data_220k_smz-f1_a _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ' 4-amino-N-(4-methylpyrimidin-2-yl) ' _chemical_name_common ' Sulfamerazine ' _chemical_melting_point ? _chemical_formula_moiety 'C11 H12 N4 O2 S' _chemical_formula_sum 'C11 H12 N4 O2 S' _chemical_formula_weight 264.31 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_H-M_alt 'P n a 21' _space_group_name_Hall 'P 2c -2n' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' _cell_length_a 14.47950(10) _cell_length_b 8.19740(10) _cell_length_c 21.8693(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 2595.76(5) _cell_formula_units_Z 8 _cell_measurement_temperature 220 _cell_measurement_reflns_used 11252 _cell_measurement_theta_min 1.8030 _cell_measurement_theta_max 29.4970 _exptl_crystal_description Parallelepiped _exptl_crystal_colour Colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.353 _exptl_crystal_F_000 1104 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.50 _exptl_crystal_size_mid 0.40 _exptl_crystal_size_min 0.20 _exptl_absorpt_coefficient_mu 0.249 _shelx_estimated_absorpt_T_min 0.885 _shelx_estimated_absorpt_T_max 0.952 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.97856 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _diffrn_ambient_temperature 220 _diffrn_radiation_wavelength 0.68890 _diffrn_radiation_type 'Synchrotron' _diffrn_radiation_source 'Diamond Light Source Beamline I19' _diffrn_radiation_monochromator 'double crystal Silicon 111' _diffrn_measurement_specimen_support 'MiTeGen loop' _diffrn_measurement_device 'CrystalLogic Kappa (3 circle)' _diffrn_measurement_device_type 'Rigaku Saturn724+ (2x2 bin mode)' _diffrn_measurement_method ; omega rotation with 1 degree frames ; _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 23478 _diffrn_reflns_av_unetI/netI 0.0432 _diffrn_reflns_av_R_equivalents 0.0448 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_theta_min 1.805 _diffrn_reflns_theta_max 29.476 _diffrn_reflns_theta_full 24.415 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.968 _diffrn_reflns_point_group_measured_fraction_full 0.988 _reflns_number_total 7666 _reflns_number_gt 6189 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.895 _reflns_Friedel_fraction_max 0.936 _reflns_Friedel_fraction_full 0.978 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_structure_solution 'SHELXT' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'OSCAIL' _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0541P)^2^+0.3587P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 2364 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.01(5) _chemical_absolute_configuration ad _refine_ls_number_reflns 7666 _refine_ls_number_parameters 344 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0595 _refine_ls_R_factor_gt 0.0453 _refine_ls_wR_factor_ref 0.1195 _refine_ls_wR_factor_gt 0.1081 _refine_ls_goodness_of_fit_ref 1.022 _refine_ls_restrained_S_all 1.022 _refine_ls_shift/su_max 0.029 _refine_ls_shift/su_mean 0.001 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.64534(5) 0.49522(9) 0.34400(4) 0.02926(17) Uani 1 1 d . . . . . S2 S 0.57789(5) 0.49664(9) 0.65284(4) 0.02832(17) Uani 1 1 d . . . . . O1 O 0.68867(17) 0.3705(3) 0.30832(12) 0.0380(5) Uani 1 1 d . . . . . O2 O 0.54816(16) 0.5223(3) 0.33741(13) 0.0380(6) Uani 1 1 d . . . . . O3 O 0.67531(15) 0.4692(3) 0.65927(13) 0.0359(5) Uani 1 1 d . . . . . O4 O 0.53552(17) 0.6236(3) 0.68772(12) 0.0370(5) Uani 1 1 d . . . . . N1 N 0.8422(2) 1.1168(4) 0.31238(18) 0.0457(8) Uani 1 1 d . . . . . N2 N 0.6545(2) 0.4482(4) 0.41728(15) 0.0339(6) Uani 1 1 d . . . . . N3 N 0.81414(19) 0.4090(3) 0.41719(15) 0.0345(6) Uani 1 1 d . . . . . N4 N 0.7279(2) 0.4301(5) 0.50958(15) 0.0475(8) Uani 1 1 d . . . . . N5 N 0.3803(2) -0.1199(4) 0.69533(19) 0.0546(10) Uani 1 1 d . . . . . H5A H 0.3238 -0.1186 0.7075 0.071 Uiso 1 1 calc R U . . . H5B H 0.4077 -0.2114 0.6889 0.071 Uiso 1 1 calc R U . . . N6 N 0.5682(2) 0.5393(4) 0.57956(15) 0.0353(6) Uani 1 1 d . . . . . N7 N 0.40972(19) 0.5866(4) 0.58013(14) 0.0350(6) Uani 1 1 d . . . . . N8 N 0.4957(2) 0.5654(5) 0.48740(16) 0.0467(8) Uani 1 1 d . . . . . C1 C 0.7040(2) 0.6773(4) 0.33387(17) 0.0278(6) Uani 1 1 d . . . . . C2 C 0.7941(2) 0.6792(4) 0.31066(16) 0.0287(6) Uani 1 1 d . . . . . H2 H 0.8232 0.5819 0.3003 0.037 Uiso 1 1 calc R U . . . C3 C 0.8395(2) 0.8254(4) 0.30316(17) 0.0287(7) Uani 1 1 d . . . . . H3 H 0.8993 0.8263 0.2875 0.037 Uiso 1 1 calc R U . . . C4 C 0.7967(2) 0.9731(4) 0.31887(16) 0.0304(7) Uani 1 1 d . . . . . C5 C 0.7060(2) 0.9693(4) 0.3425(2) 0.0338(7) Uani 1 1 d . . . . . H5 H 0.6767 1.0662 0.3532 0.044 Uiso 1 1 calc R U . . . C6 C 0.6608(2) 0.8233(4) 0.35000(18) 0.0334(7) Uani 1 1 d . . . . . H6 H 0.6012 0.8217 0.3659 0.043 Uiso 1 1 calc R U . . . C7 C 0.7367(2) 0.4283(4) 0.44899(16) 0.0316(7) Uani 1 1 d . . . . . C8 C 0.8060(3) 0.4052(8) 0.5407(2) 0.0659(14) Uani 1 1 d . . . . . H8 H 0.8035 0.4023 0.5831 0.086 Uiso 1 1 calc R U . . . C9 C 0.8899(3) 0.3837(7) 0.5125(2) 0.0606(12) Uani 1 1 d . . . . . H9 H 0.9434 0.3665 0.5351 0.079 Uiso 1 1 calc R U . . . C10 C 0.8920(2) 0.3884(5) 0.4498(2) 0.0429(9) Uani 1 1 d . . . . . C11 C 0.9785(3) 0.3690(6) 0.4137(2) 0.0566(11) Uani 1 1 d . . . . . H11A H 0.9824 0.2595 0.3984 0.074 Uiso 1 1 calc R U . . . H11B H 1.0308 0.3908 0.4395 0.074 Uiso 1 1 calc R U . . . H11C H 0.9783 0.4443 0.3801 0.074 Uiso 1 1 calc R U . . . C12 C 0.5189(2) 0.3159(3) 0.66584(15) 0.0272(6) Uani 1 1 d . . . . . C13 C 0.5635(2) 0.1687(4) 0.6557(2) 0.0365(8) Uani 1 1 d . . . . . H13 H 0.6244 0.1679 0.6423 0.047 Uiso 1 1 calc R U . . . C14 C 0.5180(3) 0.0238(4) 0.6653(2) 0.0423(9) Uani 1 1 d . . . . . H14 H 0.5482 -0.0744 0.6579 0.055 Uiso 1 1 calc R U . . . C15 C 0.4262(2) 0.0227(4) 0.68614(18) 0.0352(8) Uani 1 1 d . . . . . C16 C 0.3820(2) 0.1725(4) 0.69645(17) 0.0319(7) Uani 1 1 d . . . . . H16 H 0.3211 0.1739 0.7100 0.042 Uiso 1 1 calc R U . . . C17 C 0.4277(2) 0.3173(4) 0.68672(17) 0.0297(7) Uani 1 1 d . . . . . H17 H 0.3980 0.4159 0.6940 0.039 Uiso 1 1 calc R U . . . C18 C 0.4865(2) 0.5653(4) 0.54806(16) 0.0315(7) Uani 1 1 d . . . . . C19 C 0.4176(3) 0.5974(7) 0.4566(2) 0.0640(14) Uani 1 1 d . . . . . H19 H 0.4198 0.6013 0.4142 0.083 Uiso 1 1 calc R U . . . C20 C 0.3352(3) 0.6244(7) 0.4850(2) 0.0658(14) Uani 1 1 d . . . . . H20 H 0.2825 0.6486 0.4625 0.086 Uiso 1 1 calc R U . . . C21 C 0.3322(3) 0.6150(5) 0.5479(2) 0.0435(9) Uani 1 1 d . . . . . C22 C 0.2452(3) 0.6356(6) 0.5843(2) 0.0609(12) Uani 1 1 d . . . . . H22A H 0.2474 0.7372 0.6061 0.079 Uiso 1 1 calc R U . . . H22B H 0.2395 0.5473 0.6129 0.079 Uiso 1 1 calc R U . . . H22C H 0.1930 0.6354 0.5573 0.079 Uiso 1 1 calc R U . . . H1N1 H 0.890(3) 1.120(5) 0.292(2) 0.042(11) Uiso 1 1 d . . . . . H2N1 H 0.812(3) 1.200(6) 0.316(2) 0.056(13) Uiso 1 1 d . . . . . H1N2 H 0.616(3) 0.479(5) 0.438(2) 0.043(13) Uiso 1 1 d . . . . . H1N6 H 0.619(3) 0.504(5) 0.559(2) 0.056(14) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0270(3) 0.0314(3) 0.0294(4) 0.0024(3) -0.0015(3) -0.0021(3) S2 0.0263(3) 0.0309(3) 0.0278(4) 0.0032(3) -0.0013(3) -0.0017(3) O1 0.0445(13) 0.0319(11) 0.0376(14) -0.0039(10) 0.0005(11) -0.0015(10) O2 0.0274(11) 0.0472(13) 0.0395(15) 0.0071(12) -0.0049(12) -0.0052(9) O3 0.0262(11) 0.0460(13) 0.0354(14) 0.0064(11) -0.0053(11) -0.0025(9) O4 0.0407(13) 0.0302(11) 0.0402(14) -0.0035(10) -0.0001(11) -0.0021(9) N1 0.0405(17) 0.0321(15) 0.064(2) -0.0079(15) 0.0183(17) -0.0048(12) N2 0.0247(12) 0.0451(16) 0.0318(17) 0.0072(13) 0.0010(12) 0.0000(11) N3 0.0274(13) 0.0371(14) 0.0390(18) 0.0031(12) 0.0030(12) 0.0011(11) N4 0.0336(15) 0.078(2) 0.0308(18) 0.0045(16) -0.0021(13) 0.0130(15) N5 0.0461(18) 0.0324(14) 0.085(3) -0.0036(16) 0.0150(19) -0.0089(13) N6 0.0260(12) 0.0498(16) 0.0301(17) 0.0091(14) 0.0021(12) 0.0025(12) N7 0.0283(13) 0.0402(15) 0.0363(17) 0.0014(12) 0.0015(12) 0.0027(11) N8 0.0342(15) 0.073(2) 0.0328(19) 0.0054(16) -0.0033(14) 0.0132(15) C1 0.0260(14) 0.0294(13) 0.0280(17) 0.0012(12) 0.0006(13) 0.0016(10) C2 0.0283(14) 0.0308(14) 0.0271(17) -0.0011(12) 0.0002(13) 0.0038(11) C3 0.0247(14) 0.0353(16) 0.0260(18) 0.0002(13) 0.0045(13) 0.0006(11) C4 0.0313(15) 0.0327(14) 0.0272(17) -0.0013(12) 0.0001(13) -0.0031(11) C5 0.0321(15) 0.0302(14) 0.039(2) -0.0018(15) 0.0085(17) 0.0023(11) C6 0.0283(14) 0.0350(15) 0.037(2) 0.0013(14) 0.0076(14) 0.0016(11) C7 0.0278(15) 0.0337(15) 0.033(2) 0.0051(13) -0.0011(13) 0.0032(12) C8 0.046(2) 0.117(4) 0.035(2) 0.005(3) -0.0050(19) 0.023(3) C9 0.0329(19) 0.102(4) 0.047(3) -0.003(3) -0.0100(19) 0.017(2) C10 0.0301(17) 0.047(2) 0.052(3) 0.0008(18) -0.0006(16) 0.0071(14) C11 0.0326(19) 0.074(3) 0.064(3) -0.004(2) 0.0041(19) 0.0063(18) C12 0.0270(13) 0.0281(13) 0.0263(17) 0.0016(11) 0.0016(12) -0.0002(10) C13 0.0271(15) 0.0333(15) 0.049(2) -0.0027(16) 0.0074(17) 0.0025(11) C14 0.0364(17) 0.0303(15) 0.060(3) -0.0027(16) 0.0052(17) 0.0058(12) C15 0.0347(17) 0.0314(15) 0.039(2) -0.0024(13) 0.0038(15) -0.0015(12) C16 0.0304(15) 0.0345(15) 0.0309(18) -0.0055(13) 0.0031(13) -0.0020(11) C17 0.0295(15) 0.0314(14) 0.0284(18) -0.0016(13) 0.0032(13) 0.0006(11) C18 0.0274(14) 0.0362(15) 0.0309(19) 0.0041(13) 0.0000(13) 0.0010(12) C19 0.046(2) 0.111(4) 0.035(2) 0.001(2) -0.0090(19) 0.023(2) C20 0.041(2) 0.109(4) 0.047(3) -0.006(3) -0.012(2) 0.028(2) C21 0.0316(17) 0.049(2) 0.050(3) -0.0034(18) -0.0023(16) 0.0087(15) C22 0.0311(18) 0.079(3) 0.073(3) -0.005(3) 0.005(2) 0.0092(19) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 O1 1.431(3) . ? S1 O2 1.432(2) . ? S1 N2 1.654(3) . ? S1 C1 1.732(3) . ? S2 O4 1.429(2) . ? S2 O3 1.435(2) . ? S2 N6 1.646(3) . ? S2 C12 1.733(3) . ? N1 C4 1.357(4) . ? N1 H1N1 0.82(4) . ? N1 H2N1 0.81(4) . ? N2 C7 1.388(4) . ? N2 H1N2 0.76(5) . ? N3 C7 1.328(4) . ? N3 C10 1.344(5) . ? N4 C7 1.331(5) . ? N4 C8 1.335(5) . ? N5 C15 1.360(4) . ? N5 H5A 0.8600 . ? N5 H5B 0.8600 . ? N6 C18 1.386(4) . ? N6 H1N6 0.92(5) . ? N7 C18 1.326(4) . ? N7 C21 1.346(5) . ? N8 C18 1.333(5) . ? N8 C19 1.342(5) . ? C1 C6 1.396(4) . ? C1 C2 1.399(4) . ? C2 C3 1.378(4) . ? C2 H2 0.9300 . ? C3 C4 1.403(4) . ? C3 H3 0.9300 . ? C4 C5 1.412(4) . ? C5 C6 1.373(4) . ? C5 H5 0.9300 . ? C6 H6 0.9300 . ? C8 C9 1.374(6) . ? C8 H8 0.9300 . ? C9 C10 1.372(6) . ? C9 H9 0.9300 . ? C10 C11 1.488(5) . ? C11 H11A 0.9600 . ? C11 H11B 0.9600 . ? C11 H11C 0.9600 . ? C12 C13 1.387(4) . ? C12 C17 1.397(4) . ? C13 C14 1.374(5) . ? C13 H13 0.9300 . ? C14 C15 1.405(5) . ? C14 H14 0.9300 . ? C15 C16 1.403(4) . ? C16 C17 1.376(4) . ? C16 H16 0.9300 . ? C17 H17 0.9300 . ? C19 C20 1.363(6) . ? C19 H19 0.9300 . ? C20 C21 1.380(7) . ? C20 H20 0.9300 . ? C21 C22 1.499(6) . ? C22 H22A 0.9600 . ? C22 H22B 0.9600 . ? C22 H22C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 S1 O2 119.12(16) . . ? O1 S1 N2 109.07(17) . . ? O2 S1 N2 102.26(16) . . ? O1 S1 C1 109.32(16) . . ? O2 S1 C1 109.63(14) . . ? N2 S1 C1 106.60(17) . . ? O4 S2 O3 118.93(16) . . ? O4 S2 N6 109.19(16) . . ? O3 S2 N6 102.25(16) . . ? O4 S2 C12 108.86(16) . . ? O3 S2 C12 109.52(14) . . ? N6 S2 C12 107.42(16) . . ? C4 N1 H1N1 120(3) . . ? C4 N1 H2N1 117(3) . . ? H1N1 N1 H2N1 118(4) . . ? C7 N2 S1 125.5(3) . . ? C7 N2 H1N2 112(4) . . ? S1 N2 H1N2 116(4) . . ? C7 N3 C10 116.4(3) . . ? C7 N4 C8 115.1(4) . . ? C15 N5 H5A 120.0 . . ? C15 N5 H5B 120.0 . . ? H5A N5 H5B 120.0 . . ? C18 N6 S2 126.1(2) . . ? C18 N6 H1N6 119(3) . . ? S2 N6 H1N6 110(3) . . ? C18 N7 C21 116.5(3) . . ? C18 N8 C19 114.5(3) . . ? C6 C1 C2 120.0(3) . . ? C6 C1 S1 119.1(2) . . ? C2 C1 S1 120.9(2) . . ? C3 C2 C1 119.9(3) . . ? C3 C2 H2 120.1 . . ? C1 C2 H2 120.1 . . ? C2 C3 C4 120.7(3) . . ? C2 C3 H3 119.7 . . ? C4 C3 H3 119.7 . . ? N1 C4 C3 120.6(3) . . ? N1 C4 C5 120.6(3) . . ? C3 C4 C5 118.8(3) . . ? C6 C5 C4 120.4(3) . . ? C6 C5 H5 119.8 . . ? C4 C5 H5 119.8 . . ? C5 C6 C1 120.2(3) . . ? C5 C6 H6 119.9 . . ? C1 C6 H6 119.9 . . ? N3 C7 N4 127.1(3) . . ? N3 C7 N2 118.5(3) . . ? N4 C7 N2 114.4(3) . . ? N4 C8 C9 122.7(4) . . ? N4 C8 H8 118.7 . . ? C9 C8 H8 118.7 . . ? C10 C9 C8 117.7(4) . . ? C10 C9 H9 121.2 . . ? C8 C9 H9 121.2 . . ? N3 C10 C9 121.0(3) . . ? N3 C10 C11 116.0(4) . . ? C9 C10 C11 123.0(4) . