Raw data files for X-ray diffraction (XRD), high-performance liquid chromatography (HPLC) alongside data and calculations of quantum yield (QY), electrical energy per order (EEO) end measured UV lamp irradiance associated with the paper "Fast Sintering of Titania Monoliths for Photocatalytic Degradation of Organic Micropollutants". XRD contains raw data of XRD spectra. HPLC contains the raw data used to produce degradation profiles of primidone when exposed to the photocatalyst.