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        <formatdesc>Electrochemical movies for the PhD Thesis of Thom Harris-Lee, as part of supporting information for Chapter 6.</formatdesc>
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          <given>T. R.</given>
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        <orcid>0000-0002-7783-1537</orcid>
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    <title>Dataset for &quot;Systematic Design and Characterisation of Photoelectrodes for Light-Driven Water Splitting&quot;, a PhD Thesis</title>
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      <item>CA0030</item>
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    <keywords>Electrochemical activity movies, hydrogen evolution catalysis</keywords>
    <abstract>Electrochemical activity movies obtained by scanning electrochemical cell microscopy (SECCM) of a porous a-MoSx thin film. The dataset contains short movies denoted Movie S1-S13, consisting of independent SECCM scans on the a-MoSx film, covering homogeneous and heterogeneous areas to characterise the local structure-activity relationship with respect to total (current) and specific (current density) electrochemical activity.</abstract>
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    <collection_method>Scanning electrochemical cell microscopy (SECCM) scans using voltammetric hopping mode, 500 nm diameter nanopipettes filled with 0.5 M H2SO4, with a Ag/AgCl QRCE, measuring an electrodeposited a-MoSx thin film WE.</collection_method>
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