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C13 C12 C17 119.9(3) . . ? C13 C12 S2 119.2(2) . . ? C17 C12 S2 120.8(2) . . ? C14 C13 C12 120.3(3) . . ? C14 C13 H13 119.8 . . ? C12 C13 H13 119.8 . . ? C13 C14 C15 120.5(3) . . ? C13 C14 H14 119.7 . . ? C15 C14 H14 119.7 . . ? N5 C15 C16 120.4(3) . . ? N5 C15 C14 121.0(3) . . ? C16 C15 C14 118.6(3) . . ? C17 C16 C15 120.7(3) . . ? C17 C16 H16 119.7 . . ? C15 C16 H16 119.6 . . ? C16 C17 C12 119.9(3) . . ? C16 C17 H17 120.0 . . ? C12 C17 H17 120.0 . . ? N7 C18 N8 127.6(3) . . ? N7 C18 N6 118.3(3) . . ? N8 C18 N6 114.2(3) . . ? N8 C19 C20 122.8(4) . . ? N8 C19 H19 118.6 . . ? C20 C19 H19 118.6 . . ? C19 C20 C21 118.2(4) . . ? C19 C20 H20 120.9 . . ? C21 C20 H20 120.9 . . ? N7 C21 C20 120.3(4) . . ? N7 C21 C22 116.3(4) . . ? C20 C21 C22 123.4(4) . . ? C21 C22 H22A 109.5 . . ? C21 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C21 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 S1 N2 C7 60.7(3) . . . . ? O2 S1 N2 C7 -172.3(3) . . . . ? C1 S1 N2 C7 -57.3(3) . . . . ? O4 S2 N6 C18 -57.8(3) . . . . ? O3 S2 N6 C18 175.4(3) . . . . ? C12 S2 N6 C18 60.1(3) . . . . ? O1 S1 C1 C6 162.4(3) . . . . ? O2 S1 C1 C6 30.2(4) . . . . ? N2 S1 C1 C6 -79.8(3) . . . . ? O1 S1 C1 C2 -18.5(3) . . . . ? O2 S1 C1 C2 -150.7(3) . . . . ? N2 S1 C1 C2 99.3(3) . . . . ? C6 C1 C2 C3 -0.7(5) . . . . ? S1 C1 C2 C3 -179.8(3) . . . . ? C1 C2 C3 C4 0.3(5) . . . . ? C2 C3 C4 N1 178.9(3) . . . . ? C2 C3 C4 C5 0.0(5) . . . . ? N1 C4 C5 C6 -178.9(4) . . . . ? C3 C4 C5 C6 0.0(6) . . . . ? C4 C5 C6 C1 -0.4(6) . . . . ? C2 C1 C6 C5 0.7(6) . . . . ? S1 C1 C6 C5 179.8(3) . . . . ? C10 N3 C7 N4 0.3(5) . . . . ? C10 N3 C7 N2 -179.3(3) . . . . ? C8 N4 C7 N3 -1.9(6) . . . . ? C8 N4 C7 N2 177.7(4) . . . . ? S1 N2 C7 N3 -15.9(5) . . . . ? S1 N2 C7 N4 164.5(3) . . . . ? C7 N4 C8 C9 1.7(8) . . . . ? N4 C8 C9 C10 0.0(9) . . . . ? C7 N3 C10 C9 1.6(6) . . . . ? C7 N3 C10 C11 -179.2(3) . . . . ? C8 C9 C10 N3 -1.7(7) . . . . ? C8 C9 C10 C11 179.2(5) . . . . ? O4 S2 C12 C13 -157.3(3) . . . . ? O3 S2 C12 C13 -25.7(3) . . . . ? N6 S2 C12 C13 84.6(3) . . . . ? O4 S2 C12 C17 22.3(3) . . . . ? O3 S2 C12 C17 153.9(3) . . . . ? N6 S2 C12 C17 -95.8(3) . . . . ? C17 C12 C13 C14 0.9(6) . . . . ? S2 C12 C13 C14 -179.6(3) . . . . ? C12 C13 C14 C15 -0.7(6) . . . . ? C13 C14 C15 N5 179.5(4) . . . . ? C13 C14 C15 C16 0.5(6) . . . . ? N5 C15 C16 C17 -179.4(3) . . . . ? C14 C15 C16 C17 -0.4(6) . . . . ? C15 C16 C17 C12 0.6(5) . . . . ? C13 C12 C17 C16 -0.8(5) . . . . ? S2 C12 C17 C16 179.7(3) . . . . ? C21 N7 C18 N8 -1.5(5) . . . . ? C21 N7 C18 N6 178.6(3) . . . . ? C19 N8 C18 N7 2.8(6) . . . . ? C19 N8 C18 N6 -177.3(4) . . . . ? S2 N6 C18 N7 12.6(5) . . . . ? S2 N6 C18 N8 -167.3(3) . . . . ? C18 N8 C19 C20 -1.2(8) . . . . ? N8 C19 C20 C21 -1.4(9) . . . . ? C18 N7 C21 C20 -1.4(6) . . . . ? C18 N7 C21 C22 178.8(4) . . . . ? C19 C20 C21 N7 2.8(8) . . . . ? C19 C20 C21 C22 -177.5(5) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N5 H5B O4 0.86 2.29 3.083(4) 152.8 1_545 N1 H1N1 O4 0.82(4) 2.53(5) 3.251(4) 147(4) 4_654 N1 H2N1 O1 0.81(4) 2.27(4) 3.045(4) 159(4) 1_565 N2 H1N2 N8 0.76(5) 2.17(5) 2.925(5) 174(5) . N6 H1N6 N4 0.92(5) 2.00(5) 2.913(5) 177(5) . _refine_diff_density_max 0.293 _refine_diff_density_min -0.324 _refine_diff_density_rms 0.047 _shelx_res_file ; 220k_smz-f1_a.res created by SHELXL-2014/7 TITL 220k_smz-f1_a.res in Pna2(1) REM Old TITL 010_220K_SulfamerazineF1_ in Pna2(1) REM SHELXT solution in Pna2(1) REM R1 0.098, Rweak 0.022, Alpha 0.002, Orientation as input REM Flack x = 0.020 ( 0.042 ) from Parsons' quotients REM Formula found by SHELXT: C26 N4 O4 S2 CELL 0.68890 14.4795 8.1974 21.8693 90.000 90.000 90.000 ZERR 8.000 0.0001 0.0001 0.0003 0.000 0.000 0.000 REM SG 33 4 4 Pna21 PGmm2 Orthorhombic LATT -1 REM SG ASUN 1 .5 .5 1. REM SG ORGN on 2(1) SYMM -X,-Y,0.5+Z SYMM 0.5+X,0.5-Y,Z SYMM 0.5-X,0.5+Y,0.5+Z SFAC C H N O S UNIT 88.00 96.00 32.00 16.00 8.00 L.S. 10 SIZE 0.50 0.40 0.20 BOND $H FMAP 2 PLAN 20 ACTA CONF EQIV $1 x, y-1, z HTAB N5 O4_$1 EQIV $2 -x+3/2, y+1/2, z-1/2 HTAB N1 O4_$2 EQIV $3 x, y+1, z HTAB N1 O1_$3 HTAB N2 N8 HTAB N6 N4 LIST 4 WGHT 0.054100 0.358700 FVAR 0.51638 0.35344 S1 5 0.645337 0.495222 0.344002 11.00000 0.02701 0.03139 = 0.02937 0.00240 -0.00153 -0.00214 S2 5 0.577894 0.496636 0.652835 11.00000 0.02631 0.03089 = 0.02776 0.00324 -0.00132 -0.00167 O1 4 0.688668 0.370472 0.308320 11.00000 0.04448 0.03190 = 0.03764 -0.00386 0.00046 -0.00151 O2 4 0.548157 0.522288 0.337412 11.00000 0.02741 0.04723 = 0.03948 0.00708 -0.00485 -0.00520 O3 4 0.675309 0.469193 0.659274 11.00000 0.02618 0.04605 = 0.03537 0.00635 -0.00532 -0.00254 O4 4 0.535517 0.623573 0.687723 11.00000 0.04066 0.03016 = 0.04016 -0.00355 -0.00010 -0.00211 N1 3 0.842174 1.116826 0.312381 11.00000 0.04047 0.03209 = 0.06441 -0.00794 0.01826 -0.00477 N2 3 0.654469 0.448192 0.417279 11.00000 0.02468 0.04511 = 0.03179 0.00719 0.00100 -0.00002 N3 3 0.814144 0.409023 0.417190 11.00000 0.02738 0.03710 = 0.03904 0.00312 0.00300 0.00106 N4 3 0.727895 0.430122 0.509576 11.00000 0.03360 0.07798 = 0.03079 0.00448 -0.00214 0.01304 N5 3 0.380276 -0.119899 0.695334 11.00000 0.04612 0.03242 = 0.08526 -0.00361 0.01504 -0.00886 AFIX 93 H5A 2 0.323817 -0.118597 0.707534 11.00000 -1.30000 H5B 2 0.407693 -0.211391 0.688947 11.00000 -1.30000 AFIX 0 N6 3 0.568240 0.539292 0.579563 11.00000 0.02604 0.04978 = 0.03012 0.00914 0.00208 0.00255 N7 3 0.409719 0.586580 0.580126 11.00000 0.02833 0.04023 = 0.03635 0.00141 0.00147 0.00269 N8 3 0.495733 0.565384 0.487400 11.00000 0.03418 0.07328 = 0.03276 0.00536 -0.00334 0.01325 C1 1 0.704046 0.677326 0.333869 11.00000 0.02600 0.02941 = 0.02799 0.00122 0.00064 0.00158 C2 1 0.794090 0.679171 0.310665 11.00000 0.02834 0.03079 = 0.02707 -0.00108 0.00021 0.00381 AFIX 43 H2 2 0.823194 0.581866 0.300331 11.00000 -1.30000 AFIX 0 C3 1 0.839539 0.825442 0.303159 11.00000 0.02472 0.03530 = 0.02603 0.00020 0.00454 0.00058 AFIX 43 H3 2 0.899263 0.826322 0.287516 11.00000 -1.30000 AFIX 0 C4 1 0.796660 0.973119 0.318869 11.00000 0.03129 0.03272 = 0.02721 -0.00129 0.00007 -0.00306 C5 1 0.705979 0.969317 0.342544 11.00000 0.03209 0.03019 = 0.03926 -0.00179 0.00850 0.00231 AFIX 43 H5 2 0.676655 1.066205 0.353152 11.00000 -1.30000 AFIX 0 C6 1 0.660829 0.823323 0.349998 11.00000 0.02834 0.03502 = 0.03699 0.00129 0.00765 0.00157 AFIX 43 H6 2 0.601237 0.821731 0.365851 11.00000 -1.30000 AFIX 0 C7 1 0.736741 0.428346 0.448990 11.00000 0.02782 0.03368 = 0.03331 0.00510 -0.00110 0.00321 C8 1 0.806001 0.405192 0.540661 11.00000 0.04562 0.11698 = 0.03495 0.00533 -0.00498 0.02262 AFIX 43 H8 2 0.803501 0.402277 0.583140 11.00000 -1.30000 AFIX 0 C9 1 0.889900 0.383674 0.512463 11.00000 0.03294 0.10224 = 0.04658 -0.00349 -0.00998 0.01731 AFIX 43 H9 2 0.943409 0.366516 0.535088 11.00000 -1.30000 AFIX 0 C10 1 0.892015 0.388375 0.449762 11.00000 0.03013 0.04667 = 0.05199 0.00082 -0.00056 0.00714 C11 1 0.978544 0.369014 0.413741 11.00000 0.03257 0.07363 = 0.06358 -0.00357 0.00411 0.00627 AFIX 137 H11A 2 0.982363 0.259511 0.398385 11.00000 -1.30000 H11B 2 1.030811 0.390752 0.439490 11.00000 -1.30000 H11C 2 0.978265 0.444294 0.380115 11.00000 -1.30000 AFIX 0 C12 1 0.518920 0.315948 0.665837 11.00000 0.02703 0.02810 = 0.02632 0.00158 0.00161 -0.00018 C13 1 0.563479 0.168651 0.655675 11.00000 0.02710 0.03330 = 0.04916 -0.00274 0.00742 0.00254 AFIX 43 H13 2 0.624446 0.167922 0.642298 11.00000 -1.30000 AFIX 0 C14 1 0.517976 0.023762 0.665278 11.00000 0.03642 0.03032 = 0.06022 -0.00267 0.00525 0.00576 AFIX 43 H14 2 0.548181 -0.074410 0.657906 11.00000 -1.30000 AFIX 0 C15 1 0.426203 0.022733 0.686140 11.00000 0.03465 0.03142 = 0.03940 -0.00241 0.00377 -0.00153 C16 1 0.381985 0.172493 0.696451 11.00000 0.03042 0.03449 = 0.03089 -0.00545 0.00307 -0.00201 AFIX 43 H16 2 0.321113 0.173905 0.710008 11.00000 -1.30000 AFIX 0 C17 1 0.427714 0.317294 0.686721 11.00000 0.02946 0.03139 = 0.02837 -0.00164 0.00321 0.00061 AFIX 43 H17 2 0.397969 0.415936 0.694032 11.00000 -1.30000 AFIX 0 C18 1 0.486531 0.565293 0.548059 11.00000 0.02740 0.03619 = 0.03094 0.00405 -0.00001 0.00100 C19 1 0.417640 0.597384 0.456635 11.00000 0.04575 0.11087 = 0.03546 0.00061 -0.00900 0.02307 AFIX 43 H19 2 0.419843 0.601263 0.414159 11.00000 -1.30000 AFIX 0 C20 1 0.335237 0.624443 0.484970 11.00000 0.04101 0.10914 = 0.04738 -0.00631 -0.01191 0.02778 AFIX 43 H20 2 0.282481 0.648638 0.462473 11.00000 -1.30000 AFIX 0 C21 1 0.332159 0.614986 0.547932 11.00000 0.03159 0.04893 = 0.04987 -0.00339 -0.00235 0.00871 C22 1 0.245189 0.635566 0.584330 11.00000 0.03112 0.07874 = 0.07280 -0.00494 0.00489 0.00916 AFIX 137 H22A 2 0.247371 0.737183 0.606103 11.00000 -1.30000 H22B 2 0.239501 0.547323 0.612943 11.00000 -1.30000 H22C 2 0.193008 0.635371 0.557250 11.00000 -1.30000 AFIX 0 H1N1 2 0.890225 1.120124 0.292442 11.00000 0.04236 H2N1 2 0.811972 1.200001 0.315564 11.00000 0.05574 H1N2 2 0.615595 0.479042 0.437827 11.00000 0.04302 H1N6 2 0.619391 0.503709 0.558615 11.00000 0.05611 HKLF 4 REM 220k_smz-f1_a.res in Pna2(1) REM R1 = 0.0453 for 6189 Fo > 4sig(Fo) and 0.0595 for all 7666 data REM 344 parameters refined using 1 restraints END WGHT 0.0513 0.3779 REM Highest difference peak 0.293, deepest hole -0.324, 1-sigma level 0.047 Q1 1 0.5448 0.3989 0.6558 11.00000 0.05 0.29 Q2 1 0.8086 0.7619 0.3065 11.00000 0.05 0.25 Q3 1 0.8170 0.9024 0.3135 11.00000 0.05 0.25 Q4 1 0.6800 0.5951 0.3451 11.00000 0.05 0.25 Q5 1 0.2063 0.5412 0.5629 11.00000 0.05 0.22 Q6 1 0.5470 0.2405 0.6681 11.00000 0.05 0.21 Q7 1 0.6926 0.7530 0.3496 11.00000 0.05 0.21 Q8 1 0.7539 0.6786 0.3425 11.00000 0.05 0.20 Q9 1 0.4130 0.2337 0.6908 11.00000 0.05 0.20 Q10 1 0.8092 0.4135 0.3715 11.00000 0.05 0.20 Q11 1 0.4179 0.1016 0.6979 11.00000 0.05 0.20 Q12 1 0.7555 0.9620 0.3390 11.00000 0.05 0.19 Q13 1 0.4718 0.3138 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3.37 3.42 5 4 26 -1.44 2.14 5 -5 -27 6.61 3.32 5 -5 -26 16.12 5.58 5 -5 -25 13.71 4.83 5 -5 -24 44.79 8.57 5 -5 -23 9.30 4.70 5 -5 -22 6.85 2.14 5 -5 -21 47.36 8.15 -5 -5 -20 121.49 12.86 5 -5 -20 111.89 11.91 5 -5 -20 120.49 13.14 -5 -5 -19 5.97 3.74 5 -5 -19 1.42 2.50 5 -5 -19 6.41 3.02 -5 -5 -18 4.34 1.99 5 -5 -18 11.92 3.96 5 -5 -18 9.33 3.81 -5 -5 -17 65.29 9.04 5 -5 -17 81.41 10.32 5 -5 -17 53.21 7.94 5 5 -16 1.93 1.77 -5 -5 -16 -0.91 1.71 5 -5 -16 -1.24 3.46 5 -5 -16 -0.04 1.69 -5 -5 -15 157.89 13.24 5 -5 -15 152.85 13.53 5 5 -15 145.75 12.69 5 -5 -15 150.58 13.33 5 5 -14 46.76 6.97 -5 -5 -14 66.68 8.33 5 -5 -14 70.37 9.09 5 -5 -14 64.06 9.04 5 -5 -13 2.82 2.70 5 5 -13 6.13 2.56 -5 -5 -13 0.91 1.93 5 -5 -13 5.71 3.24 5 5 -12 15.84 4.01 -5 -5 -12 23.81 5.13 5 -5 -12 22.92 5.34 5 -5 -12 30.84 6.16 5 5 -11 180.41 13.63 -5 -5 -11 189.96 13.48 -5 5 -11 167.01 11.38 5 -5 -11 184.16 14.37 5 -5 -11 188.71 13.95 -5 -5 -10 67.60 8.44 -5 5 -10 53.26 6.77 5 -5 -10 52.94 7.70 5 -5 -10 38.24 6.62 5 5 -10 60.63 7.83 5 5 -9 106.88 10.15 -5 -5 -9 108.80 9.95 -5 5 -9 121.64 9.71 5 -5 -9 101.95 10.15 5 -5 -9 117.17 11.03 5 5 -8 23.20 4.68 -5 5 -8 37.63 5.67 5 -5 -8 30.04 5.76 5 5 -8 19.47 3.22 5 -5 -8 32.19 5.46 5 5 -7 24.74 5.05 -5 5 -7 21.51 3.92 5 -5 -7 21.29 5.39 5 -5 -7 31.98 5.63 5 5 -7 31.42 4.55 5 5 -6 331.40 17.23 5 5 -6 358.75 15.11 -5 5 -6 382.25 17.54 5 -5 -6 338.76 17.45 5 -5 -6 358.40 18.58 5 -5 -5 179.54 12.60 5 5 -5 181.57 11.40 -5 5 -5 178.60 12.07 5 5 -5 178.21 12.68 5 -5 -5 191.54 13.63 5 -5 -4 12.06 3.08 5 5 -4 10.72 3.95 5 5 -4 11.94 3.07 5 -5 -4 8.86 2.64 -5 5 -4 13.77 3.66 5 5 -3 44.21 6.19 5 5 -3 39.09 5.42 -5 5 -3 39.88 5.68 5 -5 -3 44.98 6.15 5 -5 -3 31.40 5.37 5 5 -2 26.26 4.76 5 5 -2 33.85 5.06 5 -5 -2 34.31 5.59 5 -5 -2 29.21 5.22 5 5 -1 70.81 7.38 5 -5 -1 70.95 8.19 5 5 -1 63.80 7.86 5 -5 -1 59.45 7.00 5 5 0 191.41 12.85 5 5 0 229.81 13.54 5 -5 0 213.82 13.35 5 -5 0 206.28 13.57 5 5 1 63.06 7.52 5 5 1 61.08 6.99 5 -5 1 55.81 6.62 5 -5 1 62.69 7.40 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5.10 5 6 -11 19.22 4.93 -5 -6 -11 22.72 4.79 5 -6 -11 16.79 4.24 5 6 -10 7.60 2.66 -5 -6 -10 3.47 1.43 -5 6 -10 13.65 3.67 5 -6 -10 5.97 3.13 5 -6 -10 12.17 4.47 5 6 -9 25.71 4.92 -5 -6 -9 42.50 6.83 -5 6 -9 44.45 6.52 5 -6 -9 39.50 6.55 5 -6 -9 40.85 7.10 -5 6 -8 36.87 6.71 5 -6 -8 32.18 6.60 5 -6 -8 26.71 5.13 5 6 -8 40.23 6.82 5 6 -7 95.64 8.53 5 6 -7 93.82 9.79 -5 6 -7 105.81 10.16 5 -6 -7 99.51 10.26 5 -6 -7 122.28 11.26 5 6 -6 7.48 3.07 5 6 -6 5.08 2.14 -5 6 -6 5.32 3.08 5 -6 -6 7.48 3.29 5 -6 -6 9.75 3.55 5 6 -5 11.08 2.85 5 6 -5 10.60 3.82 5 -6 -5 11.51 3.71 -5 6 -5 11.02 3.49 5 -6 -5 13.34 3.77 5 -6 -4 137.71 11.34 5 6 -4 130.17 10.37 -5 6 -4 147.79 11.77 5 -6 -4 143.31 12.36 5 6 -4 129.38 11.46 5 6 -3 30.40 5.59 5 6 -3 32.96 5.42 -5 6 -3 27.73 5.72 5 -6 -3 26.15 4.66 5 -6 -3 29.11 5.40 5 6 -2 70.10 7.85 -5 6 -2 58.29 7.26 5 -6 -2 47.50 7.03 5 6 -2 56.29 7.73 5 -6 -2 67.86 7.95 5 -6 -1 72.62 8.45 5 6 -1 92.35 9.79 5 6 -1 66.89 7.66 -5 6 -1 79.44 9.08 5 -6 -1 88.65 8.80 5 -6 0 78.54 8.82 5 6 0 79.93 9.10 5 6 0 71.18 7.96 -5 6 0 76.15 8.48 5 -6 0 67.97 7.83 5 6 1 91.17 9.31 5 6 1 90.11 9.19 -5 6 1 68.05 8.21 5 -6 1 76.56 8.94 5 -6 1 85.27 8.60 5 6 2 62.56 7.53 5 6 2 63.12 7.80 -5 6 2 69.13 8.30 5 -6 2 74.47 8.70 5 -6 2 71.22 8.24 5 6 3 45.12 6.99 -5 6 3 36.91 6.19 5 -6 3 31.38 5.36 5 6 3 27.87 5.39 5 -6 3 26.30 4.73 5 -6 4 132.33 11.38 5 6 4 126.49 11.52 -5 6 4 138.30 11.84 5 6 4 