 4.28 8 -5 -5 14.72 3.37 8 5 -4 64.07 8.71 8 5 -4 62.41 7.51 8 -5 -4 71.79 8.99 8 -5 -4 65.76 8.80 8 5 -3 49.48 7.37 8 5 -3 66.79 7.55 8 -5 -3 61.32 8.46 8 -5 -3 49.40 8.06 8 5 -2 41.17 6.57 8 5 -2 36.53 5.95 8 -5 -2 21.43 4.01 8 -5 -2 34.33 6.21 8 5 -1 15.46 4.80 8 -5 -1 14.89 3.88 8 5 -1 16.72 3.95 8 -5 -1 15.42 4.63 8 5 0 23.49 4.70 8 -5 0 14.49 4.07 8 5 0 20.14 4.19 8 5 1 26.05 5.24 8 -5 1 17.58 5.19 8 5 1 24.68 4.93 8 -5 1 17.50 4.62 8 5 2 28.47 5.70 8 -5 2 38.40 6.54 8 5 2 34.38 6.24 8 -5 2 31.02 5.57 8 -5 3 55.94 8.04 8 5 3 46.80 7.07 8 5 3 50.73 7.37 8 -5 3 48.62 7.64 8 -5 4 72.52 9.11 8 5 4 64.66 7.83 8 5 4 54.16 7.61 8 -5 4 70.97 8.48 8 5 5 18.98 4.64 8 -5 5 28.64 5.84 8 5 5 23.63 5.29 8 -5 5 21.76 5.02 8 5 6 24.10 4.60 8 -5 6 22.54 5.21 8 5 6 28.26 5.86 8 -5 6 13.43 4.21 8 -5 7 66.95 9.36 8 5 7 63.79 8.48 8 5 7 68.07 8.43 8 -5 7 59.48 8.10 8 5 8 26.57 5.57 8 -5 8 15.93 4.82 8 5 8 22.01 5.28 8 -5 8 23.81 5.61 8 5 9 3.26 2.62 8 -5 9 6.70 1.42 8 5 9 4.56 2.03 8 -5 9 8.46 3.62 8 5 10 0.37 2.05 8 -5 10 5.78 3.39 8 5 10 -0.02 1.69 8 -5 10 1.90 3.02 8 5 11 20.50 4.61 8 -5 11 13.95 4.43 8 5 11 15.11 4.21 8 5 12 23.39 4.93 8 -5 12 13.82 4.23 8 5 12 16.48 5.16 8 5 13 17.51 4.95 8 -5 13 10.24 4.49 8 5 13 6.77 2.79 8 5 14 25.92 5.31 8 -5 14 31.60 6.40 8 5 14 39.30 7.28 8 5 15 46.10 7.07 8 -5 15 27.23 6.16 8 5 15 34.42 6.51 8 5 16 35.20 6.48 8 -5 16 35.98 6.58 8 5 16 46.02 8.00 8 5 17 23.36 5.51 8 5 17 14.35 5.42 8 -5 17 18.58 5.91 8 5 18 8.05 3.85 8 5 19 8.70 3.81 8 5 20 1.93 2.53 8 5 21 8.48 4.61 8 5 22 1.23 2.84 8 5 23 -2.53 2.36 8 5 24 1.12 3.38 8 5 25 1.58 2.48 8 -6 -23 0.32 2.09 8 -6 -22 4.03 3.83 8 -6 -21 41.03 8.12 8 -6 -20 9.71 3.33 8 -6 -20 0.65 1.83 8 -6 -19 14.36 5.29 8 -6 -19 10.96 4.27 8 -6 -18 47.69 8.92 8 -6 -18 38.63 7.94 8 -6 -17 26.13 5.83 8 -6 -17 25.35 6.33 8 6 -16 22.44 5.42 8 -6 -16 29.29 6.68 8 -6 -16 27.07 6.92 8 -6 -15 106.18 12.24 8 -6 -15 111.38 12.77 8 6 -15 86.70 10.99 8 -6 -14 45.47 8.16 8 -6 -14 40.96 7.77 8 6 -14 56.95 8.96 8 6 -13 3.03 2.41 8 -6 -13 3.87 1.99 8 -6 -13 5.35 3.08 8 6 -12 83.78 10.63 8 -6 -12 84.76 10.75 8 -6 -12 55.78 8.88 8 6 -11 140.02 13.15 8 -6 -11 141.06 13.48 8 -6 -11 134.05 13.44 8 6 -10 27.77 5.92 8 -6 -10 20.39 5.57 8 -6 -10 26.49 6.10 8 6 -9 106.07 11.22 -8 6 -9 94.78 10.08 8 -6 -9 82.14 10.38 8 -6 -9 91.36 10.84 8 6 -8 45.39 7.79 -8 6 -8 57.29 7.79 8 -6 -8 45.21 7.91 8 -6 -8 48.72 7.80 8 -6 -7 23.75 5.90 8 6 -7 25.08 5.26 -8 6 -7 38.03 6.24 8 -6 -7 27.24 6.71 8 6 -6 199.59 15.12 8 -6 -6 180.87 14.66 8 6 -6 164.64 12.62 -8 6 -6 170.56 13.58 8 -6 -6 160.12 14.78 8 6 -5 208.90 15.63 8 6 -5 213.67 14.39 8 -6 -5 223.93 16.93 8 -6 -5 240.42 17.23 8 -6 -4 29.09 6.26 8 6 -4 20.94 4.91 8 6 -4 15.73 4.25 8 -6 -4 18.46 4.72 8 6 -3 53.92 8.07 8 -6 -3 55.36 8.51 8 6 -3 67.21 8.18 8 -6 -3 51.20 8.44 8 6 -2 81.49 9.59 8 -6 -2 76.40 9.36 8 6 -2 58.80 8.19 8 -6 -2 76.88 9.50 8 6 -1 79.13 9.82 8 -6 -1 63.15 9.29 8 6 -1 102.82 10.37 8 -6 -1 78.77 9.88 8 6 0 105.27 10.78 8 -6 0 95.54 10.89 8 6 0 113.53 10.75 8 -6 0 108.18 11.52 8 6 1 95.93 10.61 8 -6 1 100.31 10.71 8 -6 1 90.13 10.73 8 6 2 77.26 9.17 8 -6 2 63.79 8.44 8 6 2 64.90 8.59 8 -6 2 79.60 9.71 8 6 3 63.55 8.37 8 -6 3 67.60 9.24 8 6 3 59.57 8.17 8 -6 3 57.40 8.31 8 -6 4 14.06 4.14 8 6 4 22.56 5.19 8 6 4 10.21 3.96 8 -6 4 9.81 4.11 8 6 5 212.62 15.75 8 -6 5 212.77 16.50 8 6 5 219.15 15.57 8 -6 5 242.06 17.13 8 6 6 202.28 14.88 8 -6 6 180.55 15.36 8 6 6 219.58 15.74 8 -6 6 196.82 15.32 8 -6 7 16.75 5.20 8 6 7 34.44 6.04 8 6 7 26.17 5.84 8 -6 7 25.70 6.40 8 -6 8 51.52 8.53 8 6 8 42.73 7.08 8 -6 8 46.02 8.30 8 -6 9 84.93 10.68 8 6 9 79.98 9.77 8 -6 9 80.25 9.68 8 6 9 91.66 10.45 8 6 10 20.54 5.30 8 -6 10 29.10 6.27 8 6 10 32.35 6.25 8 -6 10 20.37 5.16 8 -6 11 152.87 13.86 8 6 11 155.09 13.74 8 6 11 143.47 13.58 8 -6 11 133.56 13.45 8 -6 12 67.81 9.86 8 6 12 83.49 10.01 8 6 12 63.35 8.96 8 -6 12 77.97 10.78 8 6 13 -2.57 3.11 8 6 13 4.59 3.07 8 -6 13 3.18 2.72 8 -6 13 3.49 3.13 8 -6 14 48.85 9.11 8 6 14 43.39 7.52 8 6 14 53.83 8.53 8 -6 14 65.70 9.20 8 6 15 123.95 12.23 8 6 15 125.92 12.79 8 6 16 20.39 5.11 8 -6 16 13.82 5.29 8 6 16 27.83 6.55 8 6 17 16.98 5.61 8 6 17 29.74 6.78 8 6 18 49.80 8.60 8 6 19 10.99 4.28 8 6 20 3.85 4.13 8 6 21 26.16 7.04 8 6 22 8.84 3.62 8 6 23 2.55 2.43 -8 6 23 1.83 2.88 8 -7 -21 -1.35 3.03 8 -7 -21 -3.75 5.00 8 -7 -20 1.47 2.33 8 -7 -20 0.76 2.42 8 -7 -19 0.38 3.12 8 -7 -19 13.79 5.83 8 -7 -18 12.30 4.52 8 -7 -18 8.03 4.67 8 -7 -17 8.44 4.84 8 -7 -17 5.93 3.62 8 7 -16 2.38 3.13 8 -7 -16 -2.03 2.23 8 -7 -16 7.54 4.49 8 7 -15 0.71 3.65 8 -7 -15 3.83 4.07 8 -7 -15 -0.24 2.95 8 7 -14 10.26 3.50 8 -7 -14 7.17 3.73 8 -7 -14 0.45 2.96 8 7 -13 7.72 3.73 8 -7 -13 10.63 4.97 8 -7 -13 4.40 1.86 8 7 -12 36.83 7.02 8 -7 -12 37.62 7.75 8 -7 -12 44.18 8.13 8 7 -11 54.18 8.62 8 -7 -11 51.14 8.93 8 -7 -11 63.69 9.61 8 7 -10 38.64 7.27 8 -7 -10 20.94 6.25 8 -7 -10 32.52 7.27 8 7 -9 4.02 2.16 8 -7 -9 6.14 3.72 8 -7 -9 5.69 4.18 8 7 -8 38.23 6.98 -8 7 -8 39.02 6.77 8 -7 -8 51.23 8.54 8 -7 -8 57.57 9.06 8 7 -7 43.76 7.39 8 -7 -7 49.90 8.64 8 -7 -7 57.46 8.88 -8 7 -7 41.75 6.94 8 7 -6 12.17 4.40 8 -7 -6 19.00 6.11 -8 7 -6 15.31 4.72 8 -7 -6 14.97 4.47 8 7 -5 68.46 9.44 8 -7 -5 92.88 11.03 -8 7 -5 75.25 9.72 8 -7 -5 65.20 9.54 8 -7 -4 28.61 6.52 8 7 -4 34.68 6.29 8 -7 -4 23.66 6.28 8 7 -4 39.51 6.57 -8 7 -4 27.15 6.13 8 7 -3 54.01 8.85 -8 7 -3 57.94 8.25 8 -7 -3 50.75 8.88 8 7 -3 31.53 5.82 8 -7 -3 42.24 7.93 8 -7 -2 33.72 6.62 8 7 -2 38.20 6.91 -8 7 -2 35.33 6.59 8 7 -2 31.97 5.88 8 -7 -2 28.10 6.52 8 7 -1 68.02 9.03 -8 7 -1 57.44 8.38 8 -7 -1 77.25 10.71 8 -7 -1 65.32 9.17 8 7 0 87.87 10.35 -8 7 0 93.28 10.73 8 -7 0 66.97 9.40 8 7 0 104.56 10.93 8 -7 0 115.02 11.95 8 7 1 65.73 9.02 8 -7 1 55.04 8.59 8 7 1 73.29 9.31 8 -7 1 64.39 9.89 8 -7 2 37.82 7.47 8 7 2 40.98 7.70 8 -7 2 43.79 7.74 8 7 2 33.63 6.65 8 7 3 37.76 6.23 8 -7 3 63.58 9.27 8 7 3 44.59 6.94 8 -7 3 63.34 9.01 8 -7 4 25.47 5.94 8 7 4 22.61 4.90 8 -7 4 39.77 7.31 8 7 4 37.85 7.01 8 7 5 71.62 9.08 8 -7 5 69.34 9.67 8 7 5 72.65 9.28 8 -7 5 79.69 10.12 8 -7 6 18.94 4.95 8 7 6 17.81 4.88 8 -7 6 12.88 4.42 8 7 6 14.08 3.56 8 -7 7 40.41 7.24 8 7 7 33.05 6.40 8 -7 7 50.64 8.65 8 7 7 39.53 7.30 8 7 8 60.66 8.90 8 -7 8 49.80 8.26 8 7 8 53.13 8.05 8 -7 8 48.51 8.54 8 -7 9 4.81 3.42 8 7 9 0.34 2.15 8 -7 9 -2.27 3.27 8 7 9 -2.35 3.19 8 -7 10 24.15 5.54 8 7 10 25.96 5.76 8 -7 10 26.41 6.42 8 7 10 30.30 6.84 8 7 11 50.78 8.45 8 -7 11 22.17 4.60 8 -7 11 46.06 8.51 8 7 11 49.34 7.43 8 -7 12 34.83 6.75 8 7 12 35.85 7.07 8 7 12 51.67 7.98 8 -7 13 8.33 4.91 8 7 13 10.44 4.54 8 7 13 3.84 1.86 8 -7 14 -1.47 2.65 8 7 14 8.11 4.11 8 7 14 4.92 3.28 8 7 15 0.71 3.39 8 7 15 1.47 2.41 8 7 16 13.86 6.34 8 7 16 5.84 3.89 8 7 17 -0.68 2.92 -8 7 17 6.59 2.75 8 7 17 1.17 2.33 -8 7 18 7.48 4.19 8 7 18 5.30 2.86 8 7 19 3.34 3.10 -8 7 19 5.19 2.29 8 7 20 6.98 4.39 -8 7 20 8.51 4.17 8 7 21 7.88 4.19 -8 7 21 10.99 5.94 8 -8 -19 5.54 3.37 8 -8 -19 2.42 3.64 8 -8 -18 18.20 6.10 8 -8 -18 25.84 6.26 8 -8 -17 61.88 9.50 8 -8 -17 42.04 8.53 8 -8 -16 0.09 2.49 8 -8 -16 -0.36 2.05 8 8 -15 19.31 5.79 8 -8 -15 15.00 3.87 8 -8 -15 30.55 7.40 8 -8 -14 27.24 7.41 8 8 -14 26.82 6.80 8 -8 -14 22.56 6.52 8 8 -13 -0.62 1.70 8 -8 -13 3.94 2.82 8 -8 -13 2.26 3.79 8 8 -12 57.05 9.11 8 -8 -12 45.65 7.89 8 -8 -12 37.04 7.97 8 8 -11 92.77 12.07 8 -8 -11 83.59 11.51 8 -8 -11 81.65 11.36 8 -8 -10 6.29 4.33 8 -8 -10 1.84 1.76 8 8 -9 52.75 8.88 8 -8 -9 60.14 9.42 8 -8 -9 60.75 10.03 8 8 -8 40.87 7.75 8 -8 -8 58.49 9.49 -8 8 -8 74.06 11.01 8 -8 -8 70.88 10.14 8 8 -7 15.20 4.45 8 -8 -7 20.95 5.85 8 -8 -7 12.14 3.96 -8 8 -7 14.04 4.29 8 8 -6 24.93 5.58 -8 8 -6 22.59 6.15 8 -8 -6 18.20 5.29 8 -8 -6 20.38 5.17 8 8 -5 74.53 10.09 -8 8 -5 71.91 9.89 8 -8 -5 73.22 11.04 8 -8 -5 83.72 11.41 8 8 -4 7.22 3.40 8 -8 -4 15.67 5.10 8 -8 -4 11.70 4.67 8 8 -3 10.90 4.05 8 -8 -3 7.37 3.53 8 8 -3 11.87 4.52 -8 8 -3 12.75 3.73 8 -8 -3 5.04 3.34 8 8 -2 50.95 8.22 -8 8 -2 48.24 8.66 8 -8 -2 78.33 10.21 8 -8 -2 47.36 8.53 8 8 -2 50.89 7.95 8 -8 -1 37.87 7.86 8 8 -1 24.11 5.97 -8 8 -1 38.84 7.27 8 -8 -1 45.49 8.04 8 8 -1 38.96 7.04 8 -8 0 3.28 2.00 8 8 0 2.86 2.07 -8 8 0 3.73 2.37 8 -8 0 9.22 4.04 8 -8 1 22.80 6.12 8 8 1 28.87 6.68 8 -8 1 19.94 4.80 8 8 1 25.09 5.49 8 -8 2 41.74 8.02 8 8 2 51.38 8.64 -8 8 2 45.90 7.66 8 -8 2 42.50 8.28 8 8 2 48.71 7.83 8 -8 3 3.53 2.11 8 8 3 5.25 3.43 -8 8 3 11.80 4.21 8 -8 3 13.29 4.85 8 8 3 6.89 3.45 8 -8 4 11.47 4.37 8 8 4 31.34 7.05 -8 8 4 12.34 4.46 8 -8 4 15.35 4.92 8 8 4 29.38 6.71 8 8 5 71.26 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11.88 9 -4 2 162.70 13.53 9 4 3 24.98 5.27 9 4 3 23.83 5.15 9 -4 3 25.59 5.55 9 -4 3 16.54 4.56 9 4 4 61.38 7.84 9 -4 4 61.02 8.18 9 4 4 59.01 7.66 9 -4 4 79.19 9.53 9 4 5 87.24 9.64 9 -4 5 92.06 10.00 9 4 5 112.91 10.81 9 -4 5 101.81 10.77 9 4 6 240.32 15.64 9 -4 6 222.88 15.43 9 4 6 196.10 14.09 9 -4 6 232.38 16.27 9 4 7 0.68 1.23 9 4 7 0.49 2.38 9 -4 7 0.12 2.66 9 -4 7 1.07 2.41 9 4 8 118.96 11.04 9 -4 8 123.55 11.80 9 4 8 122.49 11.42 9 -4 9 177.24 14.39 9 4 9 192.70 14.33 9 4 10 5.60 3.19 9 4 10 0.91 1.98 9 -4 10 2.43 2.50 9 4 11 245.09 15.93 9 -4 11 231.40 16.38 9 4 11 247.86 16.98 9 4 12 66.20 8.41 9 -4 12 80.74 9.81 9 4 12 57.37 8.07 9 4 13 2.51 2.00 9 4 13 5.58 3.41 9 -4 13 1.58 1.79 9 4 14 26.21 6.48 9 4 14 23.24 5.80 9 -4 14 21.43 5.92 9 4 15 10.05 4.58 9 4 15 12.38 4.41 9 -4 15 14.30 3.98 9 4 16 4.69 3.25 9 -4 16 4.88 3.17 9 -4 17 228.85 17.43 9 4 17 185.71 15.93 9 -4 18 3.22 2.00 9 4 18 2.39 2.55 9 -4 19 -0.96 2.24 9 4 19 3.84 2.58 9 4 20 -2.28 3.87 9 4 21 8.01 5.28 9 4 22 0.75 3.06 9 4 23 18.15 5.60 9 4 24 1.79 2.95 9 4 25 1.85 2.60 9 4 26 8.11 4.31 9 -5 -24 1.28 3.60 9 -5 -23 7.13 2.78 9 -5 -22 16.10 4.28 9 -5 -21 58.74 9.68 9 -5 -20 12.43 4.58 9 -5 -19 11.98 3.83 9 -5 -19 14.55 5.91 9 5 -18 5.06 3.84 9 -5 -18 -1.18 2.25 9 -5 -18 3.58 3.82 9 5 -17 9.26 4.22 