Dataset supporting "In situ X-ray reflectivity and GISAXS study of mesoporous silica films grown from sodium silicate solution precursors"

1151 41 16052 5 53336 document 16052 DLS.pxp application/octet-stream 106e3bb00c2810e6219ef108f97aef24 MD5 96018 2022-05-30 10:12:13 https://researchdata.bath.ac.uk/1151/1/DLS.pxp 1151 1 1 application/octet-stream other Dynamic light scattering data en public cc_by

DLS.pxp

data 16053 4 53340 document 16053 small-angle-X-ray-scattering-lab-based-SAXS.7z application/x-7z-compressed d9a7c523bcd6decf98d8c438efabcd6b MD5 551045 2022-05-30 10:26:45 https://researchdata.bath.ac.uk/1151/2/small-angle-X-ray-scattering-lab-based-SAXS.7z 1151 2 2 application/x-7z-compressed other Small angle X-ray scattering data (lab-based) en public cc_by

small-angle-X-ray-scattering-lab-based-SAXS.7z

data 16054 4 53342 document 16054 TGA-data.7z application/x-7z-compressed 7206bee5f2b1e1bd07a08c6686d8bc42 MD5 125360 2022-05-30 12:08:42 https://researchdata.bath.ac.uk/1151/3/TGA-data.7z 1151 3 3 application/x-7z-compressed other Thermogravimetric analysis data en public cc_by

TGA-data.7z

data 16055 4 53344 document 16055 XRR-data.7z application/x-7z-compressed 4048fcdeb263d0531e283c92042892e4 MD5 161056 2022-05-30 12:10:16 https://researchdata.bath.ac.uk/1151/4/XRR-data.7z 1151 4 4 application/x-7z-compressed other In-situ X-ray reflectivity data en public cc_by

XRR-data.7z

data 16056 4 53346 document 16056 surface-pressure-data.7z application/x-7z-compressed e18960e2d00134270814cd9bf2f63eb4 MD5 4833364 2022-05-30 12:10:49 https://researchdata.bath.ac.uk/1151/5/surface-pressure-data.7z 1151 5 5 application/x-7z-compressed other Surface pressure data en public cc_by

surface-pressure-data.7z

data 16057 4 53348 document 16057 GISAXS-data.7z application/x-7z-compressed 299d4a4b0fd0c967fc323cc6acd11775 MD5 21103400 2022-05-30 12:11:38 https://researchdata.bath.ac.uk/1151/6/GISAXS-data.7z 1151 6 6 application/x-7z-compressed other Grazing incidence X-ray scattering data en public cc_by

GISAXS-data.7z

data 16058 3 53350 document 16058 N2-isotherm.7z application/x-7z-compressed 4708331a30b4ea2de8dc0033ea3a7392 MD5 17565 2022-05-30 12:12:17 https://researchdata.bath.ac.uk/1151/7/N2-isotherm.7z 1151 7 7 application/x-7z-compressed other Nitrogen sorption data en public cc_by

N2-isotherm.7z

data archive 513 disk0/00/00/11/51 2022-06-01 12:24:52 2024-07-22 10:52:28 2022-06-01 12:24:52 data_collection show Di Andi A.Di@bath.ac.uk 0000-0003-4527-2504 University of Bath FALSE Schmitt Julien J.M.F.Schmitt@bath.ac.uk 0000-0002-3452-6655 University of Bath; French National Centre for Scientific Research FALSE Elstone Naomi N.Elstone@bath.ac.uk 0000-0003-0176-1445 University of Bath FALSE Arnold Thomas tom.arnold@esss.se 0000-0001-7196-7831 Diamond Light Source; European Spallation Source FALSE Edler Karen K.Edler@bath.ac.uk 0000-0001-5822-0127 University of Bath TRUE Dataset supporting "In situ X-ray reflectivity and GISAXS study of mesoporous silica films grown from sodium silicate solution precursors" dept_chem small angle scattering, silica film, air-solution interface, X-ray reflectivity, grazing incidence small angle scattering SAXS data has three columns: Q (x axis), scattering intensity (y axis) and error for scattering intensity. GISAXS data are images. XRR data has three columns: Q as x axis, reflectivity (y axis) and error in y axis. Surface pressure data contains two columns: time and surface pressure. This dataset includes data relating to mesoporous silica films grown from sodium silicate solution precursors: dynamic light scattering (DLS) data for solutions containing cetrimonium bromide and sodium nitrate; small angle X-ray scattering (SAXS) data for films contain cetyltrimethylammonium bromide (CTAB), silica and polyethylenimine (PEI), and silica film; thermogravimetric analysis (TGA) data recording the decomposition of CTAB–PEI–silica in air with temperature; in-situ X-ray reflectivity (XRR) data, surface pressure data, and grazing incidence X-ray scattering (GISAXS) data for the interface between the solution (sodium silicate, CTAB, PEI) and air; and nitrogen sorption data. 2022-05-25 University of Bath public RightsHolder University of Bath Engineering and Physical Sciences Research Council https://doi.org/10.13039/501100000266 EP/L016354/1 EPSRC Centre for Doctoral Training in Sustainable Chemical Technologies China Scholarship Council https://doi.org/10.13039/501100004543 PhD Studentship Full details of the methodology can be found in the Experimental section of the associated paper. The XRR data were normalised. All the data are plotted in Igor Pro software, https://www.wavemetrics.com/. https://doi.org/10.1016/j.micromeso.2022.112018 en 1 10.15125/BATH-01151 https://doi.org/10.1016/j.micromeso.2022.112018 pub