146.49 11.93 5 -6 4 114.07 10.15 5 6 5 12.21 3.58 5 -6 5 10.31 3.65 5 6 5 13.44 4.37 5 -6 5 10.44 3.37 5 6 6 3.34 2.17 5 -6 6 11.27 3.58 5 6 6 6.92 3.64 5 -6 6 6.21 1.86 5 6 7 87.12 9.53 5 6 7 111.31 10.71 5 -6 7 104.70 9.83 5 -6 7 95.33 10.07 5 -6 8 44.34 6.28 5 6 8 30.43 5.93 5 6 8 40.87 6.88 5 -6 8 43.10 6.35 5 -6 9 34.68 5.72 5 6 9 36.59 6.18 5 6 9 37.57 6.40 5 -6 9 45.85 6.91 5 -6 10 8.32 3.21 5 6 10 8.85 3.81 5 6 10 5.85 2.88 5 -6 10 4.25 2.24 5 6 11 15.07 3.97 5 -6 11 12.22 3.86 5 6 11 13.73 3.88 5 -6 11 8.62 2.74 5 6 12 85.63 9.73 5 6 12 75.35 9.41 5 -6 12 85.79 9.45 5 -6 12 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16.47 4.84 5 -7 -15 10.43 4.16 -5 -7 -14 11.88 3.96 5 -7 -14 29.40 6.78 5 -7 -14 23.32 6.03 5 7 -14 28.35 6.73 5 7 -13 34.04 6.84 -5 -7 -13 15.65 4.61 5 -7 -13 36.86 6.68 5 -7 -13 23.34 5.30 5 7 -12 33.39 6.36 -5 -7 -12 31.62 6.16 5 -7 -12 19.55 5.08 5 -7 -12 27.68 5.78 5 7 -11 110.13 11.76 -5 -7 -11 110.14 11.16 5 -7 -11 131.47 12.86 5 -7 -11 119.18 12.20 -5 7 -10 183.87 14.39 -5 -7 -10 185.82 14.12 5 -7 -10 165.49 14.50 5 -7 -10 174.26 14.71 5 7 -10 165.62 13.91 -5 7 -9 92.26 10.00 5 -7 -9 88.39 10.35 5 -7 -9 110.57 11.36 5 7 -9 90.14 10.52 5 7 -8 115.87 11.44 -5 7 -8 105.78 10.85 5 -7 -8 108.42 11.03 5 -7 -8 95.85 10.68 -5 7 -7 130.02 11.76 5 -7 -7 141.88 12.37 5 -7 -7 131.46 12.50 5 7 -7 122.33 11.82 5 7 -6 62.06 8.77 5 7 -6 48.36 6.77 -5 7 -6 55.05 8.51 5 -7 -6 50.07 8.01 5 -7 -6 44.88 7.11 5 7 -5 128.97 12.12 5 7 -5 105.65 10.30 -5 7 -5 124.09 11.70 5 -7 -5 117.89 11.35 5 -7 -5 112.94 11.34 5 -7 -4 30.74 5.91 5 7 -4 25.22 4.94 5 7 -4 38.70 7.21 -5 7 -4 39.12 6.82 5 -7 -4 35.96 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17 2.30 2.08 6 2 17 -1.15 2.18 6 -2 18 27.43 5.57 6 2 18 26.06 5.24 6 -2 19 0.56 1.11 6 2 19 3.24 1.76 6 -2 20 30.35 5.29 6 2 20 39.24 6.79 6 2 21 9.47 4.56 6 2 22 11.30 4.82 6 2 23 1.33 2.66 6 2 24 80.71 10.34 6 2 25 9.71 3.85 6 -3 -28 -0.75 2.08 6 -3 -27 11.81 3.84 6 -3 -26 24.83 6.26 6 -3 -25 53.39 8.83 6 -3 -24 13.26 4.24 6 -3 -23 4.44 4.20 6 -3 -22 5.36 3.00 6 -3 -21 13.28 4.72 6 -3 -20 36.35 6.54 6 -3 -19 132.39 12.43 6 -3 -18 55.09 7.70 6 -3 -18 62.61 8.91 6 3 -18 78.61 8.95 6 -3 -17 159.74 12.77 6 -3 -17 168.73 13.84 6 3 -17 151.99 12.04 6 -3 -16 56.51 7.59 6 -3 -16 61.81 8.74 6 3 -16 57.69 7.50 6 -3 -15 31.30 5.62 6 3 -15 29.36 5.41 6 -3 -15 26.72 5.07 6 3 -14 172.25 10.64 6 -3 -14 202.81 14.08 6 3 -14 199.53 13.36 6 -3 -13 63.14 8.09 6 3 -13 55.54 5.71 6 3 -13 65.95 7.65 6 -3 -13 70.44 7.96 6 3 -12 70.71 7.81 6 -3 -12 71.85 8.64 6 3 -12 73.27 6.35 6 -3 -12 83.32 8.65 6 3 -11 175.16 12.07 6 3 -11 160.47 9.00 -6 3 -11 160.03 8.56 6 -3 -11 178.08 12.97 6 -3 -11 179.19 12.45 6 -3 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1.57 6 -4 4 1.74 1.10 6 -4 4 2.05 1.04 6 4 4 1.86 1.48 6 -4 5 519.04 21.05 6 4 5 549.96 21.21 6 -4 5 505.56 20.41 6 -4 6 71.80 7.77 6 4 6 74.95 7.83 6 -4 6 82.45 8.29 6 4 6 83.69 8.42 6 -4 7 36.28 5.57 6 4 7 40.44 5.84 6 4 7 26.07 5.16 6 4 8 516.96 20.78 6 -4 8 483.04 20.58 6 4 8 520.01 21.61 6 4 9 124.09 10.27 6 -4 9 123.45 10.24 6 4 9 117.28 10.51 6 4 10 36.69 5.76 6 -4 10 23.76 4.60 6 4 10 32.80 5.55 6 4 11 188.03 12.56 6 4 11 160.78 12.34 6 4 12 384.69 18.27 6 -4 12 388.20 19.04 6 4 12 387.85 19.90 6 4 13 77.21 9.45 6 4 13 84.21 8.63 6 -4 13 93.26 9.16 6 4 14 12.24 3.09 6 -4 14 13.98 3.29 6 4 14 16.13 4.90 6 4 15 51.65 7.02 6 -4 15 36.91 6.24 6 4 15 50.18 7.49 6 4 16 59.70 7.33 6 -4 16 38.94 6.42 6 4 16 55.64 8.38 6 4 17 63.95 8.14 6 -4 17 57.94 7.69 6 4 17 64.46 9.02 6 4 18 228.90 16.66 6 4 19 6.02 2.81 6 4 20 32.72 6.73 6 4 21 42.55 8.15 6 4 22 37.82 8.04 6 4 23 23.67 6.02 6 4 24 59.71 9.34 6 4 25 10.71 4.13 6 4 26 13.75 4.52 6 -5 -26 3.39 1.91 6 -5 -25 30.91 7.02 6 -5 -24 6.01 3.81 6 -5 -23 2.07 2.06 6 -5 -22 16.40 5.56 6 -5 -21 13.48 4.49 6 -5 -21 34.23 7.41 6 -5 -20 3.34 2.53 6 -5 -20 2.34 1.57 6 -5 -19 8.29 3.79 6 -5 -19 -0.39 2.99 6 -5 -18 14.67 5.51 6 -5 -18 4.49 2.17 6 -5 -17 29.45 6.44 6 -5 -17 31.83 6.54 6 5 -16 13.09 3.91 6 -5 -16 11.18 4.20 6 -5 -16 22.88 5.75 6 5 -15 10.35 4.50 6 -5 -15 18.71 4.36 6 -5 -15 13.28 4.45 6 -5 -14 20.06 5.52 6 5 -14 18.41 4.53 6 -5 -14 17.58 4.66 6 5 -13 78.54 8.88 6 -5 -13 84.48 9.89 6 -5 -13 73.27 9.37 6 5 -12 10.35 3.71 6 -5 -12 10.94 3.48 6 -5 -12 8.74 4.03 6 5 -11 2.07 1.07 6 -5 -11 4.76 2.30 6 -5 -11 5.18 2.83 6 -5 -10 9.20 3.04 6 5 -10 9.14 2.95 -6 5 -10 10.81 2.94 6 -5 -10 17.62 4.71 6 5 -9 40.96 6.45 -6 5 -9 33.78 5.14 6 -5 -9 37.16 6.15 6 -5 -9 43.68 6.87 -6 5 -8 35.05 5.59 6 5 -8 19.28 4.45 6 5 -8 23.86 4.25 6 -5 -8 22.24 5.01 6 -5 -8 22.27 5.03 6 5 -7 18.66 4.05 -6 5 -7 20.52 4.44 6 5 -7 18.91 3.92 6 -5 -7 16.19 4.41 6 -5 -7 28.11 5.56 6 -5 -6 8.77 3.32 6 5 -6 11.83 3.17 6 5 -6 6.61 1.36 6 -5 -6 11.76 3.51 -6 5 -6 13.00 3.26 6 -5 -5 37.42 6.08 6 5 -5 41.24 6.46 6 5 -5 45.43 5.55 6 -5 -5 43.15 6.73 6 5 -4 91.40 9.23 6 -5 -4 105.32 9.91 6 -5 -4 95.57 9.68 6 5 -4 104.09 8.68 6 5 -3 84.56 8.90 6 -5 -3 93.05 8.99 6 -5 -3 93.30 9.29 6 5 -3 70.54 7.29 6 5 -2 76.36 8.56 6 -5 -2 79.05 8.67 6 -5 -2 74.95 8.49 6 5 -2 84.91 8.08 6 5 -1 26.52 4.66 6 -5 -1 22.93 5.17 6 5 -1 14.90 3.83 6 -5 -1 19.56 4.24 6 5 0 23.54 4.48 6 -5 0 19.46 4.36 6 5 0 24.10 5.14 6 -5 0 23.77 4.81 6 5 1 26.53 5.05 6 5 1 16.46 4.05 6 -5 1 20.83 4.35 6 5 2 54.70 6.98 6 5 2 88.45 8.80 6 -5 2 76.59 8.22 6 -5 2 76.38 8.67 6 5 3 79.34 8.27 6 5 3 88.69 9.19 6 -5 3 91.93 9.27 6 -5 3 91.92 9.41 6 -5 4 93.72 9.21 6 5 4 101.32 9.55 6 5 4 113.19 10.22 6 -5 4 87.42 8.78 6 -5 5 55.34 7.39 6 5 5 33.94 5.94 6 5 5 47.18 7.10 6 -5 5 54.16 6.90 6 -5 6 5.70 1.91 6 5 6 9.46 2.83 6 5 6 9.93 3.34 6 -5 7 24.54 4.83 6 5 7 23.73 5.06 6 5 7 22.45 5.08 6 -5 7 21.24 4.87 6 -5 8 25.83 4.83 6 5 8 23.85 4.99 6 5 8 24.13 5.05 6 -5 8 28.85 5.72 6 -5 9 31.72 4.90 6 5 9 39.79 5.70 6 5 9 40.60 6.10 6 -5 9 32.61 5.95 6 5 10 17.47 4.29 6 -5 10 5.67 2.03 6 5 10 14.05 3.78 6 5 11 0.11 1.98 6 -5 11 1.04 1.36 6 5 11 -1.17 2.85 6 5 12 10.79 4.29 6 5 12 11.18 2.70 6 -5 12 6.24 2.54 6 5 13 58.23 7.60 6 5 13 87.36 9.73 6 5 14 23.67 4.88 6 -5 14 21.46 5.28 6 5 14 16.58 4.72 6 5 15 17.14 4.43 6 -5 15 17.42 4.95 6 5 15 22.15 4.77 6 5 16 17.23 4.25 6 -5 16 12.01 4.33 6 5 16 11.83 4.52 6 5 17 33.74 6.47 6 5 17 37.68 6.99 6 5 18 18.40 5.82 6 5 19 -0.52 1.80 6 5 20 2.50 1.46 6 5 21 18.33 5.57 6 5 22 32.11 6.35 6 5 23 2.19 3.42 -6 5 23 2.40 2.28 6 5 24 -4.89 3.69 6 5 25 23.58 6.36 6 5 26 14.32 6.11 6 -6 -25 22.56 5.31 6 -6 -24 61.53 9.83 6 -6 -23 9.03 2.63 6 -6 -22 100.16 12.32 6 -6 -21 29.97 7.71 6 -6 -21 29.18 6.85 6 -6 -20 1.89 2.75 6 -6 -20 10.04 4.87 6 -6 -19 20.77 5.38 6 -6 -19 24.77 6.37 6 -6 -18 218.17 16.40 6 -6 -18 169.08 15.57 6 -6 -17 35.28 6.74 6 -6 -17 38.48 7.23 6 6 -16 -0.23 2.08 6 -6 -16 -0.98 2.95 6 -6 -16 1.22 1.79 6 6 -15 11.58 4.03 6 -6 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357.34 19.26 -6 6 -2 319.02 17.79 6 -6 -2 308.30 18.07 6 -6 -2 356.10 18.67 6 6 -1 77.66 8.24 6 -6 -1 75.20 8.33 6 6 -1 66.11 8.12 -6 6 -1 86.08 9.35 6 -6 -1 74.64 8.81 6 6 0 2.59 2.26 6 -6 0 0.59 1.03 6 6 0 5.33 2.10 6 6 1 88.26 9.43 6 6 1 73.01 8.38 6 -6 1 86.00 9.03 6 -6 1 72.58 8.45 6 6 2 352.71 19.00 6 6 2 323.73 17.82 6 -6 2 302.54 17.23 6 -6 2 323.24 18.47 6 -6 3 5.02 3.03 6 6 3 3.74 1.97 6 -6 3 1.21 1.06 6 6 3 5.91 2.96 6 6 4 194.14 14.05 6 6 4 170.80 13.07 6 -6 4 196.39 14.02 6 -6 4 179.03 13.64 6 6 5 65.83 8.42 6 6 5 40.20 6.81 6 -6 5 58.53 7.78 6 -6 5 56.61 7.87 6 -6 6 0.96 1.48 6 6 6 0.13 2.36 6 6 6 1.10 2.62 6 -6 6 0.96 1.86 6 6 7 58.74 7.93 6 6 7 72.40 8.67 6 -6 7 76.25 8.79 6 -6 7 87.26 9.52 6 6 8 394.59 20.59 6 6 8 395.51 20.94 6 -6 8 392.90 19.73 6 -6 8 403.93 20.75 6 6 9 42.38 6.99 6 6 9 41.93 7.06 6 -6 9 36.24 5.87 6 -6 9 39.90 6.66 6 -6 10 1.61 3.13 6 6 10 3.35 2.39 6 6 10 2.27 1.73 6 -6 10 4.02 3.37 6 6 11 28.37 5.90 6 6 11 30.61 6.19 6 -6 11 40.76 6.91 6 -6 11 48.38 7.30 6 6 12 159.90 13.61 6 6 12 156.24 13.51 6 -6 12 149.17 13.12 6 -6 12 141.96 12.90 6 -6 13 13.93 4.19 6 6 13 19.72 4.78 6 6 13 15.29 4.21 6 -6 13 11.34 3.34 6 6 14 1.99 2.82 6 6 14 0.69 1.75 6 -6 14 2.09 2.08 6 6 15 10.80 3.98 6 -6 15 8.28 3.14 6 6 15 14.70 4.82 6 6 16 1.80 2.20 6 6 16 -1.54 2.51 6 6 17 26.18 5.50 6 6 17 31.80 6.65 6 6 18 177.22 15.13 6 6 18 204.56 16.40 -6 6 19 23.32 6.02 6 6 19 23.06 6.15 -6 6 20 -1.68 3.12 6 6 20 -0.69 2.11 6 6 21 36.38 6.75 -6 6 21 46.33 8.75 -6 6 22 82.01 11.94 6 6 22 97.47 12.33 6 6 23 6.94 4.77 -6 6 23 -0.73 3.92 6 6 24 56.27 9.58 6 6 25 18.86 6.42 6 -7 -23 7.65 4.52 6 -7 -22 1.46 4.38 6 -7 -21 40.54 8.12 6 -7 -21 30.87 6.93 6 -7 -20 13.99 4.49 6 -7 -20 28.25 6.77 6 -7 -19 24.83 6.86 6 -7 -19 22.15 6.39 6 -7 -18 52.04 8.77 6 -7 -18 43.87 8.21 6 -7 -17 3.44 2.66 6 -7 -17 5.96 2.96 6 -7 -16 25.75 5.34 6 -7 -16 15.80 4.92 6 7 -15 24.52 5.55 6 -7 -15 15.09 4.49 6 -7 -15 21.26 6.20 6 7 -14 18.80 4.90 6 -7 -14 10.46 4.40 6 -7 -14 9.90 4.76 6 7 -13 36.44 6.83 6 -7 -13 36.88 7.41 6 -7 -13 47.30 8.31 6 7 -12 19.80 4.98 6 -7 -12 18.82 5.12 6 -7 -12 19.08 6.19 6 7 -11 7.32 3.11 6 -7 -11 4.61 3.59 6 -7 -11 9.20 3.21 6 -7 -10 55.72 8.86 6 -7 -10 53.00 8.34 6 7 -10 56.34 8.30 6 7 -9 7.48 3.29 -6 7 -9 2.53 2.46 6 -7 -9 4.72 2.82 6 -7 -9 11.69 4.98 6 7 -8 92.25 10.76 6 -7 -8 90.95 10.44 -6 7 -8 75.80 9.29 6 -7 -8 76.09 10.16 6 7 -7 20.61 5.24 6 -7 -7 27.88 6.17 -6 7 -7 22.16 5.41 6 -7 -7 29.23 6.10 6 7 -6 16.94 4.53 6 7 -6 11.00 3.51 6 -7 -6 9.62 3.16 -6 7 -6 18.98 5.15 6 -7 -6 9.67 2.75 6 7 -5 32.08 6.29 6 7 -5 22.87 4.90 -6 7 -5 39.94 6.70 6 -7 -5 26.93 5.65 6 -7 -5 23.02 5.64 6 7 -4 97.57 9.83 6 7 -4 114.22 11.65 6 -7 -4 103.75 10.84 -6 7 -4 98.37 10.78 6 -7 -4 101.43 11.35 6 7 -3 44.32 7.14 6 7 -3 41.04 6.46 -6 7 -3 38.61 6.44 6 -7 -3 33.59 6.25 6 -7 -3 41.69 7.14 6 7 -2 130.51 11.94 6 7 -2 143.96 12.04 -6 7 -2 169.45 14.00 6 -7 -2 125.95 11.82 6 -7 -2 147.45 13.48 6 -7 -1 30.77 6.06 6 7 -1 22.66 4.91 -6 7 -1 19.36 4.99 6 7 -1 20.14 5.25 6 -7 -1 23.88 5.53 6 -7 0 1.92 1.51 6 7 0 9.37 3.60 -6 7 0 7.17 3.40 6 7 0 6.41 2.96 6 -7 0 2.54 2.83 6 -7 1 15.05 4.12 6 7 1 26.51 5.67 -6 7 1 20.38 5.50 6 7 1 18.52 4.40 6 -7 1 26.45 5.95 6 7 2 153.71 13.26 6 7 2 156.53 12.95 -6 7 2 151.35 13.31 6 -7 2 132.08 11.94 6 -7 2 124.61 12.18 6 7 3 39.79 6.71 6 7 3 39.13 5.72 -6 7 3 49.29 7.54 6 -7 3 28.72 5.50 6 -7 3 45.29 6.98 6 7 4 96.67 10.44 6 7 4 120.19 11.58 -6 7 4 117.99 11.87 6 -7 4 106.14 10.57 6 -7 4 101.63 10.93 6 -7 5 26.18 5.38 6 7 5 19.36 4.40 -6 7 5 28.89 5.94 6 7 5 35.05 6.18 6 -7 5 23.33 5.40 6 -7 6 13.40 4.31 6 7 6 6.13 1.91 6 7 6 9.28 4.29 -6 7 6 8.88 4.92 6 -7 6 1.42 1.71 6 -7 7 14.75 3.94 6 7 7 18.80 5.41 -6 7 7 13.30 4.85 6 7 7 23.93 5.31 6 -7 7 19.27 4.97 6 7 8 78.28 10.04 6 7 8 75.62 9.59 6 -7 8 83.90 9.73 -6 7 8 87.55 10.33 6 -7 8 84.73 10.18 6 -7 9 12.63 3.39 6 7 9 5.15 2.94 6 7 9 13.38 3.78 -6 7 9 3.89 3.67 6 -7 9 4.78 1.70 6 7 10 58.83 8.31 -6 7 10 55.72 8.25 6 7 10 35.05 6.57 6 -7 10 46.23 7.78 6 -7 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10.58 6 -8 -13 57.41 8.45 6 -8 -12 59.94 9.32 6 8 -12 39.20 7.37 6 -8 -12 42.62 7.77 6 8 -11 31.67 6.40 6 -8 -11 29.97 6.24 6 -8 -11 38.58 7.39 6 8 -10 26.75 6.08 6 -8 -10 31.37 7.12 6 -8 -10 18.54 6.22 6 8 -9 18.48 5.31 -6 8 -9 21.32 6.47 6 -8 -9 13.24 3.66 6 -8 -9 30.07 6.34 6 8 -8 119.19 12.06 -6 8 -8 102.36 11.40 6 -8 -8 89.15 10.85 6 -8 -8 98.90 11.65 6 8 -7 60.02 8.76 -6 8 -7 52.97 7.97 6 -8 -7 59.77 8.86 6 -8 -7 48.80 8.54 6 8 -6 14.27 4.52 -6 8 -6 17.11 5.57 6 -8 -6 17.73 4.99 6 -8 -6 11.18 4.19 6 8 -5 31.34 6.41 -6 8 -5 47.26 7.79 6 -8 -5 49.84 7.81 6 -8 -5 44.39 7.71 6 8 -4 64.12 9.79 6 8 -4 59.74 8.36 -6 8 -4 69.89 9.74 6 -8 -4 77.25 10.01 6 -8 -4 66.67 9.91 6 8 -3 2.55 2.77 6 8 -3 -0.05 2.05 -6 8 -3 1.05 2.12 6 -8 -3 0.48 1.79 6 -8 -3 0.76 2.10 6 8 -2 87.30 10.54 6 8 -2 71.08 9.23 6 -8 -2 81.77 10.22 -6 8 -2 81.40 10.41 6 -8 -2 86.52 11.01 6 8 -1 20.46 5.68 -6 8 -1 20.97 5.21 6 8 -1 22.33 5.73 6 -8 -1 19.94 5.01 6 -8 -1 26.40 6.02 6 8 0 2.16 2.52 -6 8 0 3.77 3.24 6 -8 0 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7 -7 -8 308.08 19.26 7 -7 -8 283.56 19.32 -7 7 -7 9.04 3.91 7 7 -7 13.91 4.16 7 -7 -7 11.51 3.71 7 -7 -7 13.41 4.46 7 7 -6 38.62 7.09 -7 7 -6 49.15 7.67 7 -7 -6 46.60 7.78 7 -7 -6 31.16 6.54 7 -7 -5 15.34 4.42 7 7 -5 15.15 4.77 -7 7 -5 23.12 5.49 7 7 -5 12.52 4.00 7 -7 -5 18.99 5.57 7 7 -4 116.98 11.80 7 -7 -4 126.52 12.04 -7 7 -4 102.72 10.96 7 -7 -4 102.38 11.44 7 7 -4 105.76 10.63 7 -7 -3 1.28 2.35 7 7 -3 1.51 1.63 7 7 -3 -0.93 2.35 -7 7 -3 2.52 3.16 7 -7 -3 -0.80 2.16 7 7 -2 143.98 13.22 -7 7 -2 157.24 13.70 7 -7 -2 121.34 12.13 7 -7 -2 150.00 13.62 7 7 -2 145.08 12.69 7 -7 -1 16.48 5.34 7 7 -1 21.86 5.23 7 7 -1 13.89 3.84 -7 7 -1 23.69 5.37 7 -7 -1 23.09 4.98 7 -7 0 1.85 2.58 7 7 0 3.91 1.81 7 7 0 1.47 2.02 -7 7 0 2.23 3.62 7 -7 0 5.45 3.59 7 -7 1 19.73 5.04 7 7 1 26.12 