9 -5 -17 22.17 6.19 9 -5 -17 11.67 4.08 9 5 -16 20.38 5.88 9 -5 -16 22.37 5.40 9 -5 -16 22.20 6.04 9 -5 -15 178.89 15.83 9 -5 -15 215.55 17.58 9 5 -15 189.45 15.79 9 5 -14 25.48 5.50 9 -5 -14 25.70 6.64 9 -5 -14 15.16 4.60 9 5 -13 5.38 2.57 9 -5 -13 2.86 1.93 9 -5 -13 3.54 3.16 9 -5 -12 37.75 7.11 9 5 -12 44.11 7.64 9 -5 -12 42.09 7.18 9 -5 -11 234.11 17.07 9 -5 -11 235.82 17.49 9 5 -11 263.58 18.07 9 -5 -10 12.77 4.65 9 5 -10 12.26 4.44 9 -5 -10 6.56 4.23 9 -5 -9 5.78 3.00 9 5 -9 7.46 3.37 9 -5 -9 4.02 1.97 9 -5 -8 2.46 2.49 9 5 -8 -0.44 1.87 9 -5 -8 -0.42 2.41 9 5 -7 60.51 8.24 9 -5 -7 44.67 7.88 9 -5 -7 66.16 9.63 9 -5 -6 24.81 5.57 9 5 -6 22.28 5.07 9 -5 -6 25.59 6.20 9 5 -6 21.64 4.23 9 5 -5 394.37 20.94 9 5 -5 444.60 20.26 9 -5 -5 411.48 21.96 9 -5 -5 422.01 22.37 9 5 -4 42.14 6.79 9 5 -4 32.97 5.84 9 -5 -4 47.34 7.90 9 -5 -4 45.04 7.48 9 5 -3 16.22 4.84 9 -5 -3 12.11 4.57 9 -5 -3 11.57 3.32 9 5 -3 9.42 2.50 9 5 -2 8.26 3.23 9 5 -2 12.07 4.55 9 -5 -2 12.70 4.67 9 -5 -2 13.15 4.27 9 5 -1 434.81 22.10 9 5 -1 425.83 20.60 9 -5 -1 468.22 23.75 9 -5 -1 376.05 20.91 9 -5 0 45.28 7.85 9 5 0 35.91 6.66 9 5 0 42.99 6.62 9 -5 0 31.85 6.32 9 -5 1 407.58 21.79 9 5 1 395.53 20.61 9 5 1 388.25 19.84 9 -5 1 385.62 21.52 9 5 2 9.56 4.38 9 5 2 14.38 4.54 9 -5 2 15.82 3.99 9 -5 2 18.36 5.12 9 5 3 19.38 4.98 9 5 3 16.17 4.41 9 -5 3 5.99 4.04 9 -5 3 15.29 3.48 9 5 4 32.46 6.35 9 -5 4 35.99 6.56 9 5 4 39.87 6.90 9 -5 4 49.42 7.74 9 -5 5 439.63 22.79 9 5 5 479.03 22.81 9 -5 5 418.78 22.59 9 5 6 23.31 5.22 9 5 6 22.80 5.55 9 -5 6 15.21 5.33 9 -5 6 20.23 5.34 9 5 7 51.54 7.37 9 -5 7 58.95 8.42 9 5 7 68.84 8.82 9 -5 7 61.45 8.77 9 5 8 0.21 2.68 9 5 8 -0.40 1.64 9 -5 8 -0.85 1.54 9 -5 8 1.70 2.33 9 5 9 12.76 4.13 9 5 9 11.22 3.66 9 -5 9 10.12 4.66 9 -5 9 14.30 4.85 9 5 10 21.25 5.55 9 5 10 8.29 3.35 9 -5 10 10.62 3.06 9 -5 10 14.92 4.89 9 5 11 258.72 17.21 9 -5 11 241.89 17.57 9 5 11 271.89 18.03 9 -5 11 225.35 17.02 9 5 12 33.26 6.69 9 -5 12 34.73 6.80 9 5 12 40.67 6.86 9 5 13 5.18 2.95 9 5 13 9.32 4.30 9 -5 13 2.46 1.79 9 5 14 16.19 4.81 9 5 14 18.50 4.55 9 -5 14 13.16 4.78 9 5 15 179.58 14.62 9 -5 15 196.88 16.73 9 5 15 204.50 16.89 9 5 16 24.57 5.73 9 5 16 17.86 5.54 9 -5 16 17.06 5.10 9 5 17 7.16 3.96 9 -5 17 7.19 3.36 9 5 18 1.32 2.19 9 5 19 21.72 5.74 9 5 20 3.72 2.73 9 5 21 53.13 8.92 9 5 22 27.20 6.37 9 5 23 6.58 2.76 9 5 24 1.09 2.31 9 -6 -23 4.09 2.93 9 -6 -22 7.41 3.68 9 -6 -21 6.33 4.63 9 -6 -20 2.51 3.83 9 -6 -20 -4.94 3.10 9 -6 -19 10.00 4.48 9 -6 -19 13.07 5.88 9 -6 -18 12.98 4.01 9 -6 -18 9.57 5.30 9 6 -17 7.01 3.60 9 -6 -17 9.01 5.63 9 -6 -17 14.46 6.00 9 6 -16 23.31 6.08 9 -6 -16 20.89 6.21 9 -6 -16 21.88 5.85 9 6 -15 41.66 7.84 9 -6 -15 33.23 7.11 9 -6 -15 31.46 7.60 9 6 -14 6.54 2.86 9 -6 -14 4.80 3.83 9 -6 -14 8.54 4.25 9 6 -13 19.11 5.67 9 -6 -13 15.78 5.33 9 -6 -13 23.86 6.53 9 6 -12 -0.17 2.35 9 -6 -12 8.49 4.42 9 -6 -12 6.38 4.59 9 6 -11 -2.13 3.24 9 -6 -11 -0.83 2.61 9 -6 -11 -0.87 2.06 9 6 -10 29.11 6.12 9 -6 -10 23.70 6.26 9 -6 -10 20.71 5.90 9 -6 -9 3.64 3.28 9 6 -9 12.33 4.41 -9 6 -9 -2.99 1.93 9 -6 -9 5.91 3.16 9 6 -8 49.96 7.69 -9 6 -8 56.02 8.23 9 -6 -8 63.41 9.16 9 -6 -8 54.29 8.55 9 6 -7 52.07 7.46 9 -6 -7 43.47 7.05 9 -6 -7 52.54 8.98 9 -6 -6 0.61 2.26 9 6 -6 0.99 2.40 9 -6 -6 4.04 3.29 9 6 -5 6.75 3.46 9 -6 -5 2.20 3.06 9 6 -5 6.58 1.48 9 -6 -5 7.94 4.20 9 -6 -4 20.42 5.65 9 6 -4 17.20 4.33 9 6 -4 15.87 4.07 9 -6 -4 15.49 5.18 9 -6 -3 5.96 2.76 9 6 -3 9.24 3.38 9 6 -3 5.48 2.74 9 -6 -3 5.62 3.66 9 -6 -2 9.05 3.63 9 6 -2 6.83 3.16 9 6 -2 1.57 1.32 9 -6 -2 2.38 3.12 9 6 -1 52.28 8.04 9 6 -1 43.86 7.03 9 -6 -1 61.80 9.04 9 -6 -1 48.38 8.12 9 6 0 79.14 9.62 9 6 0 79.76 9.59 9 -6 0 67.85 9.38 9 -6 0 69.39 9.53 9 6 1 58.52 8.32 9 6 1 68.79 8.35 9 -6 1 56.00 8.61 9 -6 1 56.00 8.28 9 -6 2 6.50 3.93 9 6 2 4.30 1.52 9 6 2 1.15 1.33 9 -6 2 5.56 3.98 9 6 3 8.55 3.89 9 -6 3 12.45 4.39 9 6 3 6.59 3.86 9 -6 3 3.88 3.88 9 6 4 18.20 5.03 9 -6 4 14.97 4.95 9 6 4 12.20 2.79 9 -6 4 18.20 4.81 9 6 5 9.09 4.62 9 -6 5 2.75 2.88 9 6 5 6.23 2.96 9 -6 5 7.13 2.46 9 6 6 1.69 2.86 9 -6 6 -1.09 3.54 9 6 6 2.84 2.90 9 -6 6 0.56 2.40 9 -6 7 54.72 8.65 9 6 7 69.07 9.23 9 -6 7 63.33 9.13 9 -6 8 57.45 8.63 9 6 8 63.95 8.73 9 6 8 47.30 8.33 9 -6 8 73.23 10.19 9 6 9 9.21 3.20 9 -6 9 6.34 3.80 9 6 9 7.43 3.20 9 -6 9 3.51 2.32 9 6 10 21.13 5.25 9 -6 10 30.62 7.30 9 6 10 19.40 4.83 9 -6 10 32.79 6.83 9 6 11 2.32 2.64 9 -6 11 1.22 2.09 9 6 11 0.79 2.24 9 -6 11 5.97 4.11 9 6 12 4.84 4.27 9 -6 12 8.43 3.61 9 6 12 7.43 4.45 9 -6 12 6.21 4.30 9 6 13 13.04 4.69 9 -6 13 18.35 5.58 9 6 13 21.74 5.25 9 -6 13 19.36 5.93 9 6 14 9.98 4.55 9 -6 14 6.24 3.64 9 6 14 3.54 2.39 9 -6 14 0.01 2.76 9 6 15 53.15 8.47 9 -6 15 48.75 8.59 9 6 15 42.76 8.08 9 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6.37 2.94 9 -7 7 8.41 4.68 9 -7 8 11.17 4.99 9 7 8 18.63 5.25 9 7 8 11.50 4.28 9 -7 8 13.38 4.01 9 7 9 43.17 7.33 9 7 9 43.47 7.70 9 -7 9 32.51 7.60 