Raw data files for XRD, HPLC, UV dosage, ICPMS, Eeo, MicroCT and hydrodynamic calculations associated with manuscript titled "Synthesis of Photocatalytic Pore Size-Tuned ZnO Molecular Foams" XRD contains raw data of XRD spectra used to analyse crystallinity and crystal phase of ZnO samples. HPLC contains the raw data used to produce degradation profiles of carbamazepine when exposed to the photocatalyst. UV dosage contains the raw data used to plot degradation against UV irradiation supplied to allow for greater analysis between flow rates of reactor. ICPMS contains the raw data collected to analyse the concentration of metal in the pollutant stream, allowing for analysis of material stability. Eeo contains the calculations used to work out the electrical energy efficiency of the system, allowing for analysis of efficiency when operating the reactor under different conditions. MicroCT is the raw data collected from analysis of the 3D reconstruction of the samples, used to analyse the pore structure (size, sphericity, ect) Hydrodynamic calculations contains the calculations conducted to understand the reactor system and to calculate key parameters allowing for the discussion of the reactor.