6.08 7 7 1 18.52 4.68 -7 7 1 25.12 5.58 7 -7 1 14.20 4.02 7 7 2 137.69 12.49 7 7 2 149.20 13.28 -7 7 2 126.49 12.10 7 -7 2 127.53 12.30 7 -7 2 146.91 13.43 7 -7 3 3.37 1.45 7 7 3 2.90 3.00 7 7 3 2.27 2.95 -7 7 3 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56.89 5.85 8 3 -8 61.78 7.58 8 -3 -8 57.31 7.40 8 -3 -7 90.87 9.39 8 3 -7 92.39 7.37 8 3 -7 91.62 7.34 8 3 -7 72.76 8.32 8 -3 -7 84.81 8.94 8 -3 -6 23.93 4.97 8 -3 -6 33.18 5.67 8 3 -6 34.89 4.63 8 3 -6 30.74 4.26 8 3 -6 31.68 5.60 8 3 -5 12.21 3.62 8 -3 -5 10.42 3.34 8 3 -5 12.99 3.27 8 -3 -5 18.67 4.31 8 3 -5 14.00 2.83 8 3 -4 -0.02 1.56 8 -3 -4 -0.59 1.86 8 3 -4 0.39 0.92 8 -3 -4 2.91 1.39 8 3 -4 1.08 0.97 8 3 -3 41.15 5.83 8 -3 -3 37.96 5.87 8 3 -3 46.87 5.87 8 -3 -3 39.90 5.88 8 3 -3 41.96 5.19 8 3 -2 49.61 6.45 8 -3 -2 41.04 5.92 8 3 -2 41.91 5.59 8 -3 -2 54.49 6.98 8 3 -2 48.25 5.50 8 3 -1 23.07 4.66 8 3 -1 17.34 3.66 8 -3 -1 11.74 3.15 8 3 0 5.33 2.30 8 -3 0 8.95 2.73 8 -3 0 5.81 1.48 8 3 0 8.49 2.78 8 3 1 17.58 3.81 8 -3 1 23.41 4.42 8 -3 1 21.95 4.34 8 3 1 21.11 4.09 8 3 2 49.45 6.29 8 -3 2 40.77 5.96 8 3 2 39.58 5.45 8 -3 2 52.84 6.80 8 3 3 29.87 5.05 8 -3 3 46.91 6.49 8 3 3 47.43 6.36 8 -3 3 44.65 6.34 8 3 4 -0.07 1.33 8 3 4 1.24 1.24 8 -3 4 0.49 0.95 8 -3 4 -0.62 1.28 8 3 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-19 15.89 5.37 8 -4 -19 -0.78 1.29 8 -4 -18 39.43 7.67 8 -4 -18 25.24 6.10 8 4 -18 31.88 5.80 8 -4 -17 6.50 2.96 8 4 -17 5.35 2.71 8 -4 -16 117.41 12.17 8 4 -16 128.95 12.17 8 -4 -16 104.82 11.54 8 -4 -15 174.85 14.36 8 4 -15 187.41 14.70 8 -4 -14 54.74 8.29 8 -4 -14 59.01 8.49 8 4 -14 70.82 8.83 8 -4 -13 54.08 8.22 8 -4 -13 42.49 6.96 8 4 -13 46.51 6.95 8 4 -12 29.82 5.65 8 -4 -12 30.50 6.13 8 -4 -12 36.81 6.89 8 -4 -11 128.55 11.98 8 -4 -11 116.16 11.32 8 4 -11 117.49 10.89 8 -4 -10 33.66 6.67 8 -4 -10 38.66 6.39 8 4 -10 37.16 6.50 8 4 -9 29.97 5.42 8 -4 -9 29.69 5.87 8 -4 -9 33.39 5.95 8 4 -8 15.76 3.91 8 -4 -8 7.06 3.10 8 4 -8 9.25 2.24 8 -4 -8 12.48 3.66 8 4 -7 122.72 11.01 8 4 -7 116.24 9.02 8 -4 -7 126.32 11.76 8 -4 -7 91.94 9.88 8 4 -6 21.97 4.75 8 -4 -6 22.21 5.09 8 4 -6 19.07 3.68 8 -4 -6 24.80 5.26 8 4 -5 395.04 19.27 8 4 -5 397.34 17.39 8 -4 -5 384.28 19.74 8 4 -5 408.82 14.83 8 -4 -5 384.28 19.56 8 -4 -4 212.08 14.57 8 4 -4 213.65 14.24 8 4 -4 199.94 12.23 8 -4 -4 201.65 14.50 8 4 -4 207.22 10.79 8 -4 -3 66.14 8.07 8 4 -3 63.03 8.06 8 4 -3 57.15 6.65 8 -4 -3 56.80 7.51 8 4 -3 60.70 5.82 8 -4 -2 376.57 19.06 8 4 -2 394.12 19.21 8 4 -2 339.80 16.45 8 4 -1 554.29 22.98 8 -4 -1 585.10 23.88 8 4 -1 594.97 22.08 8 -4 -1 586.66 23.82 8 4 0 82.79 8.98 8 -4 0 68.29 8.31 8 4 0 82.94 8.31 8 -4 0 61.53 7.87 8 4 1 608.74 23.86 8 -4 1 622.06 24.92 8 4 1 576.09 21.95 8 -4 1 634.44 24.94 8 4 2 384.82 18.84 8 -4 2 389.62 19.50 8 4 2 344.45 17.50 8 -4 2 363.66 18.78 8 4 3 61.36 7.81 8 -4 3 53.50 7.30 8 4 3 56.10 7.07 8 -4 3 59.21 7.52 8 4 4 189.93 13.33 8 -4 4 209.70 14.62 8 4 4 219.59 14.37 8 -4 4 207.46 14.17 8 4 5 386.30 18.92 8 -4 5 423.43 20.40 8 4 5 390.75 19.24 8 -4 5 380.29 19.16 8 4 6 22.87 5.29 8 4 6 20.25 4.76 8 -4 6 22.00 4.38 8 4 7 127.80 11.18 8 -4 7 135.24 11.50 8 4 7 121.68 10.94 8 -4 7 126.29 11.31 8 4 8 12.17 4.33 8 4 8 17.25 4.33 8 -4 8 13.02 4.59 8 4 9 35.46 6.51 8 -4 9 27.55 4.95 8 4 9 31.73 6.26 8 4 10 39.73 6.32 8 -4 10 39.62 6.05 8 4 10 37.72 6.13 8 4 11 136.95 11.66 8 -4 11 131.58 11.67 8 4 11 126.18 11.81 8 4 12 48.99 7.33 8 -4 12 44.32 6.55 8 4 12 42.19 7.24 8 4 13 50.14 7.39 8 -4 13 57.13 7.85 8 4 13 44.96 7.62 8 4 14 84.31 9.35 8 -4 14 68.26 9.14 8 4 14 56.26 8.33 8 4 15 194.78 14.21 8 -4 15 187.74 14.89 8 4 15 159.15 14.25 8 4 16 143.56 12.18 8 -4 16 104.81 11.48 8 4 16 118.77 11.97 8 4 17 13.52 4.44 8 -4 17 6.03 3.48 8 4 18 34.68 7.17 8 -4 18 28.44 6.19 8 4 19 12.09 3.61 8 4 20 -1.11 2.48 8 4 21 46.47 8.07 8 4 22 40.61 7.78 8 4 23 2.57 2.30 8 4 24 51.59 9.47 8 4 25 36.89 7.67 8 4 26 -0.50 1.75 8 -5 -25 2.89 1.92 8 -5 -24 5.10 4.15 8 -5 -23 -0.25 2.67 8 -5 -22 0.85 2.26 8 -5 -21 6.93 4.06 8 -5 -20 -0.76 2.02 8 -5 -20 -2.47 2.13 8 -5 -19 14.09 4.92 8 -5 -19 4.12 1.56 8 -5 -18 10.26 5.16 8 -5 -18 10.10 3.95 8 5 -17 15.13 5.09 8 -5 -17 17.00 5.00 8 -5 -17 10.59 4.14 8 -5 -16 50.15 8.03 8 -5 -16 53.24 8.88 8 5 -16 64.75 9.18 8 -5 -15 30.33 6.66 8 -5 -15 41.81 7.83 8 5 -15 46.71 7.71 8 5 -14 27.78 5.96 8 -5 -14 32.30 6.94 8 -5 -14 43.14 7.57 8 5 -13 13.26 4.64 8 -5 -13 15.35 5.47 8 -5 -13 18.52 5.07 8 5 -12 20.17 5.04 8 -5 -12 25.32 5.41 8 -5 -12 20.66 5.19 8 5 -11 12.61 3.68 8 -5 -11 23.45 5.44 8 -5 -11 18.97 5.18 -8 5 -10 -4.25 2.02 8 -5 -10 1.00 1.74 8 5 -10 2.89 2.97 8 -5 -10 -0.31 1.69 8 -5 -9 12.72 4.20 8 5 -9 5.37 2.42 8 -5 -9 11.60 4.44 8 -5 -8 19.31 4.81 8 5 -8 21.42 5.28 8 -5 -8 22.17 5.43 8 5 -7 75.37 8.97 8 5 -7 58.56 6.86 8 -5 -7 82.01 9.67 8 -5 -7 90.50 10.09 8 -5 -6 24.38 4.47 8 5 -6 21.01 4.55 8 -5 -6 15.89 3.71 8 5 -6 26.08 4.32 8 5 -5 13.26 3.31 8 -5 -5 14.70 4.27 8 5 -5 10.91 3.40 8 -5 -5 15.40 4.32 8 5 -4 60.55 8.19 8 5 -4 70.69 7.82 8 -5 -4 69.72 8.55 8 -5 -4 71.61 8.80 8 5 -3 60.45 7.79 8 5 -3 71.78 7.70 8 -5 -3 51.54 7.50 8 -5 -3 52.63 7.43 8 5 -2 35.43 6.23 8 -5 -2 29.19 5.65 8 5 -2 37.02 5.81 8 -5 -2 24.84 5.30 8 5 -1 13.96 3.87 8 -5 -1 20.26 4.31 8 5 -1 22.67 4.39 8 -5 -1 16.98 4.53 8 5 0 29.63 5.20 8 -5 0 31.21 5.52 8 5 0 30.14 5.13 8 -5 0 31.15 5.97 8 5 1 13.29 3.91 8 -5 1 21.23 4.89 8 5 1 28.08 5.22 8 -5 1 15.67 5.03 8 5 2 27.92 5.20 8 -5 2 32.57 5.71 8 5 2 37.09 5.99 8 -5 2 33.78 6.36 8 -5 3 54.16 7.59 8 5 3 50.78 7.28 8 5 3 67.87 8.32 8 -5 3 60.04 8.22 8 -5 4 63.00 8.14 8 5 4 64.19 7.59 8 5 4 59.96 7.49 8 -5 4 66.19 8.55 8 5 5 22.84 4.42 8 -5 5 16.67 4.64 8 5 5 24.52 5.10 8 -5 5 22.95 5.19 8 -5 6 15.36 4.22 8 5 6 21.13 4.88 8 -5 6 16.20 4.67 8 -5 7 62.65 8.63 8 5 7 90.09 9.41 8 -5 7 78.81 9.23 8 5 7 81.67 9.28 8 5 8 25.52 5.62 8 -5 8 22.01 5.10 8 5 8 13.71 4.12 8 -5 8 23.60 5.09 8 5 9 10.08 3.77 8 -5 9 12.25 3.70 8 5 9 6.22 2.80 8 -5 9 10.82 3.77 8 5 10 -0.16 2.01 8 -5 10 -0.85 2.27 8 5 10 -0.71 1.52 8 -5 10 -2.32 2.96 8 5 11 15.97 4.40 8 -5 11 21.97 5.40 8 5 11 17.48 4.53 8 5 12 32.37 6.27 8 -5 12 18.83 5.03 8 5 12 17.37 5.43 8 5 13 11.44 3.43 8 -5 13 14.41 4.75 8 5 13 11.30 4.32 8 5 14 25.73 5.13 8 -5 14 33.97 6.44 8 5 14 35.13 6.90 8 5 15 49.76 7.65 8 -5 15 52.87 8.47 8 5 15 47.55 7.70 8 5 16 36.28 6.66 8 -5 16 44.74 7.59 8 5 16 48.53 7.65 8 5 17 13.14 5.17 8 -5 17 13.50 4.48 8 5 18 3.34 1.91 8 5 19 10.18 4.66 8 5 20 2.68 3.18 8 5 21 2.55 2.60 8 5 22 -0.43 1.91 8 5 23 0.29 2.68 8 5 24 -0.94 2.30 8 5 25 3.12 3.82 8 -6 -23 4.37 2.81 8 -6 -22 10.55 5.00 8 -6 -21 34.91 7.02 8 -6 -21 -0.43 1.05 8 -6 -20 5.82 2.32 8 -6 -20 3.55 2.63 8 -6 -19 24.37 6.18 8 -6 -19 23.40 6.95 8 -6 -18 45.24 8.48 8 -6 -18 51.05 8.50 8 -6 -17 31.30 6.75 8 -6 -17 27.74 6.26 8 6 -17 44.62 8.82 8 6 -16 24.90 6.43 8 -6 -16 21.80 6.36 8 -6 -16 16.95 5.26 8 -6 -15 121.15 12.88 8 -6 -15 95.59 11.81 8 6 -15 143.37 13.59 8 -6 -14 59.88 9.13 8 -6 -14 55.11 8.67 8 6 -14 78.24 10.06 8 -6 -13 3.13 3.01 8 6 -13 1.22 2.08 8 -6 -13 -0.70 2.50 8 6 -12 79.07 10.26 8 -6 -12 88.70 10.49 8 -6 -12 75.40 10.07 8 6 -11 134.94 12.94 8 -6 -11 162.17 14.54 8 -6 -11 142.10 13.45 8 6 -10 20.91 4.86 8 -6 -10 24.41 5.54 8 -6 -10 25.10 5.90 8 6 -9 80.01 9.94 -8 6 -9 77.75 9.33 8 -6 -9 99.00 10.86 8 -6 -9 91.02 10.81 8 6 -8 43.35 6.85 -8 6 -8 42.06 7.03 8 -6 -8 57.87 8.27 8 -6 -8 41.52 7.28 8 -6 -7 18.45 4.93 8 6 -7 30.09 6.23 8 -6 -7 19.74 5.55 -8 6 -7 25.05 5.09 8 6 -6 169.66 13.89 8 6 -6 203.09 14.04 -8 6 -6 188.03 14.11 8 -6 -6 181.72 14.42 8 -6 -6 180.91 15.06 8 6 -5 216.29 14.59 8 -6 -5 231.21 16.47 8 -6 -5 216.93 16.18 8 -6 -4 28.68 6.10 8 6 -4 15.06 3.91 8 -6 -4 19.81 5.37 8 6 -4 20.84 4.64 8 6 -3 61.04 8.29 8 6 -3 60.19 7.77 8 -6 -3 64.85 8.63 8 -6 -3 53.70 8.25 8 6 -2 65.52 8.73 8 6 -2 73.35 8.61 8 -6 -2 73.48 9.21 8 -6 -2 53.48 7.92 8 6 -1 82.97 9.70 8 -6 -1 93.48 10.07 8 6 -1 98.64 9.84 8 -6 -1 88.47 10.59 8 6 0 112.77 11.13 8 -6 0 111.90 11.65 8 6 0 87.02 9.51 8 -6 0 90.01 9.82 8 6 1 82.39 10.22 8 -6 1 99.56 10.85 8 -6 1 94.65 10.36 8 6 2 100.78 10.67 8 -6 2 78.96 9.59 8 6 2 84.91 9.67 8 -6 2 73.95 9.05 8 6 3 60.39 8.31 8 -6 3 61.81 8.46 8 6 3 65.06 8.40 8 -6 3 72.72 9.22 8 -6 4 17.89 4.29 8 6 4 16.23 4.94 8 6 4 21.06 5.08 8 -6 4 19.46 4.23 8 6 5 257.55 16.98 8 -6 5 228.14 16.65 8 6 5 223.35 15.73 8 -6 5 231.89 16.44 8 -6 6 200.59 15.24 8 6 6 209.57 15.41 8 -6 6 178.42 15.09 8 6 6 195.91 14.79 8 -6 7 32.04 6.33 8 6 7 32.14 6.31 8 6 7 28.82 6.04 8 -6 7 24.53 5.50 8 -6 8 76.06 9.53 8 6 8 48.51 7.61 8 -6 8 63.15 9.21 8 -6 9 87.82 10.59 8 6 9 107.22 11.08 8 -6 9 86.38 10.24 8 6 9 95.80 10.69 8 6 10 29.74 6.32 8 -6 10 25.42 5.40 8 6 10 22.34 5.54 8 -6 10 23.97 5.95 8 -6 11 152.91 13.79 8 6 11 149.53 13.20 8 -6 11 145.18 13.77 8 6 11 153.41 13.62 8 -6 12 77.63 9.99 8 6 12 87.23 9.99 8 -6 12 68.51 10.11 8 6 12 95.50 10.87 8 6 13 2.01 2.36 8 -6 13 1.20 2.81 8 6 13 -0.95 3.08 8 -6 13 4.52 3.11 8 -6 14 58.09 9.30 8 6 14 58.30 8.23 8 6 14 48.02 7.85 8 -6 14 60.02 8.07 8 -6 15 103.68 12.05 8 6 15 120.10 12.20 8 6 15 99.89 11.47 8 6 16 27.51 6.01 8 -6 16 14.51 4.81 8 6 16 31.41 6.66 8 6 17 32.69 6.78 8 6 17 37.14 7.29 8 6 18 47.14 8.22 8 6 19 11.35 4.32 8 6 20 9.72 5.24 8 6 21 31.16 7.29 8 6 22 15.63 5.49 8 6 23 3.44 2.65 -8 6 23 3.27 3.89 8 -7 -21 7.63 4.08 8 -7 -21 0.97 3.06 8 -7 -20 9.50 3.78 8 -7 -20 4.28 2.80 8 -7 -19 4.89 2.03 8 -7 -19 0.12 3.63 8 -7 -18 8.48 3.79 8 -7 -18 5.30 2.06 8 -7 -17 9.14 4.77 8 -7 -17 0.26 3.89 8 7 -16 -0.85 2.93 8 -7 -16 -0.71 2.72 8 -7 -16 7.12 3.58 8 7 -15 1.21 2.64 8 -7 -15 -1.08 1.67 8 7 -14 0.40 3.21 8 -7 -14 4.50 2.02 8 -7 -14 -0.69 1.55 8 7 -13 5.65 3.94 8 -7 -13 7.78 4.23 8 -7 -13 9.89 3.40 8 7 -12 21.17 5.47 8 -7 -12 45.18 7.93 8 -7 -12 34.69 7.16 8 7 -11 47.42 8.42 8 -7 -11 44.10 7.77 8 -7 -11 53.89 8.65 8 7 -10 37.03 7.41 8 -7 -10 37.83 7.64 8 -7 -10 30.95 6.78 8 7 -9 0.38 1.80 8 -7 -9 1.41 2.24 8 -7 -9 1.58 1.32 8 7 -8 66.62 9.24 -8 7 -8 52.14 8.02 8 -7 -8 58.15 9.12 8 -7 -8 43.38 7.91 8 7 -7 56.63 8.63 8 -7 -7 47.13 8.03 -8 7 -7 34.47 6.55 8 -7 -7 55.08 8.11 8 7 -6 17.85 4.42 -8 7 -6 15.95 4.89 8 -7 -6 27.39 5.86 8 -7 -6 13.56 3.51 8 7 -5 73.33 9.72 8 -7 -5 79.61 10.34 -8 7 -5 86.19 10.42 8 -7 -5 77.12 10.09 8 7 -4 38.18 6.50 -8 7 -4 41.03 7.00 8 7 -4 30.47 5.66 8 -7 -4 35.08 6.53 8 -7 -4 34.26 7.03 8 7 -3 62.53 9.32 -8 7 -3 37.45 7.07 8 -7 -3 42.71 7.34 8 7 -3 42.79 6.79 8 -7 -3 45.64 8.24 8 -7 -2 32.53 6.70 8 7 -2 42.24 7.27 -8 7 -2 35.60 6.77 8 -7 -2 36.11 6.99 8 7 -2 35.15 6.54 8 7 -1 82.40 10.11 -8 7 -1 72.08 9.41 8 -7 -1 62.03 8.93 8 -7 -1 52.22 8.78 8 7 0 110.60 11.43 8 -7 0 125.24 12.09 8 7 0 91.39 10.27 8 -7 0 111.36 11.61 8 7 1 81.43 9.96 8 -7 1 59.73 8.73 8 7 1 73.55 9.09 8 -7 1 75.45 10.60 8 7 2 31.61 6.33 8 -7 2 38.20 7.64 8 7 2 25.97 5.93 8 -7 2 42.19 7.51 8 7 3 52.30 7.95 8 -7 3 53.91 8.06 8 7 3 37.77 7.08 8 -7 3 48.52 8.03 8 -7 4 34.47 6.96 8 7 4 30.61 6.36 8 -7 4 32.92 6.12 8 7 4 27.96 5.59 8 7 5 72.82 9.27 8 -7 5 70.26 9.61 8 7 5 86.06 9.94 8 -7 5 67.19 9.46 8 -7 6 23.44 6.13 8 7 6 17.99 4.86 8 -7 6 13.11 4.86 8 7 6 19.23 4.82 8 7 7 49.08 8.14 8 -7 7 37.66 7.17 8 7 7 42.62 7.73 8 -7 7 47.38 7.90 8 -7 8 34.54 7.28 8 7 8 57.46 9.11 8 -7 8 43.23 7.75 8 7 8 58.54 8.65 8 -7 9 2.11 2.07 8 7 9 -0.55 2.31 8 -7 9 -0.23 2.47 8 7 9 2.83 3.22 8 -7 10 28.23 6.23 8 7 10 25.12 5.84 8 -7 10 34.69 7.46 8 7 10 22.32 5.41 8 7 11 60.29 8.97 8 -7 11 40.45 7.64 8 7 11 61.38 9.11 8 -7 11 57.06 8.41 8 7 12 42.12 8.05 8 7 12 59.10 9.06 8 -7 13 11.32 4.70 8 7 13 5.29 4.66 8 7 13 10.78 4.08 8 -7 14 4.59 2.84 8 7 14 4.31 3.03 8 7 14 -0.40 1.88 8 7 15 -2.89 2.80 8 7 15 -0.74 2.78 8 7 16 5.20 5.09 8 7 16 3.46 3.03 8 7 17 0.27 2.71 8 7 17 0.86 2.57 8 7 18 5.96 3.39 -8 7 18 10.97 4.56 8 7 19 4.33 3.73 -8 7 19 2.95 4.04 -8 7 20 3.44 3.35 8 7 20 7.01 3.84 8 7 21 0.53 2.93 -8 7 21 8.24 3.71 8 -8 -19 11.53 5.07 8 -8 -19 5.48 3.12 8 -8 -18 20.10 5.14 8 -8 -18 40.68 8.49 8 -8 -17 78.53 10.23 8 -8 -17 51.19 8.94 8 -8 -16 1.42 3.83 8 -8 -16 6.19 4.03 8 8 -15 20.13 6.40 8 -8 -15 25.38 5.93 8 -8 -15 23.90 6.68 8 -8 -14 13.28 5.65 8 8 -14 12.70 5.09 8 -8 -14 19.36 5.30 8 8 -13 5.93 3.37 8 -8 -13 7.77 3.46 8 -8 -13 2.93 3.01 8 8 -12 51.71 8.34 8 -8 -12 55.54 9.38 8 -8 -12 61.73 9.89 8 8 -11 95.13 11.50 8 -8 -11 105.99 12.16 8 -8 -11 116.43 13.12 8 8 -10 7.71 4.04 8 -8 -10 10.39 5.29 8 -8 -10 4.58 2.87 8 8 -9 57.90 8.97 8 -8 -9 60.39 10.03 8 -8 -9 46.41 7.94 8 8 -8 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5.51 9 -10 5 9.98 4.85 9 10 6 118.18 13.47 -9 10 6 83.98 11.68 9 -10 6 80.52 11.94 9 10 7 9.90 4.06 -9 10 7 3.94 4.19 9 10 7 6.40 4.08 9 -10 7 18.89 7.11 9 10 8 55.31 9.25 -9 10 8 43.38 8.50 9 10 8 47.42 8.52 9 -10 8 54.70 10.41 10 0 -25 10.41 4.37 10 0 -24 54.26 9.04 10 0 -23 118.29 12.99 10 0 -22 38.79 7.25 10 0 -21 170.57 