9 -7 9 53.29 9.13 9 -7 10 15.81 5.71 9 7 10 17.44 4.74 9 7 10 12.15 3.36 9 -7 10 20.54 6.21 9 7 11 199.27 16.33 9 7 11 174.27 15.22 9 -7 11 168.65 15.85 9 -7 11 184.36 15.87 9 -7 12 1.29 2.32 9 7 12 9.31 4.21 9 7 12 1.70 1.61 9 -7 12 5.74 3.86 9 -7 13 16.22 5.51 9 7 13 14.40 4.38 9 7 13 10.19 4.57 9 -7 14 6.60 4.49 9 7 14 3.14 4.01 9 7 14 0.85 2.39 9 7 15 134.98 14.17 9 7 15 133.17 14.12 9 -7 15 144.66 15.70 9 7 16 -0.21 4.45 9 7 16 6.85 2.95 9 7 17 25.39 6.31 9 7 17 31.55 7.09 9 7 18 4.73 3.41 9 7 19 1.69 1.99 9 7 20 10.66 4.94 -9 7 20 7.66 4.54 9 7 21 21.07 6.43 -9 7 21 24.05 6.33 9 -8 -18 6.28 4.29 9 -8 -18 7.44 4.08 9 -8 -17 5.13 4.06 9 -8 -17 1.76 3.00 9 8 -16 -3.27 2.62 9 -8 -16 0.95 2.26 9 -8 -16 -5.27 3.88 9 8 -15 -3.14 3.80 9 -8 -15 7.70 3.91 9 -8 -15 0.40 3.33 9 -8 -14 -1.19 3.65 9 -8 -14 3.12 2.57 9 8 -13 1.54 2.88 9 -8 -13 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57.81 8.71 10 -4 -16 46.66 9.12 10 4 -16 38.40 7.39 10 -4 -15 89.26 10.96 10 -4 -15 103.81 12.48 10 4 -15 87.15 10.50 10 -4 -14 70.56 10.00 10 -4 -14 77.39 10.47 10 4 -14 99.17 11.06 10 -4 -13 61.84 9.39 10 -4 -13 60.36 9.08 10 4 -13 58.87 8.76 10 -4 -12 139.33 13.64 10 -4 -12 107.09 11.79 10 4 -12 125.36 12.55 10 -4 -11 235.11 17.05 10 -4 -11 231.31 17.34 10 4 -11 258.73 17.36 10 -4 -10 75.10 9.73 10 -4 -10 78.45 10.17 10 4 -10 93.31 10.38 10 -4 -9 99.08 11.37 10 -4 -9 76.65 10.14 10 4 -9 81.20 9.95 10 -4 -8 100.71 11.40 10 -4 -8 128.13 12.83 10 4 -8 108.85 10.92 10 4 -7 32.03 6.27 10 -4 -7 29.56 6.33 10 4 -7 31.40 5.19 10 -4 -7 39.43 7.04 10 4 -6 34.41 5.28 10 -4 -6 51.65 8.13 10 4 -6 36.00 6.42 10 -4 -6 39.01 7.00 10 -4 -5 168.66 14.07 10 -4 -5 164.07 14.28 10 4 -5 171.54 12.53 10 4 -5 185.99 14.15 10 -4 -4 69.71 8.87 10 4 -4 70.90 8.20 10 -4 -4 50.12 8.05 10 4 -4 64.38 8.37 10 4 -3 68.76 8.57 10 -4 -3 63.49 8.91 10 4 -3 72.54 8.35 10 -4 -3 59.22 8.17 10 4 -3 69.87 7.58 10 4 -2 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8.91 10 4 11 247.72 16.68 10 -4 11 226.93 16.90 10 4 11 252.70 17.55 10 4 12 103.33 10.80 10 -4 12 121.49 12.38 10 4 12 95.40 11.39 10 4 13 73.59 9.29 10 -4 13 86.63 10.92 10 4 13 78.38 9.80 10 4 14 92.06 10.50 10 -4 14 95.32 11.19 10 4 14 94.07 11.08 10 4 15 91.69 10.79 10 -4 15 83.94 10.94 10 4 15 95.85 11.44 10 -4 16 32.03 7.17 10 4 16 38.46 7.43 10 4 17 67.53 10.07 10 -4 17 60.43 9.60 10 4 18 73.58 10.76 10 -4 18 82.40 11.36 10 -4 19 25.87 6.47 10 4 19 21.25 5.35 10 4 20 11.75 4.51 10 4 21 25.08 6.64 10 4 22 6.84 2.26 10 4 23 10.73 4.37 10 4 24 33.86 8.12 10 4 25 25.05 6.53 10 -5 -23 -0.51 2.87 10 -5 -22 0.16 3.73 10 -5 -21 14.27 4.50 10 -5 -20 0.51 1.82 10 -5 -19 6.63 4.54 10 -5 -18 1.46 1.77 10 -5 -18 -1.46 2.90 10 5 -18 0.87 2.94 10 5 -17 0.85 1.83 10 -5 -17 3.20 2.85 10 -5 -17 7.22 4.59 10 5 -16 20.38 6.03 10 -5 -16 11.13 3.99 10 -5 -16 12.71 4.15 10 5 -15 23.62 6.32 10 -5 -15 21.35 6.16 10 -5 -15 18.61 6.81 10 5 -14 0.73 2.68 10 -5 -14 0.19 2.36 10 -5 -14 5.20 3.01 10 5 -13 0.47 2.73 10 -5 -13 -1.68 2.60 10 -5 -13 0.42 2.21 10 -5 -12 0.19 1.71 10 5 -12 2.60 2.30 10 -5 -12 2.00 1.88 10 -5 -11 7.30 2.72 10 5 -11 3.78 2.73 10 -5 -11 6.83 2.45 10 -5 -10 15.07 5.22 10 5 -10 10.72 3.09 10 -5 -10 24.90 5.45 10 -5 -9 0.70 3.79 10 5 -9 9.60 4.17 10 -5 -9 9.68 2.33 10 5 -8 19.55 5.81 10 -5 -8 25.43 5.87 10 -5 -8 31.63 7.02 10 5 -7 28.35 6.05 10 -5 -7 15.17 4.98 10 -5 -7 19.80 5.67 10 5 -6 9.63 4.63 10 -5 -6 3.06 2.81 10 5 -6 13.81 4.31 10 -5 -6 5.04 2.69 10 5 -5 11.52 4.42 10 -5 -5 4.22 2.31 10 5 -5 13.30 3.89 10 -5 -5 5.81 3.09 10 5 -4 44.42 7.09 10 -5 -4 34.27 7.84 10 5 -4 30.82 5.74 10 -5 -4 38.80 7.21 10 5 -3 11.69 4.17 10 -5 -3 17.45 5.27 10 -5 -3 5.98 3.17 10 5 -3 22.05 4.91 10 5 -2 60.51 8.34 10 5 -2 58.57 7.48 10 -5 -2 47.61 7.87 10 -5 -2 35.20 6.89 10 5 -1 104.69 11.12 10 5 -1 126.09 11.55 10 -5 -1 120.37 12.16 10 -5 0 103.79 11.13 10 5 0 100.98 10.59 10 5 0 106.77 10.95 10 -5 0 101.99 11.56 10 -5 1 110.62 11.29 10 5 1 123.19 12.01 10 5 1 131.00 11.81 10 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19.26 5.62 10 -6 -7 32.95 7.43 10 6 -6 40.73 6.93 10 -6 -6 28.94 6.29 10 -6 -6 40.36 8.30 10 6 -5 87.40 10.67 10 6 -5 106.25 10.85 10 -6 -5 94.99 11.42 10 -6 -5 109.14 12.30 10 6 -4 60.57 8.95 10 6 -4 56.81 8.09 10 -6 -4 60.83 8.79 10 -6 -4 60.87 9.17 10 -6 -3 1.50 1.93 10 6 -3 4.55 3.78 10 -6 -3 3.53 2.26 10 6 -3 0.33 1.92 10 6 -2 34.28 6.04 10 6 -2 48.33 8.10 10 -6 -2 39.54 8.24 10 -6 -2 41.09 7.73 10 6 -1 95.18 11.09 10 6 -1 113.71 11.54 10 -6 -1 94.86 11.57 10 -6 -1 84.41 10.69 10 6 0 123.58 12.35 10 6 0 116.16 12.12 10 -6 0 117.76 12.59 10 -6 0 107.06 11.93 10 6 1 101.27 11.43 10 6 1 95.87 10.70 10 -6 1 94.49 11.55 10 -6 1 115.12 11.96 10 6 2 58.11 8.33 10 6 2 39.12 7.09 10 -6 2 44.67 8.14 10 -6 2 51.50 8.10 10 6 3 1.24 2.87 10 6 3 3.30 2.21 10 -6 3 2.05 1.95 10 -6 3 -0.28 1.83 10 -6 4 61.99 9.73 10 6 4 54.16 8.42 10 6 4 56.97 8.60 10 -6 4 49.83 8.49 10 -6 5 96.46 10.94 10 6 5 85.29 10.38 