15.27 10 0 -20 55.68 9.27 10 0 -19 65.46 9.03 10 0 -18 193.58 15.39 10 0 -17 265.22 18.45 10 0 -16 71.46 10.05 10 0 -15 275.37 18.16 10 0 -14 132.47 12.30 10 0 -13 194.86 14.42 10 0 -12 277.41 15.75 10 0 -12 269.47 16.95 10 0 -11 275.76 15.57 10 0 -11 299.85 17.86 10 0 -10 82.19 8.37 10 0 -10 89.14 9.64 10 0 -9 217.72 13.63 10 0 -9 239.67 15.45 10 0 -8 224.09 13.64 10 0 -8 231.30 14.96 10 0 -7 122.38 10.09 10 0 -7 123.91 10.93 10 0 -7 120.68 10.64 10 0 -6 49.38 6.23 10 0 -6 49.91 7.57 10 0 -6 49.22 7.07 10 0 -5 235.13 13.97 10 0 -5 243.95 15.44 10 0 -5 234.92 14.62 10 0 -4 290.51 15.45 10 0 -4 291.91 16.13 10 0 -3 220.12 13.64 10 0 -3 238.93 14.86 10 0 -3 265.08 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226.83 14.27 10 2 6 70.76 8.30 10 -2 6 65.41 8.14 10 2 6 68.76 8.04 10 2 7 93.77 9.58 10 -2 7 100.58 9.99 10 2 7 82.34 8.52 10 2 8 210.49 14.70 10 -2 8 189.44 13.88 10 2 8 194.58 13.00 10 2 9 164.82 13.23 10 -2 9 176.00 13.72 10 2 9 180.38 12.60 10 2 10 107.12 10.51 10 -2 10 98.88 10.23 10 2 10 85.66 8.79 10 2 11 385.40 20.69 10 -2 11 381.97 20.50 10 2 11 401.27 18.99 10 2 12 199.13 15.13 10 -2 12 199.28 14.85 10 2 12 203.53 13.45 10 2 13 75.95 9.09 10 -2 13 83.79 9.58 10 2 13 82.66 8.70 10 2 14 104.35 11.11 10 -2 14 102.81 10.89 10 2 14 123.36 10.71 10 2 15 159.09 13.87 10 -2 15 169.34 14.58 10 2 16 57.22 8.41 10 -2 16 41.15 7.44 10 2 17 131.26 13.14 10 -2 17 132.04 13.12 10 2 18 117.79 12.36 10 -2 18 97.69 11.58 10 2 19 40.66 7.97 10 -2 19 50.71 7.47 10 2 20 24.58 6.64 10 -2 20 12.03 4.48 10 2 21 64.90 9.91 10 -2 21 53.05 9.30 10 2 22 37.65 7.97 10 -2 22 32.13 7.81 10 2 23 11.07 3.44 10 2 24 32.22 7.57 10 2 25 18.56 5.85 10 2 26 10.89 6.36 10 -3 -26 6.26 4.22 10 -3 -25 -2.29 1.89 10 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11.09 3.42 10 3 -5 5.63 3.51 10 3 -5 2.62 1.05 10 -3 -5 5.35 2.47 10 -3 -5 1.36 1.40 10 3 -5 3.68 2.54 10 3 -4 16.63 4.37 10 3 -4 21.36 4.53 10 -3 -4 17.66 4.26 10 -3 -4 21.58 5.42 10 3 -4 20.23 4.15 10 3 -3 1.24 1.18 10 -3 -3 4.44 2.21 10 3 -3 3.09 1.73 10 -3 -3 2.27 1.37 10 3 -3 -0.47 1.16 10 3 -2 9.18 2.96 10 -3 -2 12.64 3.74 10 3 -2 12.45 4.12 10 -3 -2 5.20 3.52 10 3 -2 3.17 1.89 10 3 -1 16.93 4.16 10 -3 -1 16.73 3.67 10 3 -1 15.91 4.18 10 -3 -1 21.05 5.05 10 3 -1 19.71 4.23 10 3 0 12.41 4.34 10 -3 0 4.14 1.88 10 3 0 6.09 2.47 10 -3 0 8.15 2.50 10 3 1 17.54 4.70 10 -3 1 16.03 3.87 10 3 1 15.52 3.82 10 -3 1 22.55 5.21 10 3 2 8.42 2.75 10 -3 2 12.20 3.47 10 3 2 5.78 3.13 10 -3 2 5.05 3.42 10 3 3 2.15 2.41 10 -3 3 4.18 3.33 10 3 3 0.37 1.76 10 -3 3 0.23 2.37 10 3 4 24.25 4.87 10 -3 4 27.19 5.25 10 3 4 11.87 3.66 10 -3 4 20.70 4.33 10 3 5 -0.99 1.77 10 -3 5 1.74 2.02 10 3 5 -1.78 2.64 10 -3 5 1.66 2.71 10 3 6 18.16 4.50 10 -3 6 7.29 2.70 10 3 6 21.75 4.96 10 -3 6 17.32 4.38 10 3 7 33.23 5.89 10 -3 7 31.47 5.80 10 3 7 29.61 5.70 10 3 8 0.69 2.04 10 -3 8 2.22 2.12 10 3 8 5.26 2.36 10 3 9 10.39 3.76 10 -3 9 10.08 2.78 10 3 9 9.39 3.94 10 3 10 31.46 5.72 10 -3 10 22.17 5.03 10 3 10 28.02 5.45 10 3 11 5.26 3.39 10 -3 11 0.69 1.46 10 3 11 2.20 1.66 10 3 12 7.19 3.86 10 -3 12 14.53 4.09 10 3 12 7.80 4.42 10 3 13 15.45 3.76 10 -3 13 15.24 4.16 10 3 13 11.03 3.41 10 3 14 -1.93 2.61 10 -3 14 0.63 2.59 10 3 14 2.15 1.92 10 -3 15 -0.14 2.83 10 3 15 -2.12 2.08 10 -3 16 8.80 3.33 10 3 16 7.91 3.41 10 -3 17 1.91 3.01 10 3 17 -1.22 1.68 10 -3 18 4.62 2.97 10 3 18 -0.94 2.96 10 3 19 0.30 2.40 10 -3 19 -0.54 2.93 10 3 20 4.63 1.94 10 -3 20 -1.31 2.97 10 3 21 -0.35 1.84 10 3 22 1.65 2.33 10 3 23 7.42 2.16 10 3 24 4.56 2.56 10 3 25 -3.21 3.84 10 3 26 2.78 3.30 10 -4 -25 32.31 7.87 10 -4 -24 38.37 7.48 10 -4 -23 8.38 3.58 10 -4 -22 36.03 7.67 10 -4 -21 31.19 7.05 10 -4 -20 16.46 4.91 10 -4 -19 37.30 7.86 10 4 -19 26.25 6.47 10 -4 -18 81.57 10.81 10 4 -18 96.33 11.48 10 -4 -17 80.89 10.71 10 -4 -17 50.33 8.69 10 4 -17 67.97 9.43 10 -4 -16 45.45 7.85 10 -4 -16 34.94 7.01 10 4 -16 27.26 6.74 10 -4 -15 106.41 12.04 10 -4 -15 84.28 10.48 10 4 -15 88.36 10.61 10 -4 -14 75.58 10.06 10 -4 -14 92.44 11.01 10 4 -14 82.84 9.66 10 -4 -13 67.59 9.32 10 -4 -13 58.16 8.85 10 4 -13 69.55 9.36 10 -4 -12 107.92 11.60 10 -4 -12 103.30 11.01 10 4 -12 135.51 12.99 10 -4 -11 245.57 17.29 10 -4 -11 224.21 16.30 10 4 -11 243.82 16.85 10 -4 -10 84.26 10.15 10 -4 -10 82.13 9.60 10 4 -10 68.61 9.20 10 -4 -9 75.84 9.58 10 -4 -9 71.20 9.08 10 4 -9 88.52 9.74 10 -4 -8 109.99 11.44 10 4 -8 118.49 11.39 10 -4 -7 28.65 6.63 10 4 -7 36.03 5.32 10 4 -7 33.48 6.20 10 -4 -7 49.84 7.71 10 -4 -6 38.51 6.98 10 -4 -6 43.67 7.37 10 4 -6 36.14 5.49 10 4 -6 50.87 7.41 10 -4 -5 184.93 14.67 10 -4 -5 179.04 14.52 10 4 -5 167.14 12.31 10 4 -5 185.65 14.20 10 4 -4 57.15 7.74 10 -4 -4 59.70 7.79 10 4 -4 63.34 7.48 10 -4 -4 74.84 9.55 10 4 -3 70.64 8.88 10 -4 -3 79.17 9.12 10 4 -3 77.41 8.39 10 -4 -3 71.32 8.83 10 4 -3 48.45 6.87 10 4 -2 266.93 16.55 10 -4 -2 262.05 17.10 10 4 -2 234.08 14.97 10 -4 -2 224.38 15.90 10 4 -2 230.87 13.80 10 4 -1 239.65 15.82 10 -4 -1 259.91 17.11 10 4 -1 222.36 15.11 10 -4 -1 205.16 15.56 10 4 0 166.67 13.00 10 -4 0 133.12 12.13 10 4 0 139.30 11.80 10 -4 0 146.19 13.13 10 4 1 257.75 16.47 10 -4 1 249.06 16.46 10 4 1 255.02 16.09 10 -4 1 258.15 17.17 10 4 2 236.44 15.64 10 -4 2 253.28 16.84 10 4 2 251.16 15.83 10 -4 2 239.74 16.38 10 4 3 72.72 8.94 10 -4 3 59.96 8.19 10 4 3 64.10 8.13 10 -4 3 70.58 8.53 10 4 4 65.01 7.73 10 -4 4 74.55 9.12 10 4 4 72.79 8.88 10 -4 4 66.91 8.25 10 4 5 173.67 13.67 10 -4 5 150.70 12.79 10 4 5 179.26 14.05 10 -4 5 183.32 14.31 10 4 6 34.52 6.15 10 -4 6 36.03 6.69 10 4 6 41.50 6.83 10 -4 6 37.89 6.32 10 4 7 29.47 6.15 10 -4 7 30.15 6.38 10 -4 7 22.64 5.06 10 4 7 24.93 5.49 10 4 8 127.60 11.67 10 -4 8 114.53 11.56 10 4 8 129.75 11.90 10 -4 8 115.26 11.68 10 4 9 96.60 10.11 10 -4 9 86.09 10.04 10 4 9 89.63 9.88 10 4 10 81.94 9.34 10 -4 10 79.15 9.96 10 4 10 68.28 8.88 10 4 11 231.80 16.02 10 -4 11 253.87 17.27 10 4 11 260.47 17.54 10 4 12 104.83 11.22 10 -4 12 105.29 11.15 10 4 12 96.68 10.95 10 -4 13 61.34 8.86 10 4 13 76.37 9.70 10 4 14 91.98 10.34 10 -4 14 95.60 11.13 10 4 14 104.89 11.61 10 4 15 119.94 11.99 10 -4 15 108.56 11.77 10 4 15 100.97 11.17 10 -4 16 52.64 8.66 10 4 16 52.57 8.40 10 4 17 55.05 8.77 10 -4 17 78.26 10.26 10 4 18 76.62 10.42 10 -4 18 83.49 10.69 10 -4 19 31.73 7.51 10 4 19 43.47 8.15 10 4 20 10.98 4.82 10 4 21 18.35 4.92 10 4 22 9.59 4.18 10 4 23 2.49 2.42 10 4 24 38.97 8.29 10 4 25 30.09 7.73 10 -5 -23 1.59 2.08 10 -5 -22 8.74 4.21 10 -5 -21 9.45 4.26 10 -5 -20 3.20 1.77 10 -5 -19 7.48 4.49 10 -5 -18 1.12 2.38 10 -5 -18 0.53 2.65 10 5 -18 6.17 3.79 10 5 -17 -1.60 3.29 10 -5 -17 -2.87 3.14 10 -5 -17 -1.14 2.07 10 5 -16 8.96 3.10 10 -5 -16 12.27 4.98 10 -5 -16 13.34 4.22 10 5 -15 23.49 6.39 10 -5 -15 12.81 4.47 10 -5 -15 25.87 6.33 10 5 -14 6.28 4.16 10 -5 -14 0.31 2.87 10 -5 -14 2.04 2.99 10 5 -13 0.37 1.86 10 -5 -13 2.07 3.60 10 -5 -13 -1.17 1.64 10 -5 -12 1.72 1.83 10 5 -12 4.57 3.15 10 -5 -12 0.98 1.71 10 -5 -11 8.91 3.55 10 5 -11 9.65 3.59 10 -5 -11 4.17 1.77 10 -5 -10 20.36 5.16 10 5 -10 19.60 5.01 10 -5 -10 19.36 5.00 10 -5 -9 2.22 1.69 10 5 -9 8.15 3.54 10 -5 -9 3.95 3.48 10 5 -8 26.79 5.96 10 -5 -8 42.53 6.74 10 -5 -8 38.30 6.79 10 5 -7 12.06 3.48 10 -5 -7 8.70 3.91 10 -5 -7 19.48 5.48 10 5 -6 2.61 2.61 10 -5 -6 6.34 4.27 10 5 -6 4.24 1.95 10 -5 -6 5.47 3.65 10 5 -5 14.72 4.21 10 -5 -5 14.01 4.19 10 5 -5 9.46 3.28 10 -5 -5 6.29 3.49 10 5 -4 31.61 5.63 10 -5 -4 24.41 5.51 10 5 -4 33.06 6.11 10 -5 -4 27.66 6.19 10 5 -3 17.44 5.48 10 -5 -3 13.35 4.23 10 -5 -3 12.46 4.32 10 5 -3 17.62 4.47 10 -5 -2 39.41 7.25 10 5 -2 44.24 7.18 10 5 -2 37.07 6.00 10 -5 -2 37.72 7.19 10 -5 -1 109.88 11.32 10 5 -1 147.81 12.90 10 5 -1 132.93 11.71 10 -5 -1 134.72 12.73 10 -5 0 109.04 11.39 10 5 0 131.94 12.13 10 5 0 121.39 11.22 10 -5 0 100.23 11.23 10 5 1 108.36 10.93 10 -5 1 121.03 12.17 10 5 1 120.96 10.95 10 -5 1 126.66 12.68 10 5 2 53.60 7.91 10 -5 2 38.43 6.89 10 5 2 47.66 7.11 10 -5 2 64.55 9.16 10 5 3 15.29 4.16 10 5 3 8.78 3.48 10 -5 3 17.31 5.08 10 -5 3 15.94 5.02 10 -5 4 41.96 7.70 10 5 4 31.87 6.76 10 5 4 39.89 6.49 10 -5 4 36.68 6.10 10 5 5 10.56 4.00 10 5 5 12.84 4.03 10 -5 5 9.31 2.93 10 -5 5 12.50 4.64 10 5 6 6.56 2.71 10 5 6 2.03 1.70 10 -5 6 1.93 2.14 10 5 7 15.12 3.76 10 5 7 24.22 5.89 10 -5 7 19.22 4.92 10 -5 7 30.70 5.70 10 5 8 39.91 7.40 10 5 8 34.77 6.37 10 -5 8 25.27 5.55 10 -5 8 28.82 6.16 10 5 9 7.55 2.54 10 5 9 5.94 2.79 10 -5 9 4.59 2.75 10 5 10 19.34 5.26 10 5 10 32.93 6.80 10 -5 10 17.21 4.51 10 -5 10 26.13 5.94 10 5 11 9.39 3.42 10 5 11 7.13 3.46 10 -5 11 9.80 4.10 10 -5 11 9.32 4.23 10 5 12 1.59 2.01 10 5 12 3.59 3.57 10 -5 12 0.18 2.49 10 -5 12 1.68 4.46 10 5 13 2.25 3.92 10 5 13 -2.62 2.77 10 -5 13 3.99 3.68 10 5 14 3.66 2.82 10 5 14 1.86 2.74 10 -5 14 3.57 3.47 10 5 15 17.43 5.35 10 5 15 19.85 5.83 10 -5 15 21.15 5.39 10 5 16 20.30 5.72 10 -5 16 12.29 4.12 10 5 17 1.22 2.55 10 -5 17 3.04 3.08 10 -5 18 0.68 3.25 10 5 18 8.83 4.89 10 5 19 0.46 3.06 10 5 20 3.16 2.55 10 5 21 9.86 4.66 10 5 22 8.75 4.87 10 5 23 1.99 2.02 10 -6 -22 25.53 6.45 10 -6 -21 74.71 10.67 10 -6 -20 37.65 7.69 10 -6 -19 16.64 6.02 10 -6 -19 13.34 5.17 10 -6 -18 49.63 8.46 10 -6 -18 27.12 6.38 10 6 -17 45.14 8.07 10 -6 -17 54.77 8.51 10 -6 -17 41.19 7.83 10 -6 -16 46.13 8.66 10 -6 -16 53.46 9.00 10 6 -16 62.31 10.13 10 -6 -15 133.28 14.50 10 -6 -15 148.92 14.86 10 6 -15 111.55 12.57 10 -6 -14 80.78 11.70 10 -6 -14 64.49 9.58 10 6 -14 73.06 10.16 10 -6 -13 34.72 7.14 10 -6 -13 54.31 8.92 10 6 -13 65.61 9.58 10 -6 -12 56.16 9.05 10 -6 -12 57.88 9.21 10 6 -12 63.85 9.61 10 -6 -11 73.06 9.98 10 -6 -11 46.66 7.87 10 6 -11 61.05 9.48 10 -6 -10 41.45 7.66 10 -6 -10 42.63 7.73 10 6 -10 51.37 8.43 10 6 -9 70.36 9.28 10 -6 -9 86.38 10.42 10 -6 -9 68.45 10.01 10 -6 -8 88.42 10.85 10 -6 -8 73.98 9.88 10 -6 -7 17.86 5.55 10 6 -7 20.09 5.53 10 -6 -7 12.79 4.70 10 6 -6 39.64 6.70 10 -6 -6 35.22 6.72 10 -6 -6 44.16 7.85 10 6 -5 107.52 11.46 10 6 -5 109.51 11.01 10 -6 -5 91.02 11.27 10 -6 -5 106.88 11.76 10 6 -4 67.53 8.77 10 6 -4 68.20 8.39 10 -6 -4 69.85 9.37 10 -6 -4 76.95 9.68 10 -6 -3 8.67 4.57 10 6 -3 5.47 3.82 10 -6 -3 1.44 2.33 10 6 -3 5.02 2.73 10 6 -2 44.14 7.65 10 6 -2 44.66 7.53 10 -6 -2 36.76 7.61 10 -6 -2 46.62 8.27 10 6 -1 116.43 11.96 10 6 -1 97.37 10.41 10 -6 -1 114.06 12.30 10 -6 -1 86.06 10.45 10 6 0 138.82 12.84 10 6 0 110.15 11.84 10 -6 0 123.41 12.41 10 -6 0 124.25 12.71 10 6 1 90.32 10.51 10 6 1 108.93 11.34 10 -6 1 118.94 12.05 10 -6 1 86.32 9.96 10 -6 2 52.62 8.41 10 6 2 56.40 8.52 10 6 2 46.66 7.55 10 -6 2 37.60 6.97 10 6 3 6.64 3.41 10 6 3 7.74 3.25 10 -6 3 2.63 2.54 10 -6 3 3.19 2.70 10 -6 4 61.03 9.02 10 6 4 63.37 8.78 10 6 4 51.74 8.10 10 -6 5 105.60 11.53 10 6 5 78.44 10.26 10 6 5 107.60 11.74 10 -6 5 104.65 11.61 10 6 6 30.40 5.99 10 -6 6 23.02 5.33 10 6 6 32.35 6.68 10 -6 6 34.60 6.93 10 6 7 17.62 4.38 10 -6 7 18.07 4.70 10 6 7 19.03 5.35 10 -6 7 13.99 4.91 10 -6 8 77.72 9.96 10 6 8 58.86 8.75 10 6 8 85.80 10.16 10 -6 8 75.28 10.32 10 -6 9 75.49 10.25 10 6 9 73.20 9.90 10 6 9 65.15 9.13 10 -6 9 70.06 9.87 10 6 10 43.39 7.68 10 -6 10 32.64 7.24 10 6 10 51.57 8.41 10 -6 10 41.35 7.94 10 -6 11 51.73 8.58 10 6 11 49.39 7.61 10 6 11 68.61 9.71 10 -6 11 53.80 9.34 10 6 12 38.72 6.97 10 -6 12 51.98 8.32 10 -6 12 35.55 6.81 10 -6 13 46.78 8.95 10 6 13 46.76 8.02 10 6 13 59.80 8.68 10 -6 13 46.29 8.60 10 6 14 78.14 10.52 10 -6 14 75.39 10.54 10 6 14 98.61 11.33 10 -6 14 65.83 9.45 10 6 15 127.73 13.11 10 -6 15 124.70 13.75 10 6 15 140.44 14.16 10 -6 15 139.68 15.22 10 6 16 48.64 8.13 10 -6 16 39.04 8.43 10 6 16 63.07 9.80 10 -6 16 49.34 9.30 10 6 17 45.02 8.05 10 6 18 47.77 8.33 10 6 19 17.58 4.87 10 6 20 37.11 7.89 10 6 21 64.62 9.73 10 6 22 20.55 6.80 10 -7 -19 2.18 2.03 10 -7 -19 7.34 3.78 10 -7 -18 12.06 4.21 10 -7 -18 5.79 4.12 10 -7 -17 3.08 2.29 10 -7 -17 3.63 2.56 10 7 -16 17.53 4.90 10 -7 -16 20.72 5.45 10 -7 -16 9.15 3.84 10 7 -15 3.14 2.67 10 -7 -15 10.16 4.08 10 -7 -15 8.18 3.27 10 7 -14 13.07 4.39 10 -7 -14 9.82 4.01 10 -7 -14 16.71 4.86 10 7 -13 12.23 4.65 10 -7 -13 7.97 3.92 10 -7 -13 8.89 5.59 10 7 -12 3.90 2.41 10 -7 -12 7.75 4.36 10 -7 -12 0.64 2.25 10 7 -11 26.87 5.89 10 -7 -11 30.17 6.45 10 -7 -11 28.44 6.34 10 7 -10 35.50 7.44 10 -7 -10 26.02 6.20 10 -7 -10 32.66 6.98 10 7 -9 19.55 6.05 10 -7 -9 24.59 5.59 10 -7 -9 39.51 7.69 10 -7 -8 24.51 6.28 10 7 -8 27.25 7.04 10 -7 -8 15.71 3.98 10 -7 -7 1.36 3.96 10 7 -7 -1.03 2.06 -10 7 -7 4.36 1.78 10 -7 -7 -0.26 2.03 10 -7 -6 8.85 4.06 10 7 -6 9.29 3.80 -10 7 -6 1.16 1.45 10 -7 -6 7.37 3.57 10 -7 -5 4.03 3.95 10 7 -5 6.77 3.38 -10 7 -5 10.38 3.53 10 -7 -5 8.20 3.72 10 7 -4 -2.86 2.06 10 -7 -4 5.15 3.44 10 7 -4 0.55 2.08 10 -7 -4 3.33 3.92 10 -7 -3 8.25 3.08 10 7 -3 14.86 4.38 10 7 -3 9.05 4.39 10 -7 -3 8.56 2.81 10 -7 -2 19.53 6.20 10 7 -2 10.22 3.31 10 7 -2 24.71 5.91 10 -7 -2 15.62 6.06 10 7 -1 48.73 8.15 10 7 -1 50.70 8.09 10 -7 -1 49.81 8.07 10 -7 -1 56.09 9.11 10 -7 0 16.30 4.07 10 7 0 21.60 5.31 10 7 0 18.12 5.19 10 -7 0 31.88 6.55 10 7 1 65.13 9.28 10 -7 1 38.37 7.20 10 7 1 64.72 9.32 10 -7 1 45.58 7.81 10 -7 2 14.01 5.33 10 7 2 15.11 4.91 10 7 2 15.65 5.26 10 -7 2 11.76 3.91 10 -7 3 11.39 4.06 10 7 3 8.85 4.43 10 7 3 10.56 4.12 10 -7 3 8.97 4.41 10 -7 4 5.68 3.53 10 7 4 2.93 2.61 10 7 4 8.71 3.27 10 -7 4 2.33 2.39 10 -7 5 7.30 3.51 10 7 5 6.27 3.55 10 7 5 1.47 2.75 10 -7 5 5.76 4.40 10 -7 6 12.15 3.79 10 7 6 5.62 4.41 10 7 6 5.96 2.80 10 -7 6 8.57 4.10 10 -7 7 2.95 3.67 10 7 7 6.50 3.88 10 7 7 0.80 1.53 10 -7 7 -1.14 3.08 10 -7 8 15.73 4.45 10 7 8 20.30 5.17 10 7 8 18.43 5.11 10 -7 8 27.18 6.00 10 -7 9 22.74 5.81 10 7 9 23.75 6.21 10 7 9 21.22 5.79 10 -7 9 34.44 6.82 10 -7 10 33.75 6.97 10 7 10 25.87 5.76 10 7 10 18.52 6.03 10 -7 10 24.88 7.54 10 -7 11 30.17 6.71 10 7 11 26.72 6.12 10 7 11 29.41 6.42 10 -7 11 14.91 3.53 10 7 12 6.05 3.46 10 -7 12 8.47 3.85 10 7 12 3.37 3.31 10 -7 12 11.15 4.82 10 7 13 9.23 3.73 10 -7 13 11.96 4.46 10 7 13 1.96 2.18 10 -7 13 9.08 4.55 10 7 14 13.65 5.35 10 -7 14 14.48 5.24 10 7 14 26.29 6.12 10 7 15 5.50 2.24 10 -7 15 3.16 3.69 10 7 15 7.48 3.62 10 7 16 14.53 5.65 10 7 16 9.90 3.89 10 7 17 0.85 3.18 10 7 18 8.30 3.76 10 7 19 3.00 2.97 10 -8 -17 3.51 3.33 10 -8 -17 6.86 4.47 10 8 -16 -0.90 4.21 10 -8 -16 3.68 2.81 10 -8 -16 3.18 1.97 10 8 -15 35.24 7.64 10 -8 -15 61.25 10.40 10 -8 -15 50.94 8.98 10 8 -14 49.36 8.19 10 -8 -14 56.48 9.81 10 -8 -14 42.14 8.58 10 8 -13 14.82 5.30 10 -8 -13 11.15 5.32 10 -8 -13 18.18 5.30 10 -8 -12 19.59 6.56 10 -8 -12 9.85 4.55 10 8 -11 20.61 6.12 10 -8 -11 23.13 6.28 10 -8 -11 25.48 6.53 10 8 -10 7.28 3.07 10 -8 -10 5.11 2.77 10 -8 -10 7.13 4.08 10 8 -9 45.13 8.42 10 -8 -9 33.04 6.90 10 -8 -9 49.31 8.83 10 8 -8 64.35 10.01 10 -8 -8 51.96 9.21 10 -8 -8 43.23 8.66 10 8 -7 16.80 5.57 -10 8 -7 -2.00 2.39 10 -8 -7 14.71 5.39 10 -8 -7 12.57 4.63 10 8 -6 60.13 9.24 -10 8 -6 60.41 9.85 10 -8 -6 70.37 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11 -3 -14 92.44 11.11 11 3 -14 112.00 11.41 11 -3 -13 91.84 10.50 11 -3 -13 100.66 10.99 11 3 -13 100.30 11.14 11 -3 -12 103.71 11.94 11 3 -12 106.70 11.05 11 -3 -12 102.38 11.08 11 -3 -11 180.75 15.25 11 3 -11 152.28 13.34 11 -3 -11 157.23 13.63 11 3 -10 30.32 6.12 11 -3 -10 33.30 7.13 11 -3 -10 35.66 6.59 11 -3 -9 720.31 29.12 11 -3 -9 695.28 29.20 11 3 -9 696.29 27.84 11 -3 -8 280.39 17.69 11 3 -8 263.16 15.39 11 -3 -8 249.11 17.26 11 3 -8 249.40 15.48 11 3 -8 229.84 16.03 11 -3 -7 61.97 8.72 11 -3 -7 71.06 9.53 11 3 -7 82.63 8.91 11 3 -7 75.24 7.99 11 3 -7 93.29 10.58 11 -3 -6 45.92 7.43 11 -3 -6 57.72 8.64 11 3 -6 52.92 7.27 11 3 -6 61.57 7.60 11 3 -6 59.49 8.19 11 -3 -5 483.05 23.29 11 -3 -5 462.29 23.63 11 3 -5 487.16 21.65 11 3 -5 462.79 20.50 11 3 -5 446.87 22.03 11 -3 -4 252.54 16.66 11 -3 -4 254.95 17.48 11 3 -4 275.83 16.18 11 3 -4 237.01 14.79 11 3 -4 272.66 17.18 11 -3 -3 1690.74 43.29 11 -3 -3 1682.16 44.07 11 3 -3 1710.69 39.95 11 3 -3 1789.07 43.00 11 -3 -2 358.45 20.00 11 -3 -2 354.26 20.39 11 3 -2 343.31 17.93 11 3 -2 317.42 17.67 11 3 -2 301.72 17.65 11 -3 -1 1419.99 39.39 11 3 -1 1392.92 36.70 11 3 -1 1428.51 37.38 11 3 -1 1487.66 39.25 11 -3 0 69.46 8.58 11 -3 0 81.45 10.10 11 3 0 79.33 8.79 11 3 0 82.39 8.76 11 3 1 1415.58 37.93 11 -3 1 1487.90 39.91 11 -3 1 1465.92 41.13 11 3 1 1380.47 37.68 11 3 2 366.17 19.20 11 -3 2 327.56 18.76 11 -3 2 325.63 19.28 11 3 2 361.90 19.10 11 3 3 1669.60 41.75 11 -3 3 1718.23 43.20 11 -3 3 1695.97 44.48 11 3 3 1707.93 42.60 11 3 4 261.13 16.52 11 -3 4 265.82 17.01 11 -3 4 261.56 17.60 11 3 4 314.11 17.89 11 3 5 483.36 22.64 11 -3 5 448.02 22.53 11 -3 5 470.07 23.28 11 3 5 435.49 21.14 11 3 6 61.42 8.16 11 -3 6 49.69 7.85 11 -3 6 52.50 8.07 11 3 6 68.91 8.47 11 3 7 92.17 10.45 11 -3 7 69.55 8.77 11 3 7 84.40 9.71 11 3 8 236.79 16.36 11 -3 8 258.35 17.34 11 3 8 263.99 16.59 11 3 9 707.34 28.46 11 -3 9 709.72 28.83 11 3 9 752.23 27.98 11 3 10 31.40 5.82 11 -3 10 27.93 5.91 11 -3 11 164.32 14.29 11 3 11 180.95 14.02 11 3 12 119.94 11.96 11 -3 12 106.29 11.19 11 3 12 107.19 11.09 11 3 13 103.41 11.06 11 -3 13 98.20 11.20 11 3 13 98.61 10.21 11 3 14 118.32 12.36 11 -3 14 97.37 11.20 11 3 14 109.93 11.09 11 3 15 27.64 5.91 11 -3 15 23.71 5.96 11 3 16 -0.52 1.42 11 -3 16 -0.81 2.78 11 3 17 54.13 8.97 11 -3 17 54.81 9.13 11 3 18 103.91 12.18 11 -3 18 121.33 12.97 11 3 19 29.78 6.37 11 -3 19 20.40 5.69 11 3 20 25.94 6.59 11 -3 20 31.94 7.74 11 3 21 12.30 3.55 11 -3 21 14.33 4.56 11 3 22 17.88 5.73 11 3 23 66.12 10.32 11 3 24 54.50 9.47 11 3 25 46.61 8.95 11 -4 -24 7.23 3.27 11 -4 -23 11.64 4.08 11 -4 -22 21.40 6.25 11 -4 -21 12.53 4.41 11 -4 -20 3.98 4.14 11 -4 -19 0.90 2.04 11 4 -19 0.72 3.01 11 -4 -18 1.81 3.52 11 4 -18 4.99 3.05 11 -4 -17 1.88 3.77 11 -4 -17 5.13 3.81 11 4 -17 4.19 4.10 11 -4 -16 5.26 3.66 11 -4 -16 1.21 3.20 11 4 -16 3.89 2.71 11 -4 -15 14.19 4.27 11 4 -15 12.00 3.75 11 -4 -15 9.85 3.52 11 4 -14 0.20 1.51 11 -4 -14 2.83 3.05 11 -4 -14 1.51 2.36 11 4 -13 2.65 1.68 11 -4 -13 0.40 2.65 11 -4 -13 1.75 3.23 11 4 -12 31.92 6.63 11 -4 -12 35.07 6.90 11 -4 -12 35.88 6.67 11 4 -11 12.02 4.06 11 -4 -11 9.80 3.92 11 -4 -11 5.65 3.42 11 -4 -10 44.33 7.76 11 -4 -10 40.83 7.22 11 4 -10 43.65 7.39 11 4 -9 8.57 3.28 11 -4 -9 3.70 2.83 11 -4 -9 7.98 3.52 11 -4 -8 97.04 10.56 11 4 -8 109.93 11.62 11 -4 -8 111.83 11.52 11 4 -7 21.36 5.23 11 4 -7 13.04 3.79 11 -4 -7 9.65 4.11 11 -4 -7 13.08 4.67 11 4 -6 4.90 2.37 11 4 -6 0.33 1.75 11 -4 -6 6.19 4.44 11 4 -5 4.69 3.52 11 -4 -5 7.11 3.09 11 4 -5 7.55 2.72 11 -4 -5 8.26 4.82 11 -4 -4 751.60 30.35 11 4 -4 747.01 27.18 11 4 -4 800.52 30.31 11 -4 -3 75.97 9.51 11 -4 -3 54.11 8.24 11 4 -3 62.59 8.27 11 4 -2 190.28 14.02 11 -4 -2 185.59 14.82 11 -4 -2 185.91 14.96 11 4 -2 163.81 12.71 11 4 -2 158.27 13.10 11 4 -1 235.04 16.16 11 4 -1 264.63 16.46 11 -4 -1 283.28 18.41 11 -4 -1 259.89 17.61 11 4 -1 216.47 14.59 11 4 0 0.03 2.14 11 -4 0 2.96 2.77 11 4 0 3.62 2.46 11 -4 0 4.13 2.70 11 4 1 243.00 16.47 11 4 1 242.05 16.00 11 -4 1 231.19 16.50 11 -4 1 233.45 16.84 11 4 2 168.40 13.80 11 4 2 158.22 13.08 11 -4 2 193.57 14.74 11 -4 2 149.04 13.82 11 4 3 93.70 10.19 11 4 3 84.06 9.46 11 -4 3 69.74 9.33 11 -4 3 78.08 10.04 11 4 4 708.62 28.06 11 4 4 635.03 27.35 11 -4 4 679.76 29.17 11 4 5 2.39 2.75 11 -4 5 5.59 2.00 11 4 5 5.00 3.28 11 -4 5 1.13 2.92 11 4 6 9.11 4.01 11 -4 6 9.14 3.47 11 4 6 9.89 4.01 11 -4 6 5.46 2.02 11 4 7 19.77 4.56 11 -4 7 14.77 4.29 11 4 7 19.71 5.32 11 -4 7 17.92 4.61 11 4 8 95.63 10.13 11 4 8 85.67 10.30 11 -4 8 99.06 10.81 11 -4 8 123.90 12.51 11 4 9 10.95 3.71 11 -4 9 8.41 4.24 11 4 9 8.35 3.98 11 -4 9 4.22 3.13 11 4 10 59.59 8.39 11 4 10 47.13 7.37 11 -4 10 42.39 7.69 11 4 11 5.31 1.72 11 -4 11 4.03 2.14 11 4 12 38.48 6.97 11 -4 12 32.34 6.30 11 4 12 30.68 6.31 11 4 13 -1.16 2.49 11 -4 13 -1.80 2.66 11 4 13 -1.21 2.20 11 4 14 0.28 1.79 11 -4 14 1.22 1.83 11 4 14 5.65 3.62 11 -4 15 12.55 4.40 11 4 15 8.42 4.07 11 -4 16 -0.11 2.42 11 4 16 3.85 3.78 11 -4 17 1.84 1.88 11 4 17 -0.29 2.64 11 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8.40 11 5 -6 25.21 5.47 11 -5 -6 33.05 5.93 11 -5 -6 25.07 5.79 11 5 -5 4.11 2.80 11 -5 -5 6.53 3.62 11 5 -5 8.56 3.34 11 -5 -5 3.39 3.55 11 5 -4 306.32 19.00 11 5 -4 314.98 18.29 11 -5 -4 312.45 20.30 11 -5 -4 312.16 19.71 11 5 -3 48.07 7.98 11 -5 -3 65.12 8.72 11 5 -3 47.99 7.45 11 -5 -3 51.05 8.28 11 5 -2 107.92 11.46 11 -5 -2 100.01 11.30 11 5 -2 116.12 11.19 11 -5 -2 117.55 12.50 11 5 -1 149.42 13.52 11 -5 -1 195.93 15.38 11 5 -1 183.72 14.31 11 -5 -1 174.65 14.99 11 5 0 5.29 3.87 11 -5 0 -2.16 2.60 11 -5 0 5.15 3.58 11 5 0 2.15 1.62 11 5 1 192.76 15.05 11 -5 1 185.39 15.32 11 5 1 174.41 14.10 11 -5 1 184.81 15.60 11 5 2 134.69 12.58 11 -5 2 108.24 11.22 11 5 2 113.53 11.39 11 -5 2 133.99 13.52 11 5 3 57.97 8.41 11 -5 3 48.89 7.96 11 5 3 60.72 8.25 11 -5 3 73.89 10.28 11 5 4 298.54 19.01 11 -5 4 313.14 20.06 11 5 4 318.23 19.39 11 -5 4 291.74 19.49 11 5 5 6.03 3.50 11 -5 5 10.29 3.88 11 -5 5 3.88 2.70 11 5 5 15.04 4.95 11 5 6 35.64 6.72 11 -5 6 32.12 6.39 11 -5 6 40.77 7.49 11 5 6 28.87 5.78 11 5 7 48.00 7.88 11 5 7 43.20 7.71 11 -5 7 39.24 7.09 11 -5 7 37.56 7.49 11 5 8 282.32 18.47 11 -5 8 325.27 20.64 11 5 8 294.04 19.36 11 -5 8 332.52 21.36 11 5 9 101.38 11.54 11 -5 9 85.10 10.76 11 5 9 86.46 10.38 11 -5 9 77.34 10.64 11 -5 10 4.39 3.39 11 -5 10 -2.06 3.94 11 5 10 -1.22 1.46 11 5 11 2.13 2.47 11 -5 11 3.48 2.25 11 -5 11 7.03 5.13 11 5 11 1.28 2.46 11 5 12 9.87 4.50 11 -5 12 27.18 6.45 11 -5 12 15.78 4.60 11 5 12 15.82 4.95 11 5 13 68.66 9.61 11 -5 13 61.72 9.66 11 5 13 57.59 9.05 11 -5 13 54.79 8.86 11 5 14 97.06 11.44 11 -5 14 77.03 11.10 11 5 14 97.38 11.31 11 5 15 24.66 6.83 11 -5 15 25.65 5.98 11 5 15 14.60 4.70 11 -5 16 2.14 2.83 11 5 16 0.48 1.68 11 -5 17 18.39 5.40 11 5 17 21.33 5.57 11 5 18 51.46 8.87 11 -5 18 43.71 9.26 11 5 19 22.50 6.49 11 5 20 41.32 8.52 11 5 21 3.34 3.24 11 5 22 30.83 7.12 11 -6 -21 4.37 3.45 11 -6 -20 7.25 3.95 11 -6 -19 6.75 2.21 11 -6 -19 21.59 8.08 11 6 -18 4.84 4.17 11 -6 -18 2.99 2.38 11 -6 -18 0.84 3.52 11 6 -17 1.22 2.16 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11 -6 -1 5.82 3.18 11 -6 -1 11.00 4.92 11 6 -1 9.89 3.08 11 6 0 -0.28 2.00 11 -6 0 2.71 2.38 11 -6 0 0.71 2.06 11 6 0 3.74 2.61 11 6 1 2.36 2.50 11 -6 1 10.62 3.43 11 -6 1 3.12 1.88 11 6 1 5.92 3.18 11 -6 2 88.52 10.75 11 6 2 80.37 9.93 11 6 2 79.67 9.93 11 -6 2 69.55 9.97 11 6 3 5.03 3.96 11 6 3 1.84 1.92 11 -6 3 1.19 3.19 11 -6 3 -1.12 1.87 11 6 4 5.92 2.85 11 6 4 7.03 3.71 11 -6 4 10.93 3.26 11 -6 4 4.96 2.49 11 6 5 10.63 3.97 11 6 5 5.20 3.88 11 -6 5 5.48 2.36 11 -6 5 4.40 2.26 11 -6 6 58.36 8.81 11 6 6 43.41 6.95 11 6 6 38.96 7.35 11 -6 6 37.17 7.53 11 6 7 2.52 1.76 11 6 7 3.99 2.30 11 -6 7 5.63 3.42 11 -6 7 3.44 2.99 11 6 8 25.37 6.29 11 6 8 41.22 7.79 11 -6 8 22.46 5.74 11 -6 8 25.08 6.17 11 6 9 10.14 3.69 11 6 9 6.26 1.94 11 -6 9 1.56 2.50 11 -6 9 10.20 2.60 11 6 10 39.49 6.85 11 -6 10 42.28 8.11 11 6 10 41.77 7.68 11 -6 10 42.79 7.41 11 6 11 1.58 1.58 11 6 11 4.37 3.38 11 -6 11 1.47 1.61 11 -6 11 2.26 2.85 11 6 12 7.30 3.33 11 6 12 2.22 3.59 11 -6 12 0.51 2.11 11 -6 12 1.29 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362.98 20.73 12 4 3 233.16 16.43 12 -4 3 245.71 17.90 12 -4 3 255.62 18.15 12 4 3 249.33 17.36 12 4 4 395.70 21.57 12 -4 4 404.68 22.24 12 -4 4 428.23 23.41 12 4 4 370.60 21.27 12 4 5 171.80 14.13 12 4 5 145.69 13.31 12 -4 5 159.80 14.17 12 -4 5 176.42 15.12 12 4 6 60.87 8.32 12 4 6 68.93 9.25 12 -4 6 72.91 9.86 12 -4 6 75.01 9.90 12 4 7 206.24 15.79 12 4 7 206.15 15.65 12 -4 7 209.51 16.38 12 -4 7 221.82 17.63 12 4 8 221.80 16.33 12 4 8 221.75 16.50 12 -4 8 239.43 17.35 12 -4 8 215.93 17.11 12 4 9 64.72 9.41 12 4 9 67.82 9.49 12 -4 9 82.01 10.30 12 -4 9 83.02 10.72 12 4 10 32.68 6.72 12 -4 10 27.64 6.13 12 4 10 26.21 5.50 12 -4 10 26.73 6.82 12 4 11 14.20 4.81 12 -4 11 10.14 3.73 12 4 11 6.02 1.96 12 4 12 3.93 3.47 12 -4 12 -0.76 3.25 12 4 12 -1.12 1.46 12 4 13 43.87 8.16 12 -4 13 33.02 6.49 12 4 13 54.17 8.37 12 4 14 26.58 5.57 12 4 14 50.31 8.13 12 -4 14 40.95 7.89 12 -4 15 14.36 5.19 12 4 15 16.62 4.32 12 -4 16 13.81 5.17 12 4 16 9.33 3.77 12 -4 17 14.50 5.40 12 4 17 20.75 5.24 12 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12 -5 -5 0.43 1.50 12 5 -5 1.98 1.23 12 -5 -5 0.38 2.65 12 5 -4 2.34 1.88 12 -5 -4 1.19 4.17 12 5 -4 0.85 1.81 12 -5 -4 1.36 2.16 12 5 -3 30.74 6.74 12 -5 -3 28.04 6.26 12 5 -3 20.22 5.36 12 -5 -3 18.46 4.41 12 5 -2 75.61 9.23 12 -5 -2 49.51 8.18 12 5 -2 68.83 8.72 12 -5 -2 79.08 10.48 12 5 -1 47.86 8.26 12 -5 -1 44.31 7.90 12 5 -1 48.84 7.48 12 -5 -1 32.18 6.63 12 5 0 17.10 4.06 12 -5 0 18.98 5.44 12 5 0 16.12 4.44 12 -5 0 13.72 4.96 12 5 1 36.04 7.00 12 -5 1 26.68 5.77 12 5 1 24.15 5.24 12 -5 1 45.03 8.73 12 5 2 60.67 8.83 12 -5 2 64.08 9.50 12 -5 2 53.75 8.75 12 5 3 32.46 6.55 12 -5 3 25.49 6.61 12 5 3 14.38 4.50 12 -5 3 23.22 6.07 12 5 4 0.98 1.58 12 -5 4 -0.83 1.49 12 5 4 3.78 1.32 12 -5 4 2.17 2.65 12 5 5 1.97 2.38 12 -5 5 1.41 2.83 12 5 5 1.03 1.29 12 -5 5 -0.94 2.13 12 5 6 -0.55 2.13 12 -5 6 -2.04 2.68 12 5 6 -0.96 1.40 12 -5 6 5.39 4.31 12 5 7 11.08 3.80 12 -5 7 7.03 3.41 12 5 7 9.05 3.86 12 -5 7 11.36 5.24 12 5 8 4.02 3.83 12 -5 8 4.30 3.46 12 5 8 3.71 1.90 12 -5 8 0.62 1.79 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105.72 12.64 12 -6 -13 84.18 11.89 12 6 -13 100.03 12.08 12 -6 -12 6.92 3.12 12 6 -12 6.22 3.32 12 -6 -12 12.70 4.87 12 -6 -11 30.80 6.62 12 6 -11 42.94 7.56 12 -6 -11 31.39 6.48 12 -6 -10 58.54 9.56 12 -6 -10 58.97 9.57 12 6 -10 57.71 8.56 12 -6 -9 18.35 5.39 12 6 -9 20.00 6.39 12 -6 -9 19.09 