10 6 5 85.83 10.75 10 -6 5 107.44 12.26 10 6 6 23.54 5.33 10 -6 6 28.67 6.81 10 6 6 40.05 7.45 10 -6 6 36.72 7.16 10 6 7 12.98 4.26 10 6 7 22.92 5.73 10 -6 7 13.50 4.18 10 -6 7 22.88 5.90 10 -6 8 75.78 10.21 10 6 8 74.16 10.37 10 6 8 94.30 10.92 10 -6 8 72.74 10.22 10 -6 9 58.13 9.41 10 6 9 74.12 9.63 10 6 9 89.36 10.76 10 -6 9 66.67 10.40 10 6 10 47.60 8.04 10 6 10 42.24 7.73 10 -6 10 29.00 7.21 10 -6 11 41.49 8.47 10 6 11 43.97 7.40 10 6 11 54.01 8.78 10 -6 11 59.08 10.30 10 -6 12 50.74 9.10 10 6 12 41.61 7.10 10 6 12 47.95 8.35 10 -6 12 37.39 7.42 10 -6 13 59.96 9.66 10 6 13 48.42 8.05 10 6 13 42.29 8.02 10 -6 13 35.80 7.90 10 6 14 88.15 11.68 10 -6 14 54.64 8.91 10 6 14 70.36 9.70 10 -6 14 70.02 10.65 10 -6 15 90.62 11.82 10 6 15 125.40 13.68 10 6 15 117.58 13.06 10 6 16 40.75 7.98 10 6 16 54.70 8.43 10 -6 16 35.27 7.34 10 -6 16 48.63 9.29 10 6 17 61.24 9.60 10 6 18 35.19 7.77 10 6 19 18.63 5.86 10 6 20 41.36 7.89 10 6 21 62.22 9.24 10 6 22 27.71 7.35 10 -7 -19 2.71 3.03 10 -7 -19 3.07 3.96 10 -7 -18 6.93 2.21 10 -7 -18 4.44 4.47 10 -7 -17 0.84 2.33 10 -7 -17 -2.70 2.91 10 7 -16 4.38 2.31 10 -7 -16 13.42 4.10 10 -7 -16 9.13 2.95 10 7 -15 8.16 4.18 10 -7 -15 8.30 3.63 10 -7 -15 1.57 2.84 10 7 -14 9.69 4.17 10 -7 -14 15.02 5.36 10 -7 -14 11.76 4.57 10 7 -13 14.36 5.19 10 -7 -13 12.86 4.46 10 -7 -13 4.70 2.88 10 7 -12 3.84 1.98 10 -7 -12 8.13 3.84 10 -7 -12 5.41 3.96 10 7 -11 28.96 6.62 10 -7 -11 30.60 6.15 10 -7 -11 32.55 7.67 10 7 -10 41.97 8.34 10 -7 -10 25.11 6.47 10 -7 -10 37.03 7.57 10 7 -9 19.88 5.71 10 -7 -9 20.67 6.10 10 -7 -9 17.64 5.49 10 -7 -8 27.23 6.42 10 7 -8 23.80 5.17 10 -7 -8 10.70 4.27 10 -7 -7 4.42 4.04 10 7 -7 3.46 1.95 -10 7 -7 -1.27 1.99 10 -7 -7 -2.53 2.74 10 -7 -6 12.45 5.00 10 7 -6 3.80 1.91 -10 7 -6 8.66 4.33 10 -7 -6 14.22 4.71 10 -7 -5 5.32 3.60 10 7 -5 4.72 3.93 -10 7 -5 6.85 2.85 10 -7 -5 1.39 2.38 10 7 -4 -2.33 1.86 10 -7 -4 7.95 3.91 10 7 -4 6.85 4.20 10 -7 -4 4.49 2.77 10 -7 -3 9.88 3.97 10 7 -3 11.11 4.24 10 7 -3 7.88 4.42 10 -7 -3 8.93 4.15 10 -7 -2 25.25 6.15 10 7 -2 12.67 3.77 10 7 -2 13.27 3.84 10 -7 -2 14.45 6.08 10 7 -1 49.80 7.89 10 7 -1 49.39 8.10 10 -7 -1 55.40 8.77 10 -7 -1 54.00 9.07 10 -7 0 17.89 4.96 10 7 0 27.37 6.12 10 7 0 14.72 4.53 10 -7 0 25.81 6.35 10 7 1 53.97 8.52 10 -7 1 40.00 7.38 10 7 1 45.37 7.82 10 -7 1 40.32 8.18 10 -7 2 15.40 5.23 10 7 2 21.07 5.65 10 7 2 10.60 3.40 10 -7 2 14.97 4.76 10 -7 3 13.12 3.92 10 7 3 11.85 4.58 10 7 3 11.52 4.38 10 -7 3 11.31 4.47 10 -7 4 13.88 4.80 10 7 4 3.57 3.37 10 7 4 4.56 2.76 10 -7 4 8.08 4.21 10 -7 5 5.16 3.00 10 7 5 1.25 2.08 10 7 5 3.53 2.33 10 -7 5 6.86 4.93 10 -7 6 -2.25 2.30 10 7 6 9.95 4.31 10 7 6 9.99 3.03 10 -7 6 6.17 3.49 10 -7 7 6.20 3.14 10 7 7 3.60 4.33 10 7 7 5.28 3.15 10 -7 7 0.21 2.74 10 -7 8 20.67 5.19 10 7 8 21.50 6.03 10 7 8 23.92 5.93 10 -7 8 23.31 7.07 10 -7 9 23.51 5.93 10 7 9 31.35 6.80 10 7 9 21.27 6.02 10 -7 9 19.23 5.00 10 -7 10 27.27 7.38 10 7 10 26.12 5.85 10 7 10 17.14 5.49 10 -7 10 28.86 7.26 10 -7 11 16.17 5.48 10 7 11 23.88 6.21 10 -7 11 23.24 6.38 10 -7 12 3.61 2.31 10 7 12 0.85 2.59 10 7 12 0.58 2.27 10 7 13 3.72 3.31 10 -7 13 4.77 2.80 10 7 13 5.88 4.03 10 -7 13 8.06 3.78 10 7 14 15.64 5.30 10 -7 14 2.26 2.46 10 7 14 14.98 5.02 10 7 15 8.04 4.19 10 -7 15 11.71 6.10 10 7 15 8.37 3.76 10 7 16 6.36 3.71 10 7 16 10.99 4.43 10 7 17 -0.50 2.94 10 7 18 10.01 3.85 10 7 19 0.49 2.06 10 -8 -17 0.78 2.12 10 -8 -17 8.81 4.22 10 8 -16 1.36 5.27 10 -8 -16 8.28 6.42 10 -8 -16 2.53 3.25 10 8 -15 34.39 7.30 10 -8 -15 46.95 8.80 10 -8 -15 36.34 7.78 10 8 -14 39.58 8.28 10 -8 -14 39.92 8.27 10 -8 -14 44.58 8.59 10 8 -13 18.13 5.75 10 -8 -13 15.76 5.52 10 -8 -13 24.43 6.53 10 8 -12 14.25 5.76 10 -8 -12 27.78 6.67 10 -8 -12 10.79 4.96 10 8 -11 10.50 3.78 10 -8 -11 23.77 6.50 10 -8 -11 29.16 7.28 10 8 -10 3.23 2.41 10 -8 -10 8.70 3.79 10 -8 -10 11.01 4.78 10 8 -9 42.58 8.28 10 -8 -9 46.60 8.45 10 -8 -9 36.90 7.95 10 8 -8 41.03 8.26 10 -8 -8 63.17 10.56 10 -8 -8 56.13 9.93 10 8 -7 3.41 2.60 -10 8 -7 7.28 5.01 10 -8 -7 1.00 2.53 10 8 -6 55.23 9.28 -10 8 -6 54.68 8.98 10 -8 -6 68.67 10.38 10 -8 -6 60.28 10.27 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11 -3 -15 21.83 5.15 11 3 -15 27.58 6.44 11 -3 -14 116.06 12.45 11 -3 -14 79.21 11.25 11 3 -14 104.78 11.63 11 -3 -13 81.82 10.25 11 -3 -13 80.40 10.53 11 3 -13 102.58 11.21 11 -3 -12 111.24 11.89 11 3 -12 81.37 9.65 11 -3 -12 91.59 10.88 11 -3 -11 166.56 14.81 11 3 -11 136.34 13.17 11 -3 -11 148.88 13.53 11 -3 -10 27.21 5.79 11 -3 -10 46.77 8.68 11 3 -10 45.20 7.48 11 -3 -9 681.18 29.46 11 3 -9 738.34 29.23 11 -3 -9 634.13 27.85 11 -3 -8 258.10 17.42 11 3 -8 213.07 14.20 11 -3 -8 227.73 16.86 11 3 -8 243.06 16.71 11 -3 -7 56.05 8.30 11 -3 -7 69.04 9.18 11 3 -7 79.35 8.76 11 3 -7 50.39 7.19 11 3 -7 79.58 9.42 11 -3 -6 56.30 8.31 11 -3 -6 51.05 7.95 11 3 -6 60.77 7.68 11 3 -6 52.83 7.34 11 3 -6 71.10 9.06 11 -3 -5 427.06 22.51 11 -3 -5 473.41 24.21 11 3 -5 498.56 21.92 11 3 -5 459.28 20.73 11 3 -5 489.61 22.90 11 -3 -4 264.60 17.53 11 -3 -4 235.56 17.28 11 3 -4 269.07 15.82 11 3 -4 239.91 15.11 11 3 -4 261.98 16.76 11 -3 -3 1706.03 44.65 11 -3 -3 1755.41 46.17 11 3 -3 1756.50 41.48 11 3 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11 145.68 13.80 11 3 11 172.61 14.22 11 3 12 89.98 10.37 11 -3 12 100.30 11.16 11 3 12 107.94 10.93 11 3 13 97.62 10.35 11 -3 13 86.53 10.78 11 3 13 106.57 11.03 11 3 14 74.58 10.37 11 -3 14 104.75 11.74 11 3 14 83.99 9.40 11 3 15 28.36 5.64 11 -3 15 26.93 6.55 11 3 16 0.43 2.12 11 -3 16 1.79 2.50 11 3 17 54.80 8.73 11 -3 17 64.55 9.84 11 3 18 104.20 12.36 11 -3 18 101.33 12.09 11 3 19 15.74 4.61 11 -3 19 34.36 7.17 11 3 20 28.23 6.76 11 -3 20 25.95 6.99 11 3 21 8.00 2.46 11 -3 21 14.95 5.46 11 3 22 20.35 5.14 11 3 23 52.58 9.32 11 3 24 59.84 10.17 11 3 25 53.55 9.75 11 -4 -24 11.26 5.20 11 -4 -23 1.51 2.31 11 -4 -22 35.82 7.77 11 -4 -21 15.43 5.38 11 -4 -20 4.77 2.79 11 -4 -19 4.18 3.72 11 4 -19 6.09 3.09 11 -4 -18 -0.25 1.97 11 4 -18 0.01 2.07 11 -4 -17 3.46 3.65 11 -4 -17 2.99 2.51 11 4 -17 1.47 2.29 11 -4 -16 3.43 4.29 11 -4 -16 1.56 3.44 11 4 -16 5.49 3.54 11 -4 -15 6.58 2.51 11 4 -15 4.62 2.83 11 -4 -15 5.65 3.39 11 4 -14 -2.40 3.11 11 -4 -14 1.58 3.48 11 -4 -14 2.57 3.55 11 4 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11 4 0 3.00 2.57 11 -4 0 0.96 3.06 11 4 1 228.46 15.99 11 -4 1 240.11 16.92 11 4 1 242.38 16.22 11 -4 1 246.26 17.71 11 4 2 165.94 13.69 11 -4 2 181.89 14.73 11 4 2 156.01 12.88 11 -4 2 139.69 13.46 11 4 3 83.13 9.94 11 -4 3 67.28 9.54 11 4 3 75.06 8.83 11 -4 3 71.80 9.60 11 4 4 714.12 28.32 11 -4 4 739.39 29.95 11 4 4 694.48 28.24 11 -4 4 694.21 29.85 11 4 5 -0.23 2.49 11 -4 5 5.19 3.18 11 4 5 2.04 3.63 11 -4 5 -0.64 1.78 11 4 6 10.17 3.77 11 -4 6 7.63 1.86 11 4 6 4.87 4.00 11 -4 6 4.00 2.59 11 4 7 9.83 2.49 11 -4 7 18.36 4.81 11 4 7 14.27 4.55 11 -4 7 16.08 4.87 11 4 8 90.76 10.09 11 4 8 113.08 11.69 11 -4 8 100.15 11.19 11 -4 8 93.21 11.13 11 4 9 0.70 2.31 11 -4 9 2.03 2.88 11 4 9 1.58 1.91 11 -4 9 6.26 4.39 11 4 10 54.07 8.15 11 4 10 50.79 7.97 11 -4 10 28.71 6.39 11 4 11 9.98 2.21 11 -4 11 12.18 4.21 11 4 11 18.72 5.15 11 4 12 32.95 6.14 11 -4 12 45.35 7.90 11 4 12 41.72 6.81 11 4 13 -0.67 2.08 11 -4 13 -0.11 2.75 11 4 13 0.70 2.81 11 4 14 0.27 2.43 11 -4 14 1.17 1.74 11 4 14 0.52 2.90 11 -4 15 4.42 2.05 11 4 15 6.91 4.03 11 -4 16 0.07 2.65 11 4 16 0.65 2.10 11 -4 17 -1.63 3.35 11 4 17 -0.60 2.69 11 -4 18 1.60 4.22 11 4 18 0.63 1.80 11 -4 19 6.81 4.38 11 4 19 4.17 2.91 11 4 20 9.84 3.89 11 4 21 12.11 4.78 11 4 22 18.00 5.54 11 4 23 24.01 6.17 11 4 24 12.49 5.14 11 -5 -22 38.87 7.94 11 -5 -21 3.20 3.25 11 -5 -20 37.12 7.49 11 -5 -19 34.91 7.92 11 5 -19 -6.79 3.35 11 -5 -18 31.91 7.24 11 -5 -18 26.61 6.62 11 5 -18 43.64 8.10 11 -5 -17 27.23 7.19 11 -5 -17 11.28 4.51 11 5 -17 21.08 6.50 11 5 -16 6.20 2.73 11 -5 -16 -1.13 3.65 11 -5 -16 7.09 5.16 11 5 -15 21.85 5.93 11 -5 -15 19.99 5.30 11 -5 -15 10.82 4.37 11 -5 -14 78.99 10.89 11 -5 -14 71.12 10.68 11 5 -14 76.16 10.24 11 -5 -13 39.79 7.89 11 -5 -13 55.23 9.49 11 5 -13 55.71 9.24 11 -5 -12 11.26 4.57 11 5 -12 21.87 5.50 11 -5 -12 21.65 6.47 11 5 -11 2.64 2.97 11 -5 -11 -0.42 3.09 11 -5 -11 3.52 3.80 11 5 -10 -0.80 2.86 11 -5 -10 1.11 3.19 11 -5 -10 1.14 2.11 11 -5 -9 48.74 8.68 11 -5 -9 63.22 9.40 11 5 -9 72.51 9.64 11 -5 -8 297.42 20.39 11 -5 -8 277.24 19.38 11 5 -8 287.08 19.00 11 -5 -7 29.81 6.76 11 -5 -7 46.24 8.05 11 5 -7 45.01 7.38 11 5 -6 36.76 6.70 11 -5 -6 36.73 6.75 11 -5 -6 41.07 7.88 11 5 -5 10.66 3.80 11 -5 -5 3.79 3.53 11 5 -5 9.79 4.00 11 -5 -5 10.69 5.04 11 5 -4 280.99 17.93 11 5 -4 296.61 18.22 11 -5 -4 324.12 20.91 11 -5 -4 279.10 19.13 11 5 -3 54.87 8.50 11 5 -3 53.10 7.58 11 -5 -3 42.48 7.70 11 -5 -3 50.64 7.77 11 -5 -2 115.44 12.55 11 5 -2 105.89 11.61 11 5 -2 91.72 10.23 11 -5 -2 114.14 12.70 11 5 -1 181.45 14.62 11 -5 -1 187.79 15.55 11 5 -1 182.89 14.41 11 -5 -1 160.99 15.06 11 5 0 1.10 1.89 11 -5 0 3.64 3.09 11 -5 0 0.52 3.52 11 5 0 2.93 1.72 11 5 1 193.24 15.16 11 5 1 176.36 14.42 11 -5 1 164.95 14.99 11 5 2 84.42 9.78 11 -5 2 86.11 10.93 11 5 2 108.22 11.15 11 -5 2 99.86 11.83 11 5 3 52.70 7.94 11 -5 3 58.58 9.02 11 5 3 59.78 8.39 11 -5 3 47.41 8.08 11 5 4 260.17 18.02 11 -5 4 309.53 20.37 11 5 4 328.81 19.95 11 -5 4 278.42 19.63 11 5 5 4.77 2.93 11 -5 5 3.44 4.45 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4.44 4.43 12 6 -18 15.16 6.27 12 6 -17 25.39 6.51 12 -6 -17 37.94 7.79 12 -6 -17 35.02 8.04 12 6 -16 26.01 6.70 12 -6 -16 37.14 8.37 12 -6 -16 21.18 6.46 12 6 -15 8.09 4.97 12 -6 -15 11.18 4.06 12 -6 -15 10.04 4.63 12 -6 -14 53.51 9.54 12 6 -14 54.01 8.85 12 -6 -14 44.03 8.82 12 -6 -13 75.05 10.95 12 -6 -13 85.88 11.99 12 6 -13 82.62 11.47 12 -6 -12 5.26 1.92 12 6 -12 10.85 4.12 12 -6 -12 8.98 5.23 12 -6 -11 31.83 7.61 12 6 -11 28.59 7.11 12 -6 -11 36.49 7.06 12 -6 -10 48.09 8.22 12 -6 -10 56.06 9.46 12 