6.40 12 -6 -8 169.80 15.53 12 -6 -8 138.64 13.89 12 6 -8 127.93 13.21 12 -6 -7 151.67 14.79 12 -6 -7 160.63 14.89 12 6 -7 182.15 15.66 12 6 -6 28.72 7.06 12 -6 -6 28.80 6.24 12 -6 -6 24.51 5.71 12 6 -5 38.42 7.35 12 -6 -5 40.16 7.39 12 -6 -5 42.25 7.93 12 6 -4 102.02 11.78 12 6 -4 126.94 13.15 12 -6 -4 94.96 11.83 12 -6 -4 103.85 12.17 12 6 -3 159.33 14.33 12 6 -3 149.29 14.14 12 -6 -3 156.20 14.74 12 -6 -3 173.85 15.70 12 6 -2 171.33 15.06 12 6 -2 160.86 14.24 12 -6 -2 150.95 15.30 12 -6 -2 146.25 14.40 12 6 -1 36.64 7.14 12 6 -1 42.43 7.33 12 -6 -1 32.28 6.39 12 -6 -1 41.24 8.07 12 6 0 1.43 1.73 12 -6 0 -4.29 2.36 12 -6 0 -2.78 2.43 12 6 0 1.30 2.27 12 6 1 31.16 7.22 12 6 1 38.99 7.07 12 -6 1 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22.27 7.15 13 5 13 4.14 2.75 13 -5 13 8.82 3.90 13 5 13 3.54 2.09 13 -5 13 7.80 3.48 13 5 14 18.03 5.33 13 -5 14 29.28 6.70 13 5 14 29.02 6.90 13 -5 14 22.18 6.63 13 -5 15 6.78 4.73 13 5 15 16.30 4.50 13 -5 15 6.04 3.04 13 -5 16 19.55 5.58 13 5 16 19.77 5.65 13 -5 17 17.40 5.51 13 5 17 20.24 5.06 13 -5 18 11.80 5.75 13 5 18 14.87 5.64 13 -5 19 5.87 4.04 13 5 19 12.61 5.26 13 5 20 36.61 8.03 13 -6 -18 1.69 3.43 13 6 -18 1.90 2.68 13 -6 -17 3.13 2.86 13 -6 -17 2.68 3.39 13 6 -17 3.35 3.76 13 6 -16 -2.77 2.90 13 -6 -16 -2.43 3.69 13 -6 -16 0.27 2.05 13 6 -15 3.60 3.08 13 -6 -15 0.28 2.00 13 -6 -15 1.57 3.29 13 6 -14 8.29 3.68 13 -6 -14 6.48 4.09 13 -6 -14 -0.62 2.11 13 6 -13 3.18 1.93 13 -6 -13 4.01 3.94 13 -6 -12 2.05 3.28 13 6 -12 1.02 2.97 13 -6 -12 2.87 3.86 13 -6 -11 8.18 5.12 13 -6 -11 3.25 2.37 13 6 -10 0.65 1.63 13 -6 -10 10.57 4.74 13 -6 -10 5.99 2.93 13 6 -9 -0.78 2.03 13 -6 -9 2.88 3.74 13 -6 -9 5.14 3.80 13 6 -8 7.66 3.35 13 -6 -8 6.45 4.21 13 -6 -8 4.89 3.58 13 6 -7 5.29 4.14 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13 -6 7 0.15 3.41 13 6 8 9.13 4.08 13 -6 8 7.52 4.64 13 6 8 -0.55 1.94 13 -6 8 8.43 3.32 13 6 9 2.69 3.19 13 -6 9 2.01 3.38 13 6 9 3.71 1.30 13 -6 9 9.16 4.63 13 6 10 9.36 4.04 13 -6 10 8.09 3.92 13 6 10 2.71 2.64 13 -6 10 3.68 2.80 13 6 11 11.51 4.50 13 -6 11 5.39 4.05 13 6 11 13.55 4.94 13 -6 11 9.69 3.85 13 6 12 4.73 3.67 13 -6 12 -2.62 3.32 13 6 12 3.17 3.19 13 -6 12 2.03 2.10 13 -6 13 2.20 2.09 13 6 13 6.70 3.03 13 -6 13 1.15 2.14 13 6 14 6.96 3.63 13 -6 14 6.15 4.07 13 6 14 10.21 4.76 13 -6 14 6.79 5.16 13 -6 15 -0.70 2.46 13 6 15 0.66 1.70 13 -6 16 1.82 3.08 13 6 16 -2.34 2.35 13 -6 16 -2.77 5.16 13 -6 17 -0.49 2.80 13 6 17 0.55 2.64 13 -6 17 0.93 3.42 13 6 18 3.53 2.55 13 -6 18 -3.33 2.84 13 7 -15 6.72 5.00 13 -7 -15 9.26 3.25 13 -7 -15 -0.86 3.26 13 7 -14 12.03 4.32 13 -7 -14 5.26 2.96 13 -7 -14 8.76 3.87 13 7 -13 7.30 4.52 13 -7 -13 3.35 2.60 13 -7 -13 3.79 3.81 13 7 -12 9.43 4.82 13 -7 -12 7.00 3.26 13 -7 -12 16.40 5.20 13 7 -11 15.86 5.36 13 -7 -11 8.63 4.29 13 -7 -11 17.17 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5.33 3.22 13 8 -7 10.06 4.07 13 -8 -7 5.71 2.03 13 -8 -6 6.16 3.96 13 8 -6 6.53 5.36 13 -8 -6 7.57 4.08 13 -8 -5 2.03 3.84 13 -8 -5 3.99 2.20 13 -8 -4 0.96 2.33 13 8 -4 2.26 4.08 -13 8 -4 -0.55 3.63 13 -8 -4 1.37 2.98 13 -8 -3 0.66 3.99 13 8 -3 4.14 3.71 13 -8 -3 2.70 2.48 13 8 -2 -0.30 2.40 13 -8 -2 3.30 2.47 13 -8 -1 1.63 2.20 13 8 -1 1.99 2.83 13 -8 -1 -1.85 2.46 13 -8 0 0.90 3.48 13 8 0 -0.29 2.49 13 -8 0 4.01 4.84 13 8 0 1.35 1.81 13 -8 1 4.32 4.38 13 8 1 0.19 2.94 13 -8 1 0.68 2.40 13 8 1 2.79 3.36 13 -8 2 1.76 3.07 13 8 2 5.56 4.48 13 -8 2 2.35 2.53 13 8 2 0.35 2.40 13 -8 3 6.42 4.78 13 8 3 8.96 4.00 13 -8 3 7.40 4.72 13 8 3 2.13 1.65 13 -8 4 3.97 2.61 13 8 4 -1.80 1.94 13 -8 4 -0.12 3.70 13 8 4 1.77 2.27 13 -8 5 9.36 3.44 13 8 5 5.28 2.45 13 -8 5 1.26 2.32 13 8 5 7.69 3.70 13 8 6 3.66 2.26 13 -8 6 5.96 2.35 13 -8 6 1.37 2.53 13 8 6 4.04 4.00 13 8 7 8.00 3.64 13 -8 7 4.25 3.07 13 -8 7 1.28 3.92 13 8 7 13.28 5.90 13 8 8 10.26 3.57 13 -8 8 9.75 5.00 13 -8 8 1.72 2.67 13 8 8 6.30 3.53 13 8 9 3.96 2.84 13 -8 9 5.32 3.11 13 -8 9 11.45 6.47 13 8 9 5.42 4.05 13 8 10 -0.18 2.76 13 -8 10 2.07 4.74 13 8 10 -0.71 2.13 13 8 11 10.33 5.33 13 -8 11 5.90 4.48 13 8 11 8.49 3.73 13 -9 -3 -2.13 4.77 13 9 -3 12.08 4.45 -13 9 -3 6.92 2.48 13 -9 -3 8.16 4.87 13 -9 -2 2.58 3.95 13 9 -2 8.60 3.59 -13 9 -2 7.13 4.80 13 -9 -2 -2.61 4.51 13 -9 -1 4.20 3.12 13 9 -1 1.59 2.45 -13 9 -1 5.11 4.68 13 -9 -1 6.81 3.61 13 -9 0 23.24 5.92 13 9 0 19.44 5.76 -13 9 0 21.08 6.30 13 -9 0 21.00 7.49 13 -9 1 6.34 3.20 13 9 1 2.52 2.41 -13 9 1 0.04 2.75 13 -9 1 0.79 2.70 13 -9 2 1.81 1.83 13 9 2 7.48 3.95 -13 9 2 7.82 4.89 13 -9 2 6.07 5.50 13 9 2 -2.26 3.56 13 -9 3 -3.63 4.58 13 9 3 5.13 5.08 -13 9 3 12.12 5.10 13 -9 3 6.29 3.82 13 9 3 1.98 3.53 14 0 -20 29.93 6.99 14 0 -19 10.18 4.57 14 0 -18 3.53 4.05 14 0 -17 4.25 4.22 14 0 -16 76.89 11.22 14 0 -15 13.75 4.67 14 0 -14 40.28 7.88 14 0 -13 88.87 11.22 14 0 -12 142.98 14.01 14 0 -11 14.42 3.82 14 0 -10 154.61 14.04 14 0 -10 157.90 14.35 14 0 -9 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22.58 4.97 14 -1 -4 11.76 4.18 14 1 -4 14.94 5.01 14 1 -4 15.96 4.28 14 -1 -3 12.86 3.74 14 -1 -3 13.43 4.14 14 1 -3 11.58 4.09 14 1 -3 11.61 4.04 14 1 -3 11.17 3.13 14 -1 -2 49.33 8.16 14 1 -2 51.44 8.07 14 -1 -2 59.00 8.58 14 1 -2 57.05 8.42 14 1 -2 70.73 9.24 14 -1 -1 83.90 10.25 14 1 -1 77.41 9.68 14 -1 -1 65.19 9.21 14 1 -1 85.59 10.39 14 1 -1 71.33 9.50 14 -1 0 61.66 8.70 14 1 0 71.85 9.11 14 -1 0 58.81 8.75 14 1 0 72.25 9.24 14 1 0 44.28 7.10 14 -1 1 74.96 9.37 14 1 1 75.47 9.49 14 -1 1 58.27 8.95 14 1 1 66.83 9.52 14 1 1 71.03 9.45 14 -1 2 49.84 8.07 14 1 2 68.35 9.01 14 -1 2 64.47 9.48 14 1 2 77.31 10.09 14 1 2 53.42 8.35 14 1 3 17.74 4.92 14 -1 3 25.48 6.17 14 -1 3 9.09 3.88 14 1 3 13.00 4.16 14 1 4 18.32 4.80 14 -1 4 25.39 6.45 14 -1 4 21.19 6.06 14 1 4 14.66 5.05 14 1 5 0.99 2.35 14 -1 5 5.16 3.75 14 -1 5 -0.02 1.58 14 1 5 1.32 3.01 14 1 6 0.78 2.32 14 -1 6 4.63 2.31 14 1 6 -1.42 2.16 14 1 7 42.50 7.23 14 -1 7 32.24 6.70 14 1 7 39.06 6.83 14 1 8 0.20 1.76 14 -1 8 6.05 3.56 14 1 8 6.98 3.82 14 1 9 21.14 5.57 14 -1 9 27.96 5.80 14 1 9 18.73 6.12 14 1 10 6.60 3.17 14 -1 10 12.28 3.72 14 1 10 18.95 4.51 14 1 11 -0.62 2.48 14 -1 11 4.51 4.43 14 1 11 0.59 2.13 14 1 12 1.50 1.90 14 -1 12 -0.48 1.58 14 1 13 4.16 3.35 14 -1 13 0.41 2.66 14 1 14 1.09 1.63 14 -1 14 2.04 3.16 14 1 15 6.82 2.62 14 -1 15 12.55 4.41 14 1 16 3.86 3.09 14 -1 16 2.18 3.46 14 1 17 -0.74 3.03 14 -1 17 -2.55 2.67 14 1 18 7.60 4.02 14 -1 18 10.73 4.30 14 1 19 7.52 3.68 14 -1 19 9.86 4.35 14 1 20 0.66 2.04 14 -1 20 0.75 2.64 14 1 21 0.73 2.86 14 -1 21 1.79 2.80 14 1 22 2.30 3.60 14 -1 22 -1.42 2.23 14 -2 -22 10.63 2.42 14 -2 -21 18.26 4.71 14 -2 -20 28.63 7.17 14 -2 -19 4.17 3.38 14 -2 -18 6.89 3.90 14 -2 -17 26.30 6.86 14 -2 -16 62.50 9.95 14 -2 -15 25.54 6.25 14 -2 -14 56.39 9.39 14 2 -14 71.51 10.03 14 -2 -13 23.60 6.84 14 -2 -13 23.51 5.78 14 2 -13 15.00 4.56 14 -2 -12 66.39 10.03 14 -2 -12 62.46 9.63 14 2 -12 65.76 9.69 14 -2 -11 10.23 2.89 14 -2 -11 14.73 5.61 14 2 -11 4.45 3.40 14 -2 -10 66.74 9.56 14 -2 -10 51.49 7.89 14 2 -10 62.30 8.99 14 2 -10 79.87 10.04 14 -2 -9 109.50 12.34 14 -2 -9 101.90 12.22 14 2 -9 95.85 11.30 14 2 -9 113.27 12.01 14 -2 -8 29.19 6.47 14 2 -8 30.13 6.10 14 -2 -8 28.84 6.29 14 2 -8 23.70 5.45 14 2 -8 27.26 6.05 14 -2 -7 16.78 4.66 14 -2 -7 21.40 5.54 14 2 -7 24.70 5.26 14 2 -7 8.35 2.57 14 2 -7 27.19 6.00 14 -2 -6 73.60 9.59 14 2 -6 84.46 9.90 14 -2 -6 76.05 10.24 14 2 -6 97.38 11.33 14 2 -6 75.27 9.55 14 -2 -5 91.15 10.69 14 2 -5 82.60 10.38 14 -2 -5 84.02 10.95 14 2 -5 90.90 11.00 14 2 -5 87.17 10.33 14 -2 -4 104.67 11.74 14 2 -4 123.76 12.23 14 -2 -4 134.84 13.57 14 2 -4 116.44 11.96 14 2 -4 112.63 12.05 14 -2 -3 23.93 5.61 14 2 -3 35.70 7.10 14 -2 -3 24.79 5.91 14 2 -3 28.87 5.90 14 2 -3 24.45 5.55 14 -2 -2 14.31 5.00 14 -2 -2 19.26 5.43 14 2 -2 12.74 3.59 14 2 -2 13.38 3.63 14 2 -2 12.49 3.84 14 2 -1 23.57 5.61 14 -2 -1 23.81 6.05 14 -2 -1 11.19 4.79 14 2 -1 12.87 4.15 14 2 -1 18.63 4.98 14 -2 0 235.13 17.00 14 2 0 241.72 16.81 14 -2 0 222.16 17.30 14 2 0 196.19 16.46 14 2 0 214.27 16.26 14 2 1 12.22 3.51 14 -2 1 21.55 5.26 14 -2 1 15.50 4.94 14 2 1 10.47 3.83 14 2 1 22.24 5.29 14 2 2 14.11 4.03 14 -2 2 10.98 4.11 14 -2 2 13.61 3.97 14 2 2 9.14 3.53 14 2 2 14.99 4.44 14 2 3 25.54 6.04 14 -2 3 25.63 5.82 14 -2 3 31.40 7.13 14 2 3 28.97 5.81 14 -2 4 122.87 12.61 14 2 4 110.94 11.60 14 -2 4 137.46 13.84 14 2 4 108.06 11.34 14 -2 5 95.78 11.10 14 2 5 79.50 10.33 14 -2 5 80.38 10.67 14 2 5 73.49 9.49 14 -2 6 87.81 10.70 14 2 6 86.03 10.29 14 -2 6 82.60 10.53 14 2 6 91.95 10.57 14 2 7 17.33 4.79 14 -2 7 21.34 4.73 14 -2 7 18.17 4.87 14 2 7 18.57 4.96 14 2 8 22.83 5.91 14 -2 8 29.17 6.32 14 2 8 27.07 5.42 14 -2 9 95.24 10.96 14 2 9 101.73 11.62 14 2 9 96.65 11.22 14 -2 10 58.20 9.04 14 2 10 71.13 9.69 14 2 10 67.70 9.21 14 2 11 7.50 2.79 14 -2 11 5.87 3.42 14 2 11 11.05 3.98 14 -2 12 64.33 10.03 14 2 12 66.57 9.61 14 2 12 76.46 9.79 14 2 13 17.52 4.93 14 -2 13 20.34 6.02 14 -2 14 70.10 10.47 14 2 14 74.47 10.52 14 2 15 24.16 6.29 14 -2 15 23.39 5.75 14 -2 16 70.95 10.53 14 2 16 56.00 9.03 14 2 17 13.07 4.37 14 -2 17 20.80 5.82 14 2 18 3.76 2.07 14 -2 18 4.46 3.39 14 2 19 6.08 3.39 14 -2 19 8.68 4.58 14 2 20 29.91 7.01 14 -2 20 19.32 7.59 14 2 21 25.28 5.87 14 -2 21 14.90 5.75 14 2 22 13.72 4.53 14 -2 22 21.48 5.54 14 -3 -21 -2.49 3.85 14 -3 -20 11.19 4.92 14 -3 -19 0.63 2.99 14 -3 -18 11.03 5.20 14 3 -18 3.50 2.96 14 -3 -17 -6.06 3.94 14 3 -17 -1.50 1.83 14 -3 -16 19.61 5.70 14 3 -16 18.19 5.63 14 -3 -15 11.57 4.50 14 3 -15 7.47 3.90 14 -3 -14 7.10 3.80 14 -3 -14 9.45 4.13 14 3 -14 13.03 4.74 14 -3 -13 13.93 4.66 14 -3 -13 8.93 2.81 14 3 -13 4.15 2.77 14 -3 -12 3.20 2.87 14 -3 -12 3.21 2.61 14 3 -12 3.32 3.00 14 -3 -11 9.51 4.03 14 -3 -11 6.06 2.59 14 3 -11 11.67 3.80 14 -3 -10 42.82 8.00 14 -3 -10 58.70 9.16 14 3 -10 46.09 7.84 14 -3 -9 2.43 1.60 14 -3 -9 5.64 2.89 14 3 -9 1.57 1.47 14 -3 -8 2.12 2.09 14 -3 -8 2.28 3.47 14 3 -8 0.30 2.23 14 -3 -7 6.78 2.85 14 -3 -7 6.18 3.60 14 3 -7 3.16 2.51 14 3 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14 3 5 25.35 5.84 14 3 5 24.87 6.03 14 -3 5 16.29 5.24 14 -3 5 13.31 4.70 14 3 6 14.48 4.85 14 3 6 8.83 3.82 14 -3 6 7.24 2.99 14 -3 6 1.97 2.42 14 3 7 7.45 4.08 14 3 7 4.24 1.90 14 -3 7 7.01 3.06 14 -3 7 2.77 2.62 14 3 8 2.56 2.36 14 3 8 -0.30 1.32 14 -3 8 -1.17 2.51 14 -3 8 2.05 1.68 14 3 9 4.72 3.53 14 3 9 1.77 2.05 14 -3 9 6.17 4.95 14 -3 9 3.82 4.37 14 3 10 42.08 7.21 14 -3 10 52.93 8.65 14 3 10 57.85 8.95 14 3 11 9.38 4.32 14 3 11 7.24 2.56 14 -3 11 6.48 2.87 14 3 12 4.44 3.48 14 3 12 0.61 2.13 14 -3 12 4.65 3.51 14 3 13 5.49 3.56 14 -3 13 4.32 1.83 14 3 14 3.81 3.21 14 -3 14 6.59 3.64 14 3 15 6.26 2.92 14 -3 15 10.15 4.96 14 3 16 9.75 3.91 14 -3 16 12.11 4.70 14 3 17 1.14 2.08 14 -3 17 4.42 3.48 14 3 18 4.63 1.69 14 -3 18 0.19 4.32 14 3 19 2.89 2.69 14 -3 19 7.50 4.33 14 3 20 9.42 5.40 14 -3 20 4.35 2.24 14 3 21 4.19 2.88 14 -3 21 3.12 3.77 14 -4 -20 60.39 10.18 14 4 -20 42.72 8.91 14 -4 -19 2.90 4.50 14 4 -19 -1.73 2.00 14 -4 -18 9.21 4.15 14 4 -18 14.42 5.53 14 -4 -17 48.78 8.57 14 4 -17 41.25 8.42 14 -4 -16 37.51 7.40 14 4 -16 48.44 8.87 14 -4 -15 20.12 5.96 14 -4 -15 13.90 4.90 14 4 -15 26.36 7.13 14 -4 -14 42.30 8.40 14 -4 -14 52.87 8.64 14 4 -14 43.59 8.00 14 -4 -13 8.77 4.80 14 -4 -13 6.32 4.24 14 4 -13 1.93 1.70 14 -4 -12 38.10 7.71 14 -4 -12 33.26 7.95 14 4 -12 41.47 8.63 14 -4 -11 72.89 10.49 14 4 -11 61.15 9.42 14 -4 -11 79.78 10.82 14 -4 -10 43.32 7.60 14 4 -10 48.68 8.12 14 -4 -10 42.66 8.03 14 -4 -9 87.76 11.38 14 4 -9 100.55 11.95 14 -4 -9 76.72 10.87 14 4 -8 30.49 6.59 14 -4 -8 29.09 6.84 14 -4 -8 31.79 6.83 14 4 -7 9.31 3.80 14 -4 -7 4.32 3.23 14 -4 -7 9.22 3.71 14 -4 -6 79.88 10.94 14 -4 -6 110.03 12.74 14 4 -6 84.13 10.81 14 4 -5 25.55 6.02 14 4 -5 21.75 4.74 14 -4 -5 29.47 7.08 14 -4 -5 27.22 6.53 14 -4 -4 97.97 11.60 14 -4 -4 81.64 11.00 14 4 -4 61.62 8.75 14 4 -4 85.09 10.42 14 -4 -3 65.62 9.86 14 -4 -3 57.96 9.56 14 4 -3 50.47 7.45 14 4 -3 45.48 8.03 14 4 -2 22.37 5.26 14 4 -2 10.79 2.97 14 -4 -2 7.58 3.90 14 -4 -2 12.84 4.30 14 4 -1 19.89 5.82 14 4 -1 34.18 6.69 14 -4 -1 32.28 7.39 14 -4 -1 21.44 6.21 14 -4 0 521.84 26.65 14 -4 0 526.29 28.11 14 4 0 501.82 25.19 14 4 0 548.38 26.26 14 -4 1 36.47 7.47 14 4 1 34.03 6.89 14 -4 1 25.88 6.36 14 4 1 29.99 6.83 14 4 1 36.42 7.53 14 4 2 13.13 4.65 14 4 2 20.89 4.99 14 -4 2 14.42 4.86 14 -4 2 17.61 4.99 14 -4 3 48.22 8.32 14 -4 3 55.05 9.04 14 4 3 66.95 9.28 14 4 3 58.50 8.69 14 -4 4 73.15 10.36 14 -4 4 71.57 10.24 14 4 4 67.18 9.27 14 4 4 79.67 10.41 14 4 5 32.55 6.91 14 -4 5 38.88 7.90 14 4 5 30.00 6.47 14 -4 5 23.18 5.21 14 -4 6 88.53 11.08 14 -4 6 79.24 11.26 14 4 6 89.09 10.88 14 4 6 87.44 10.72 14 4 7 6.15 3.13 14 4 7 13.47 4.56 14 -4 7 11.03 3.64 14 -4 7 11.02 4.70 14 4 8 19.73 5.13 14 4 8 29.07 