6 -10 50.68 8.83 12 -6 -9 30.78 6.30 12 6 -9 37.75 7.68 12 -6 -9 22.34 6.88 12 -6 -8 128.46 13.97 12 -6 -8 136.45 14.11 12 6 -8 131.21 13.37 12 -6 -7 176.08 15.99 12 -6 -7 146.91 14.77 12 6 -7 155.39 14.41 12 6 -6 13.75 5.77 12 -6 -6 25.24 6.62 12 -6 -6 25.73 6.37 12 -6 -5 33.80 7.12 12 -6 -5 41.93 8.55 12 6 -5 52.81 8.95 12 6 -4 95.78 11.13 12 6 -4 114.57 13.05 12 -6 -4 100.46 12.47 12 -6 -4 101.84 12.09 12 6 -3 159.53 14.48 12 6 -3 129.13 12.75 12 -6 -3 139.06 14.49 12 -6 -3 167.46 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6.12 3.74 13 -6 6 0.66 3.21 13 6 7 5.19 2.06 13 -6 7 1.15 2.51 13 6 7 4.40 2.74 13 -6 7 5.28 4.68 13 6 8 2.45 2.04 13 -6 8 6.54 3.69 13 6 8 4.28 2.17 13 -6 8 8.93 3.76 13 6 9 4.08 3.61 13 -6 9 9.50 4.58 13 6 9 0.55 1.50 13 -6 9 8.25 5.82 13 6 10 11.13 4.52 13 -6 10 4.57 2.15 13 6 10 1.61 1.80 13 -6 10 8.93 4.99 13 6 11 6.86 4.02 13 -6 11 7.25 3.71 13 6 11 17.08 5.16 13 -6 11 6.15 2.31 13 6 12 2.41 3.57 13 -6 12 -0.03 2.14 13 6 12 1.06 2.09 13 -6 12 1.00 3.00 13 6 13 8.80 5.58 13 -6 13 14.61 5.86 13 6 13 7.92 3.52 13 -6 13 5.40 3.48 13 6 14 7.18 3.50 13 -6 14 3.00 3.81 13 6 14 7.16 2.72 13 -6 14 12.21 2.65 13 -6 15 4.67 3.68 13 6 15 1.43 1.61 13 -6 15 -2.79 4.04 13 -6 16 3.01 4.00 13 6 16 0.37 3.27 13 -6 16 -5.72 5.82 13 -6 17 -2.08 2.81 13 6 17 5.48 4.14 13 -6 17 -0.45 5.25 13 6 18 3.44 1.98 13 -6 18 1.12 4.02 13 7 -15 10.50 4.97 13 -7 -15 9.94 4.51 13 -7 -15 7.31 3.91 13 7 -14 12.85 5.25 13 -7 -14 8.71 3.92 13 -7 -14 13.34 5.77 13 7 -13 2.84 2.01 13 -7 -13 4.97 2.24 13 -7 -13 4.53 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13 -8 7 9.48 5.48 13 -8 7 1.13 2.96 13 8 7 8.85 5.28 13 8 8 3.07 1.82 13 -8 8 2.37 3.44 13 -8 8 5.60 3.21 13 8 8 1.64 2.55 13 8 9 2.85 2.46 13 -8 9 -0.89 2.52 13 8 9 3.85 2.71 13 8 10 -3.30 4.43 13 -8 10 -3.40 3.14 13 8 10 -0.83 2.67 13 8 11 1.75 2.51 13 -8 11 6.30 3.02 13 8 11 7.51 3.57 13 -9 -3 5.98 3.08 13 9 -3 6.69 4.70 -13 9 -3 5.86 5.37 13 -9 -3 2.27 2.82 13 -9 -2 12.78 5.99 13 9 -2 9.72 5.02 -13 9 -2 3.75 4.32 13 -9 -2 -1.20 3.13 13 -9 -1 -1.96 3.22 13 9 -1 7.18 4.93 -13 9 -1 -0.17 2.16 13 -9 -1 6.49 4.99 13 -9 0 12.02 4.70 13 9 0 14.63 5.00 -13 9 0 4.35 3.64 13 -9 0 10.77 5.91 13 -9 1 -1.52 3.27 13 9 1 4.47 3.37 -13 9 1 5.75 5.66 13 -9 1 4.80 4.68 13 -9 2 3.51 4.25 13 9 2 6.96 2.89 -13 9 2 5.33 3.34 13 -9 2 2.63 4.84 13 9 2 -0.45 4.50 13 -9 3 13.14 6.40 13 9 3 11.01 6.31 -13 9 3 5.20 4.13 13 -9 3 3.94 3.13 13 9 3 0.80 2.48 14 0 -21 4.12 2.85 14 0 -20 25.20 6.86 14 0 -19 10.97 5.49 14 0 -18 1.53 2.95 14 0 -17 3.76 2.45 14 0 -16 40.41 8.06 14 0 -15 14.43 5.01 14 0 -14 38.16 7.13 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36.30 7.40 19 1 6 40.55 9.18 19 -1 6 41.02 8.85 19 1 6 38.42 8.22 19 -1 7 19.55 6.00 19 -1 7 22.46 7.02 19 1 7 35.76 8.18 19 1 7 22.15 6.55 19 -1 8 12.41 4.05 19 -1 8 10.96 5.22 19 1 8 10.02 5.45 19 1 8 4.83 3.72 19 -1 9 16.26 6.00 19 -1 9 15.36 4.94 19 1 9 6.43 2.57 19 1 9 16.46 6.02 19 -1 10 99.28 13.40 19 1 10 67.74 10.72 19 -1 10 72.12 12.08 19 -1 11 66.24 10.48 19 -1 11 43.93 10.23 19 1 11 35.51 8.21 19 -1 12 3.39 2.71 19 -1 12 8.05 6.05 19 1 12 4.39 3.62 19 -2 -11 6.31 3.50 19 -2 -10 4.53 4.08 19 -2 -9 0.42 3.95 19 -2 -9 2.17 2.91 19 -2 -8 3.83 4.38 19 -2 -8 -2.01 3.86 19 -2 -7 9.54 3.31 19 -2 -7 4.05 4.77 19 -2 -6 12.36 5.34 19 -2 -6 30.33 8.10 19 2 -6 25.10 6.66 19 -2 -5 14.69 6.21 19 -2 -5 14.04 4.59 19 2 -5 26.71 6.88 19 -2 -4 6.49 4.90 19 2 -4 20.33 6.58 19 -2 -4 9.80 4.71 19 2 -4 14.92 4.97 19 -2 -3 4.50 2.87 19 2 -3 8.07 5.10 19 -2 -3 8.53 5.15 19 2 -3 10.45 7.22 19 2 -3 6.77 2.67 19 -2 -2 -3.43 2.57 19 2 -2 -3.52 2.74 19 2 -2 3.44 3.90 19 2 -2 0.44 2.44 19 -2 -1 3.20 3.51 19 2 -1 4.80 2.61 19 -2 -1 6.20 2.99 19 2 -1 1.05 4.61 19 2 -1 8.91 4.30 19 -2 0 7.14 4.65 19 -2 0 11.11 5.83 19 2 0 11.25 4.88 19 2 0 8.83 5.47 19 2 0 4.49 2.87 19 -2 1 7.01 3.43 19 -2 1 5.18 4.10 19 2 1 9.55 4.60 19 2 1 3.65 2.87 19 2 1 16.06 6.44 19 -2 2 12.09 5.26 19 -2 2 2.92 3.68 19 2 2 6.12 3.50 19 2 2 4.25 3.18 19 2 2 5.55 5.02 19 -2 3 11.75 4.71 19 -2 3 13.10 5.41 19 2 3 3.69 4.00 19 2 3 3.62 4.81 19 2 3 20.81 7.13 19 -2 4 12.40 4.93 19 -2 4 10.33 5.00 19 2 4 5.53 2.58 19 2 4 4.43 2.64 19 2 4 13.40 4.88 19 -2 5 24.72 6.94 19 -2 5 41.00 9.27 19 2 5 21.16 7.01 19 2 5 28.55 7.45 19 2 5 41.65 8.99 19 -2 6 20.28 4.95 19 -2 6 16.72 5.44 19 2 6 26.43 8.26 19 2 6 20.95 5.88 19 2 6 17.19 4.91 19 -2 7 4.77 2.32 19 -2 7 2.33 2.43 19 2 7 8.83 3.71 19 2 7 15.67 4.97 19 2 7 16.84 5.23 19 -2 8 0.19 3.16 19 -2 8 0.16 3.71 19 2 8 3.88 3.26 19 2 8 0.17 3.40 19 2 8 0.54 2.17 19 -2 9 4.52 3.74 19 -2 9 1.27 2.53 19 2 9 2.92 2.97 19 -2 10 -1.81 4.13 19 -2 10 10.41 4.96 19 2 10 6.91 4.02 19 -2 11 13.31 5.15 19 -2 11 5.59 4.38 19 2 11 5.17 3.00 19 -3 -9 9.59 5.72 19 -3 -9 16.28 6.77 19 3 -9 11.39 4.06 19 -3 -8 32.05 8.00 19 -3 -8 22.49 7.14 19 3 -8 32.46 7.80 19 -3 -7 3.89 2.49 19 -3 -7 4.06 2.39 19 3 -7 4.65 4.52 19 -3 -6 10.31 4.44 19 -3 -6 15.21 5.82 