6.55 14 -4 8 28.30 6.53 14 -4 8 33.13 8.21 14 4 9 75.64 10.98 14 -4 9 90.88 11.29 14 -4 9 81.92 11.16 14 4 9 90.23 11.04 14 4 10 17.62 4.51 14 4 10 33.54 7.07 14 -4 10 37.33 7.33 14 -4 10 18.78 5.48 14 4 11 85.35 10.97 14 -4 11 80.22 11.18 14 -4 11 81.62 11.06 14 4 11 78.08 10.66 14 4 12 55.20 9.03 14 4 12 46.73 8.21 14 -4 12 59.72 9.16 14 -4 12 48.80 9.30 14 4 13 10.85 5.37 14 4 13 10.56 4.13 14 -4 13 15.11 4.32 14 4 14 42.07 7.76 14 -4 14 32.92 7.44 14 4 15 21.56 5.51 14 -4 15 21.13 5.83 14 4 16 40.63 7.40 14 -4 16 28.00 7.01 14 4 17 38.33 7.78 14 -4 17 33.99 7.70 14 4 18 8.52 4.91 14 -4 18 6.69 4.13 14 4 19 0.43 2.99 14 -4 19 -6.81 5.46 14 -4 20 35.55 8.08 14 4 20 52.02 9.47 14 -5 -18 0.38 2.02 14 5 -18 3.89 3.61 14 -5 -17 6.33 4.58 14 5 -17 3.87 2.00 14 -5 -16 1.49 1.45 14 -5 -16 2.73 2.39 14 -5 -15 -3.18 2.08 14 -5 -15 -0.89 1.60 14 -5 -14 2.22 2.39 14 -5 -14 5.79 3.76 14 5 -14 8.46 3.30 14 5 -13 4.33 1.57 14 -5 -13 6.82 3.50 14 5 -12 27.85 6.62 14 -5 -12 16.09 6.21 14 -5 -12 16.33 4.87 14 5 -11 10.84 3.97 14 -5 -11 11.53 3.72 14 -5 -11 2.34 2.69 14 5 -10 13.61 4.42 14 -5 -10 12.58 3.69 14 5 -9 18.27 4.87 14 -5 -9 18.17 5.94 14 -5 -9 17.96 6.67 14 5 -8 3.16 3.51 14 -5 -8 7.78 4.77 14 -5 -8 2.83 2.13 14 5 -7 7.70 3.76 14 -5 -7 18.81 5.76 14 -5 -7 7.84 4.34 14 5 -6 3.03 2.86 14 -5 -6 5.40 3.36 14 -5 -6 -1.21 2.29 14 5 -5 8.87 4.62 14 -5 -5 1.19 1.86 14 -5 -5 2.39 3.03 14 5 -4 11.50 3.28 14 -5 -4 11.03 4.70 14 5 -4 15.23 3.99 14 -5 -4 14.41 6.67 14 5 -3 3.55 2.22 14 -5 -3 10.03 3.82 14 5 -3 9.29 3.60 14 -5 -3 4.10 2.48 14 5 -2 4.43 3.00 14 -5 -2 9.64 3.42 14 5 -2 15.08 4.62 14 -5 -2 18.26 6.07 14 -5 -1 52.96 8.71 14 -5 -1 50.72 8.85 14 5 -1 47.25 8.04 14 5 -1 50.20 8.71 14 -5 0 86.18 11.09 14 -5 0 100.04 12.81 14 5 0 100.49 11.66 14 5 0 116.85 11.91 14 -5 1 48.84 8.40 14 -5 1 56.30 9.01 14 5 1 45.75 8.73 14 5 1 35.87 7.71 14 5 2 12.21 5.20 14 -5 2 12.70 4.59 14 5 2 10.66 4.93 14 -5 2 11.23 4.65 14 5 3 7.11 3.24 14 -5 3 5.54 4.27 14 5 3 5.72 3.00 14 -5 3 5.19 2.93 14 5 4 21.53 5.09 14 -5 4 11.24 4.30 14 5 4 16.38 5.15 14 -5 4 17.68 5.23 14 5 5 -1.14 3.35 14 -5 5 1.03 2.83 14 5 5 3.44 3.13 14 -5 5 1.96 4.18 14 5 6 2.87 2.73 14 -5 6 -2.14 2.31 14 5 6 -1.59 3.16 14 -5 6 4.53 3.96 14 5 7 12.12 4.55 14 -5 7 21.45 5.89 14 5 7 12.91 4.12 14 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-12 37.70 8.06 14 6 -11 19.78 5.75 14 -6 -11 17.08 5.01 14 -6 -11 13.39 4.46 14 -6 -10 90.96 12.18 14 -6 -10 99.34 13.17 14 6 -10 104.11 12.53 14 6 -9 21.84 5.33 14 -6 -9 25.22 6.61 14 -6 -9 27.57 7.03 14 -6 -8 8.00 3.63 14 -6 -8 3.00 2.03 14 6 -7 26.70 6.57 14 -6 -7 9.94 4.64 14 -6 -7 30.88 6.61 14 -6 -6 107.66 13.03 14 -6 -6 118.30 13.41 14 6 -6 136.06 13.70 14 6 -5 2.06 2.92 14 -6 -5 0.96 2.43 14 -6 -5 0.11 3.15 14 -6 -4 87.68 11.66 14 -6 -4 74.44 11.20 14 6 -4 97.16 11.95 14 6 -3 40.73 7.86 14 -6 -3 34.82 7.32 14 -6 -3 45.68 8.42 14 6 -2 24.78 6.52 14 -6 -2 35.73 7.57 14 6 -2 18.96 5.69 14 -6 -2 35.10 7.39 14 -6 -1 50.66 8.81 14 6 -1 45.53 8.13 14 6 -1 23.45 5.88 14 -6 -1 34.78 7.10 14 -6 0 220.47 18.28 14 6 0 255.41 19.33 14 -6 0 239.69 19.37 14 6 0 251.69 18.60 14 -6 1 43.08 7.62 14 6 1 38.08 7.23 14 -6 1 47.74 9.13 14 6 1 65.69 9.80 14 6 2 40.44 7.17 14 -6 2 35.34 7.11 14 6 2 33.04 6.89 14 -6 2 28.03 7.49 14 6 3 34.49 7.81 14 -6 3 37.66 7.59 14 6 3 39.55 7.53 14 -6 3 28.05 6.70 14 6 4 87.24 11.48 14 -6 4 89.91 11.80 14 6 4 88.49 11.33 14 -6 4 88.92 12.08 14 6 5 0.98 2.48 14 -6 5 7.32 5.07 14 6 5 3.08 4.05 14 -6 5 1.29 4.11 14 6 6 155.32 15.10 14 -6 6 134.06 14.33 14 6 6 129.42 13.83 14 -6 6 140.81 15.62 14 6 7 24.30 6.18 14 -6 7 23.64 5.90 14 6 7 30.74 6.98 14 -6 7 27.65 7.05 14 6 8 11.81 4.10 14 -6 8 5.03 3.86 14 -6 8 9.39 4.40 14 6 9 24.00 6.71 14 -6 9 29.80 6.88 14 6 9 24.49 5.94 14 -6 9 17.13 5.58 14 6 10 89.26 12.00 14 -6 10 67.08 11.61 14 6 10 89.85 11.46 14 6 11 10.94 4.74 14 -6 11 22.15 6.54 14 6 11 29.73 6.94 14 -6 11 20.92 5.07 14 6 12 41.54 8.20 14 -6 12 46.56 9.09 14 6 12 32.15 6.08 14 -6 12 24.89 6.82 14 6 13 11.76 4.78 14 -6 13 6.30 6.09 14 6 13 5.79 3.87 14 -6 13 8.98 4.87 14 -6 14 5.11 5.40 14 6 14 3.14 1.87 14 -6 14 -0.86 4.88 14 -6 15 4.57 4.31 14 6 15 6.23 3.17 14 -6 15 4.22 2.53 14 6 16 45.08 8.30 14 -6 16 23.00 8.07 14 -6 16 27.34 7.76 14 7 -13 0.13 2.48 14 -7 -13 9.30 5.02 14 -7 -13 3.00 3.38 14 -7 -12 7.02 2.49 14 -7 -12 1.55 1.87 14 -7 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19 0 12 -2.77 3.14 19 -1 -12 5.93 4.60 19 -1 -11 32.90 7.74 19 -1 -10 47.74 9.02 19 -1 -9 9.35 5.62 19 1 -9 -2.67 4.54 19 -1 -8 17.37 5.65 19 -1 -8 11.39 4.56 19 1 -8 5.01 3.68 19 -1 -7 23.11 6.50 19 -1 -7 29.47 8.02 19 1 -7 31.28 7.37 19 1 -6 37.57 8.76 19 -1 -6 36.84 8.27 19 -1 -6 49.81 9.68 19 1 -6 46.63 9.57 19 -1 -5 54.88 10.03 19 1 -5 48.49 8.79 19 -1 -5 34.21 8.09 19 1 -5 40.06 8.47 19 -1 -4 22.89 6.64 19 1 -4 24.17 6.76 19 -1 -4 27.98 7.75 19 1 -4 33.05 8.21 19 -1 -3 20.64 5.42 19 1 -3 10.00 3.88 19 -1 -3 15.63 5.70 19 1 -3 12.69 5.21 19 -1 -2 70.87 10.76 19 1 -2 59.69 10.01 19 -1 -2 66.71 10.89 19 1 -2 76.25 11.77 19 -1 -1 61.84 11.18 19 1 -1 50.71 9.35 19 -1 -1 54.47 9.88 19 1 -1 58.33 10.33 19 -1 0 9.95 3.41 19 1 0 11.70 4.56 19 -1 0 9.91 4.52 19 1 0 3.14 3.28 19 -1 1 62.18 9.72 19 1 1 59.95 9.60 19 -1 1 53.81 10.30 19 1 1 60.89 10.75 19 -1 2 55.51 9.12 19 -1 2 52.35 9.23 19 1 2 37.04 8.40 19 -1 3 20.86 7.01 19 1 3 7.67 2.99 19 -1 3 12.76 5.55 19 1 3 13.01 5.67 19 -1 4 30.34 7.36 19 1 4 23.78 6.42 19 -1 4 29.67 7.29 19 1 4 13.18 4.85 19 -1 5 49.22 8.88 19 1 5 65.24 9.84 19 -1 5 60.18 10.16 19 1 5 28.82 7.15 19 -1 6 29.10 6.64 19 -1 6 43.18 9.12 19 1 6 46.39 8.77 19 1 6 51.83 9.76 19 1 7 47.52 9.07 19 -1 7 33.28 7.20 19 -1 7 31.37 7.76 19 1 7 18.72 6.08 19 -1 8 13.10 4.96 19 -1 8 11.49 4.23 19 1 8 14.41 3.88 19 1 8 22.65 5.99 19 -1 9 13.78 4.82 19 -1 9 6.93 3.49 19 1 9 12.22 5.05 19 1 9 24.54 7.38 19 -1 10 85.67 12.41 19 1 10 71.28 10.74 19 -1 10 92.49 12.50 19 -1 11 38.25 8.05 19 -1 11 47.80 9.69 19 1 11 36.52 7.68 19 -1 12 4.11 2.56 19 -1 12 8.58 3.40 19 1 12 4.54 5.70 19 -2 -11 10.01 3.89 19 -2 -10 9.99 4.68 19 -2 -9 11.71 4.95 19 -2 -9 1.78 2.58 19 -2 -8 0.51 2.71 19 -2 -8 5.31 3.17 19 -2 -7 15.66 5.68 19 -2 -7 23.03 7.36 19 2 -7 13.34 5.07 19 -2 -6 36.45 8.55 19 -2 -6 26.46 7.39 19 2 -6 20.03 6.19 19 -2 -5 30.99 6.73 19 -2 -5 22.16 6.91 19 2 -5 18.58 5.78 19 -2 -4 13.49 5.35 19 2 -4 5.77 4.55 19 -2 -4 11.61 4.99 19 2 -4 24.13 6.82 19 -2 -3 10.08 4.25 19 2 -3 10.46 4.85 19 -2 -3 6.51 4.65 19 2 -3 21.64 7.95 19 2 -3 8.01 3.69 19 -2 -2 6.02 4.19 19 2 -2 2.47 2.13 19 -2 -2 2.34 3.43 19 2 -2 9.37 3.63 19 2 -2 2.24 2.08 19 -2 -1 5.89 3.34 19 2 -1 6.37 2.90 19 -2 -1 9.17 4.70 19 2 -1 6.61 5.25 19 2 -1 7.61 4.44 19 -2 0 12.26 5.18 19 -2 0 11.60 5.13 19 2 0 4.00 2.86 19 2 0 3.39 2.85 19 2 0 9.84 3.53 19 -2 1 8.29 3.41 19 -2 1 11.26 5.74 19 2 1 5.98 3.16 19 2 1 3.47 2.96 19 2 1 9.74 3.68 19 -2 2 1.96 2.48 19 2 2 3.33 2.77 19 2 2 4.05 2.62 19 2 2 3.27 3.97 19 -2 3 10.23 4.29 19 -2 3 6.81 4.84 19 2 3 14.54 6.41 19 2 3 6.23 4.05 19 2 3 8.19 3.71 19 -2 4 12.63 5.18 19 -2 4 9.21 2.87 19 2 4 15.90 5.74 19 2 4 9.65 2.94 19 2 4 12.45 3.76 19 -2 5 31.34 6.91 19 -2 5 35.37 8.15 19 2 5 15.61 5.65 19 2 5 18.39 5.39 19 2 5 21.25 6.62 19 -2 6 27.30 6.23 19 -2 6 18.60 5.26 19 2 6 28.40 7.07 19 2 6 14.67 4.76 19 2 6 19.48 5.98 19 -2 7 16.96 5.51 19 -2 7 20.04 6.28 19 2 7 9.73 5.95 19 2 7 9.08 4.82 19 2 7 23.00 6.79 19 -2 8 3.11 2.32 19 -2 8 2.52 3.18 19 2 8 2.69 2.81 19 2 8 3.52 2.39 19 2 8 8.45 4.43 19 -2 9 0.54 3.09 19 -2 9 1.77 3.18 19 2 9 3.73 3.06 19 -2 10 7.91 3.57 19 -2 10 6.33 3.62 19 2 10 3.29 3.14 19 -2 11 4.11 3.44 19 -2 11 10.22 5.27 19 2 11 8.19 3.08 19 -3 -9 8.15 4.39 19 -3 -9 8.02 2.75 19 3 -9 11.09 5.04 19 -3 -8 35.37 8.15 19 -3 -8 27.84 7.37 19 3 -8 26.29 7.29 19 -3 -7 0.80 2.40 19 -3 -7 9.98 5.18 19 3 -7 14.03 5.44 19 -3 -6 6.78 3.53 19 -3 -6 10.24 3.56 19 3 -6 10.72 4.52 19 -3 -5 2.32 2.84 19 -3 -5 17.62 5.86 19 3 -5 14.94 4.81 19 -3 -4 6.00 4.13 19 -3 -4 8.73 4.92 19 3 -4 6.30 3.32 19 -3 -3 5.39 3.07 19 -3 -3 10.13 4.18 19 3 -3 4.76 2.76 19 3 -3 12.37 4.24 19 -3 -2 31.16 8.21 19 -3 -2 20.94 6.22 19 3 -2 10.51 3.01 19 3 -2 22.11 6.54 19 -3 -1 9.66 4.78 19 -3 -1 0.58 2.51 19 3 -1 15.47 5.45 19 3 -1 15.33 6.07 19 -3 0 7.38 4.09 19 -3 0 -0.34 2.57 19 3 0 2.51 2.83 19 3 0 -1.78 2.06 19 -3 1 9.09 4.80 19 -3 1 5.88 4.20 19 3 1 15.03 5.05 19 3 1 8.62 4.31 19 -3 2 10.82 4.62 19 -3 2 6.42 2.20 19 3 2 17.18 6.48 19 3 2 11.80 4.06 19 -3 3 6.57 1.49 19 -3 3 10.84 5.57 19 3 3 8.33 6.62 19 3 3 10.93 4.69 19 3 3 12.29 5.50 19 -3 4 8.71 2.54 19 -3 4 2.65 4.21 19 3 4 11.38 5.26 19 3 4 7.61 4.26 19 3 4 11.77 4.44 19 3 5 18.60 5.80 19 -3 5 18.11 4.92 19 -3 5 15.07 4.34 19 3 5 12.61 4.40 19 3 5 15.86 5.15 19 3 6 3.75 2.95 19 -3 6 15.50 5.34 19 -3 6 19.80 6.80 19 3 6 10.71 4.86 19 3 6 25.46 7.56 19 3 7 7.67 4.52 19 -3 7 10.87 4.19 19 -3 7 4.56 3.12 19 3 7 8.31 4.00 19 3 7 3.76 2.51 19 3 8 30.54 6.36 19 -3 8 34.29 8.22 19 -3 8 42.02 9.34 19 3 8 29.44 8.09 19 3 9 8.99 4.78 19 -3 9 21.43 6.57 19 -3 9 8.87 5.80 19 3 9 25.33 7.85 19 -4 -6 2.67 3.88 19 -4 -6 2.80 4.52 19 4 -6 2.85 3.73 19 -4 -5 0.49 2.72 19 -4 -5 1.42 2.39 19 4 -5 -2.10 3.25 19 -4 -4 4.91 3.06 19 -4 -4 11.12 5.68 19 4 -4 10.40 3.80 19 -4 -3 10.19 5.93 19 -4 -3 10.95 3.13 19 4 -3 5.58 2.08 19 -4 -2 3.00 2.25 19 -4 -2 21.44 6.32 19 4 -2 15.49 5.37 19 -4 -1 -0.68 1.94 19 -4 -1 2.34 2.45 19 4 -1 -1.75 2.20 19 4 -1 -0.37 3.59 19 -4 0 5.92 3.77 19 -4 0 0.03 2.72 19 4 0 8.17 4.99 19 4 0 11.16 4.67 19 4 1 1.69 2.20 19 -4 1 1.42 2.55 19 -4 1 1.39 2.22 19 4 1 0.47 1.78 19 4 2 16.00 5.34 19 -4 2 6.83 4.52 19 -4 2 9.57 4.76 19 4 2 4.55 2.99 19 4 3 4.50 4.04 19 -4 3 9.74 4.36 19 -4 3 10.55 6.99 19 4 3 7.59 4.72 19 4 4 11.09 5.54 19 -4 4 4.25 4.39 19 -4 4 10.18 5.38 19 4 4 7.02 3.87 19 4 5 -1.88 3.99 19 -4 5 -1.29 2.96 19 -4 5 1.53 4.23 19 4 5 5.80 4.90 19 4 6 0.76 2.51 19 -4 6 2.83 3.06 19 -4 6 3.94 3.47 19 4 6 11.75 5.53 20 0 -7 7.60 2.90 20 0 -6 -2.12 4.53 20 0 -6 -2.24 3.09 20 0 -5 84.76 12.28 20 0 -5 77.28 11.07 20 0 -4 206.45 19.21 20 0 -4 219.42 20.02 20 0 -3 8.38 3.82 20 0 -3 -1.31 3.47 20 0 -2 295.11 22.04 20 0 -2 303.24 23.72 20 0 -1 24.11 6.55 20 0 -1 14.30 5.17 20 0 0 0.19 3.77 20 0 0 -1.80 3.55 20 0 1 31.68 7.70 20 0 1 12.28 4.57 20 0 2 261.03 20.64 20 0 2 274.41 22.60 20 0 3 -0.50 2.30 20 0 3 3.67 3.03 20 0 4 218.31 18.79 20 0 4 229.55 19.89 20 0 5 84.55 12.40 20 0 5 93.77 13.07 20 0 6 -1.58 2.16 20 0 6 -0.64 3.15 20 0 7 3.82 3.17 20 0 7 8.72 4.88 20 -1 -7 -1.29 5.02 20 -1 -7 1.08 2.25 20 -1 -6 4.66 4.15 20 -1 -6 -1.26 2.63 20 1 -6 1.11 2.78 20 -1 -5 10.07 4.91 20 1 -5 4.44 2.65 20 -1 -5 8.42 4.59 20 1 -5 9.57 5.29 20 -1 -4 -1.94 3.43 20 1 -4 -1.40 2.34 20 -1 -4 -1.19 3.98 20 1 -4 3.42 3.20 20 -1 -3 22.96 5.78 20 1 -3 21.03 6.51 20 -1 -3 17.16 6.19 20 1 -3 5.78 5.15 20 -1 -2 10.36 4.92 20 1 -2 4.70 2.57 20 -1 -2 7.24 4.26 20 1 -2 0.56 3.09 20 -1 -1 4.49 2.07 20 1 -1 5.34 3.43 20 -1 -1 1.02 3.39 20 1 -1 11.02 4.88 20 -1 0 2.30 3.91 20 1 0 3.16 4.17 20 -1 0 3.44 3.99 20 1 0 4.34 4.91 20 -1 1 4.52 4.28 20 1 1 11.82 4.27 20 -1 1 5.41 3.90 20 1 1 3.38 3.19 20 -1 2 4.94 3.87 20 1 2 9.70 5.80 20 -1 2 5.87 3.61 20 1 2 1.68 4.53 20 -1 3 24.71 6.76 20 1 3 15.74 5.81 20 -1 3 31.16 7.81 20 1 3 11.01 4.60 20 -1 4 0.89 2.36 20 1 4 0.43 1.83 20 -1 4 0.05 2.46 20 1 4 -3.22 4.15 20 -1 5 4.98 2.58 20 1 5 5.36 3.54 20 1 5 3.80 3.71 20 -1 6 -1.78 2.26 20 1 6 2.09 3.93 20 -1 6 1.28 2.94 20 1 6 -1.49 3.31 20 -1 7 0.72 1.85 20 1 7 -0.88 1.90 20 -1 7 2.67 2.90 20 1 7 1.55 3.21 20 -2 -5 3.47 3.64 20 -2 -5 1.40 3.24 20 -2 -4 24.58 7.11 20 -2 -4 16.66 5.86 20 -2 -3 4.40 3.75 20 2 -3 5.65 4.36 20 -2 -3 4.10 2.65 20 2 -3 5.88 2.93 20 -2 -2 115.29 14.12 20 2 -2 104.43 13.18 20 -2 -2 102.69 13.60 20 2 -2 92.44 12.72 20 -2 -1 18.70 6.08 20 2 -1 7.80 4.83 20 -2 -1 8.86 5.31 20 2 -1 0.08 2.75 20 2 -1 7.08 4.47 20 -2 0 1.20 2.67 20 2 0 -1.48 3.11 20 -2 0 2.24 4.08 20 2 0 0.45 2.19 20 2 0 -0.17 3.20 20 -2 1 3.89 3.55 20 -2 1 7.65 3.45 20 2 1 8.03 4.55 20 2 1 -0.26 3.60 20 -2 2 94.49 12.85 20 2 2 97.45 12.76 20 -2 2 99.68 14.04 20 2 2 94.54 13.59 20 2 2 98.27 12.68 20 -2 3 3.32 2.95 20 -2 3 5.59 2.07 20 2 3 4.55 2.89 20 2 3 3.51 2.40 20 2 3 6.82 4.80 20 -2 4 24.88 5.58 20 -2 4 36.52 8.34 20 2 4 8.61 4.96 20 2 4 15.24 4.45 20 2 4 23.90 5.44 20 -2 5 3.10 3.09 20 -2 5 5.08 5.01 20 2 5 6.84 4.17 20 2 5 3.36 3.86 20 2 5 1.42 3.32 0 0 0 0.00 0.00 TITL 010_220K_SulfamerazineF1_ in Pna2(1) REM Pna2(1) (#33, found as Pbn2(1) in ba-c setting) CELL 0.68890 14.479456 8.197422 21.869257 90.0000 90.0000 90.0000 ZERR 8.00 0.000121 0.000076 0.000266 0.0000 0.0000 0.0000 LATT -1 SYMM -x,-y, z+1/2 SYMM x+1/2,-y+1/2, z SYMM -x+1/2, y+1/2, z+1/2 SFAC C H N O S UNIT 88.00 96.00 32.00 16.00 8.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 83722