19 3 -6 3.90 4.54 19 -3 -5 11.88 5.36 19 -3 -5 16.68 5.43 19 3 -5 6.40 4.31 19 -3 -4 8.59 3.47 19 -3 -4 2.66 2.70 19 3 -4 6.75 2.97 19 -3 -3 -1.23 4.51 19 -3 -3 1.11 2.84 19 3 -3 1.87 2.44 19 -3 -2 14.43 5.24 19 -3 -2 14.95 6.27 19 3 -2 12.99 5.01 19 3 -2 27.11 6.86 19 -3 -1 5.36 3.69 19 -3 -1 -3.35 4.16 19 3 -1 3.40 4.02 19 3 -1 10.15 3.83 19 -3 0 2.09 2.95 19 -3 0 0.69 2.66 19 3 0 3.56 4.01 19 3 0 1.31 2.17 19 -3 1 5.18 4.56 19 -3 1 10.15 5.30 19 3 1 9.35 3.98 19 3 1 6.63 3.63 19 -3 2 15.16 4.73 19 -3 2 14.42 6.79 19 3 2 15.95 4.68 19 3 2 21.92 6.38 19 -3 3 7.72 3.79 19 -3 3 13.61 5.37 19 3 3 3.35 6.93 19 3 3 6.98 3.35 19 3 3 5.34 4.30 19 -3 4 2.65 2.71 19 -3 4 3.51 1.91 19 3 4 0.26 2.86 19 3 4 -0.27 3.54 19 3 4 7.81 3.79 19 -3 5 20.45 6.14 19 -3 5 18.94 7.23 19 3 5 16.07 4.82 19 3 5 20.09 4.91 19 3 5 11.61 4.66 19 3 6 13.45 5.61 19 -3 6 7.67 4.65 19 -3 6 8.93 5.19 19 3 6 9.02 5.95 19 3 6 4.50 2.46 19 3 7 5.53 2.20 19 -3 7 9.03 3.58 19 -3 7 5.46 3.55 19 3 7 10.18 5.62 19 3 7 5.80 3.13 19 3 8 37.11 7.27 19 -3 8 31.53 6.81 19 -3 8 32.85 8.28 19 3 8 30.94 9.06 19 3 8 27.29 7.30 19 3 9 11.80 4.53 19 -3 9 12.29 5.26 19 -3 9 15.05 5.56 19 3 9 12.70 6.06 19 -4 -6 6.16 3.49 19 -4 -6 9.66 6.79 19 4 -6 10.58 5.84 19 -4 -5 -1.34 2.72 19 -4 -5 3.12 4.37 19 4 -5 4.64 4.43 19 -4 -4 14.52 6.59 19 -4 -4 15.64 5.51 19 4 -4 5.61 2.73 19 -4 -3 1.28 4.06 19 4 -3 1.78 2.62 19 -4 -2 4.19 2.50 19 -4 -2 9.76 5.09 19 4 -2 8.47 3.45 19 -4 -1 -0.14 4.23 19 -4 -1 0.32 2.75 19 4 -1 -1.67 3.40 19 4 -1 3.98 4.53 19 -4 0 4.64 3.92 19 -4 0 7.73 5.35 19 4 0 6.59 4.27 19 4 0 7.20 4.21 19 -4 1 0.75 2.38 19 -4 1 -2.28 3.70 19 4 1 1.45 1.85 19 4 1 -2.61 4.55 19 4 2 12.24 4.40 19 -4 2 11.23 4.42 19 -4 2 3.32 2.83 19 4 2 8.67 4.43 19 4 3 6.51 5.50 19 -4 3 8.13 3.74 19 -4 3 -1.21 3.22 19 4 3 4.17 3.40 19 4 4 6.70 5.01 19 -4 4 13.21 6.47 19 -4 4 10.17 5.40 19 4 4 4.38 2.80 19 4 5 -2.94 3.71 19 -4 5 3.29 2.60 19 -4 5 1.38 3.91 19 4 5 3.14 4.53 19 4 6 3.61 2.84 19 -4 6 0.53 2.32 19 -4 6 3.56 4.05 19 4 6 -2.05 3.59 20 0 -7 4.52 2.20 20 0 -6 2.27 3.26 20 0 -6 1.14 2.41 20 0 -5 71.30 10.96 20 0 -5 84.18 12.32 20 0 -4 216.17 20.12 20 0 -4 177.98 19.37 20 0 -3 3.92 3.59 20 0 -3 -1.48 3.45 20 0 -2 241.46 20.75 20 0 -2 249.25 21.61 20 0 -1 21.61 6.20 20 0 -1 17.28 5.92 20 0 0 3.15 4.13 20 0 0 -2.72 4.98 20 0 1 26.66 7.14 20 0 1 13.51 3.17 20 0 2 305.61 23.01 20 0 2 252.94 22.07 20 0 3 0.30 2.72 20 0 3 -0.95 4.46 20 0 4 226.95 19.76 20 0 4 184.42 18.60 20 0 5 52.49 9.84 20 0 5 71.87 11.32 20 0 6 -0.27 3.37 20 0 6 1.48 2.90 20 0 7 6.90 4.08 20 0 7 8.52 5.57 20 -1 -7 -3.31 4.63 20 -1 -7 1.88 3.12 20 -1 -6 -3.24 4.19 20 -1 -6 -2.14 2.03 20 1 -6 2.70 6.54 20 -1 -5 8.97 4.56 20 1 -5 1.09 2.85 20 -1 -5 1.51 4.27 20 1 -5 3.73 2.49 20 -1 -4 -1.35 2.34 20 1 -4 -0.23 4.17 20 -1 -4 -3.74 5.80 20 1 -4 8.21 6.39 20 -1 -3 26.07 7.67 20 1 -3 14.15 5.39 20 -1 -3 20.56 6.75 20 1 -3 14.24 5.66 20 -1 -2 10.39 5.29 20 1 -2 4.61 2.93 20 -1 -2 7.09 5.33 20 1 -2 1.88 3.30 20 -1 -1 10.43 5.12 20 1 -1 4.79 2.54 20 -1 -1 9.74 4.00 20 1 -1 6.49 4.42 20 -1 0 -2.64 5.05 20 1 0 0.21 3.21 20 -1 0 -2.99 4.67 20 1 0 1.45 2.16 20 -1 1 7.75 5.80 20 1 1 4.68 3.91 20 -1 1 6.77 4.18 20 1 1 0.24 3.14 20 -1 2 9.10 4.27 20 1 2 13.82 5.00 20 -1 2 2.46 2.62 20 1 2 2.78 2.61 20 -1 3 33.29 8.53 20 1 3 12.98 4.02 20 -1 3 31.69 8.23 20 1 3 25.59 6.96 20 -1 4 5.45 4.00 20 1 4 -0.80 1.97 20 -1 4 -1.17 4.84 20 1 4 2.54 3.17 20 -1 5 10.32 4.24 20 1 5 7.36 4.74 20 -1 5 5.34 4.03 20 1 5 4.30 2.58 20 -1 6 -1.04 3.08 20 1 6 2.41 3.57 20 -1 6 -2.01 2.56 20 1 6 0.26 3.39 20 -1 7 -2.19 2.67 20 1 7 3.05 3.77 20 -1 7 -0.95 3.16 20 1 7 6.00 6.18 20 -2 -5 -3.65 4.78 20 -2 -5 1.44 3.16 20 -2 -4 20.30 5.80 20 2 -4 17.86 6.39 20 -2 -4 16.07 6.67 20 -2 -3 3.96 3.47 20 2 -3 8.70 5.80 20 -2 -3 6.90 5.48 20 2 -3 10.36 5.23 20 -2 -2 119.11 14.38 20 2 -2 90.03 12.72 20 -2 -2 74.79 12.19 20 2 -2 93.01 13.15 20 -2 -1 3.16 4.00 20 2 -1 4.31 2.59 20 -2 -1 9.95 5.01 20 2 -1 5.40 5.16 20 2 -1 7.94 4.24 20 -2 0 6.21 3.88 20 2 0 0.74 2.07 20 -2 0 -0.03 4.01 20 2 0 0.18 5.22 20 2 0 -1.94 2.06 20 -2 1 8.93 4.72 20 2 1 11.08 5.15 20 -2 1 7.03 5.65 20 2 1 3.64 3.76 20 2 1 11.72 4.71 20 -2 2 102.71 13.21 20 2 2 97.80 13.33 20 -2 2 97.61 13.50 20 2 2 84.16 12.20 20 2 2 99.64 13.66 20 -2 3 15.36 4.40 20 -2 3 6.40 2.99 20 2 3 1.73 2.80 20 2 3 5.80 4.93 20 2 3 4.32 2.86 20 -2 4 8.44 3.42 20 -2 4 13.86 4.92 20 2 4 17.39 5.61 20 2 4 18.43 6.08 20 2 4 29.56 8.07 20 -2 5 -0.26 1.94 20 -2 5 9.14 3.12 20 2 5 -0.73 2.66 20 2 5 1.39 2.17 20 2 5 2.97 3.19 0 0 0 0.00 0.00 TITL 009_230K_SulfamerazineF1_ in Pna2(1) REM Pna2(1) (#33, found as Pbn2(1) in ba-c setting) CELL 0.68890 14.481447 8.199275 21.884434 90.0000 90.0000 90.0000 ZERR 8.00 0.000138 0.000086 0.000301 0.0000 0.0000 0.0000 LATT -1 SYMM -x,-y, z+1/2 SYMM x+1/2,-y+1/2, z SYMM -x+1/2, y+1/2, z+1/2 SFAC C H N O S UNIT 88.00 96.00 32.00 16.00 8.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 18772