Dataset for Structural and optical emission uniformity of m-plane InGaN single quantum wells in core-shell nanorods

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GaN_Nanorod_template_cross_section.bmp

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GAN_Nanorod_template_planar.bmp

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Faceted_GaN_Nanorod_cross_section.bmp

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Faceted_GaN_Nanorod_planar.bmp

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TEM_image_HAADF__cplane_and_semipolar.bmp

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TEM_image_HAADF__semipolar_and_top.bmp

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TEM_image_HAADF__top.bmp

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TEM_image_HAADF__middle.bmp

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TEM_image_HAADF__base.bmp

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fig4a_InN_content_map_semipolarplane_650degC.xlsx

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fig4b_InN_content_map_mplane_700degC.xlsx

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fig4c_InN_content_map_mplane_650degC.xlsx

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fig5b_Mean_InN_content_and_error_650degC_semipolar.xlsx

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fig5c_Mean_InN_content_and_error_700degC.xlsx

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fig5d_Mean_InN_content_and_error_650degC.xlsx

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Fig6a_SEM_image_750degC.tif

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Fig6b_SEM_image_700degC.tif

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Fig6c_SEM_image_650degC.tif

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fig6d_rawdata.txt

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fig6e_rawdata.txt

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fig6f_rawdata.txt

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fig6g_rawdata.txt

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fig6h_rawdata.txt

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fig6i_rawdata.txt

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Fig6j_meanspectrum_alltemp.xlsx

data 2414 2 5849 document 2414 Fig6k_Rodtoroduniformity_700deg.xlsx application/vnd.openxmlformats-officedocument.spreadsheetml.sheet f916d2e2d174a9d4a0d33fdf6b07ce88 MD5 108473 2016-02-12 12:38:28 https://researchdata.bath.ac.uk/150/43/Fig6k_Rodtoroduniformity_700deg.xlsx 150 43 43 application/vnd.openxmlformats-officedocument.spreadsheetml.sheet other Figure 6 k): Raw data related to the m-plane emission peak of multiple individual nanorods for samples grown 700°C en public cc_by

Fig6k_Rodtoroduniformity_700deg.xlsx

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Fig6l_Rodtoroduniformity_650deg.xlsx

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Fig7a_linescan_mplane750deg_CL_3745_43_31_43_132.txt

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Fig7b_linescan_mplane700deg_CL_3831_53_11_55_39.txt

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Fig7c_linescan_mplane650deg_CL_3833_px_119_0_130_70.txt

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Fig7d_resonance_raw_data.xlsx

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fig8a_750deg_rawdata.xlsx

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fig8b_700deg_rawdata.xlsx

data 2467 2 5912 document 2467 fig8c_650deg_rawdata.xlsx application/vnd.openxmlformats-officedocument.spreadsheetml.sheet ed9b7a6cae563957a803a564ddbff321 MD5 13538 2016-02-12 14:12:11 https://researchdata.bath.ac.uk/150/96/fig8c_650deg_rawdata.xlsx 150 96 96 application/vnd.openxmlformats-officedocument.spreadsheetml.sheet other Figure 8 a): Raw data centroid emission energy measured along the length of several nanorod m-plane facets for growth at 650°C taken at room temperature en public cc_by

fig8c_650deg_rawdata.xlsx

data 2468 2 5915 document 2468 Fig9_rawdata.xlsx application/vnd.openxmlformats-officedocument.spreadsheetml.sheet 34f873c61fc9aa6d54626f5c810bf22b MD5 12501 2016-02-12 14:20:06 https://researchdata.bath.ac.uk/150/97/Fig9_rawdata.xlsx 150 97 97 application/vnd.openxmlformats-officedocument.spreadsheetml.sheet other InN fraction obtained from EDX map and Vegard's law raw data used to plot figure 9 en public cc_by

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Fig3e_HRTEM_700degC.bin.tif

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Fig3e_inset_HRTEM_fourier_transform.tif

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http://eprints.org/relation/isVersionOf https://researchdata.bath.ac.uk/id/document/2559 http://eprints.org/relation/isVolatileVersionOf https://researchdata.bath.ac.uk/id/document/2559 http://eprints.org/relation/issmallThumbnailVersionOf https://researchdata.bath.ac.uk/id/document/2559 archive 3087 disk0/00/00/01/50 2016-03-03 13:05:38 2024-10-05 04:47:26 2016-03-03 13:05:38 data_collection show Le Boulbar Emmanuel elb43@bath.ac.uk 0000-0001-6364-3976 University of Bath TRUE Hosseini Vajargah Shahrzad ~Shahrzad-HosseiniVajargah@cam.ac.uk University of Cambridge FALSE Edwards Paul 0000-0001-7671-7698 University of Strathclyde FALSE Griffiths Ian 0000-0001-7303-1375 University of Bristol FALSE Girgel Ionut I.Girgel@bath.ac.uk University of Bath FALSE Coulon Pierre-Marie P.Coulon@bath.ac.uk 0000-0002-9120-7554 University of Bath FALSE Cherns David d.cherns@bristol.ac.uk University of Bristol FALSE Martin Robert W. r.w.martin@strath.ac.uk 0000-0002-6119-764X University of Strathclyde FALSE Humphreys Colin J. colin.humphreys@msm.cam.ac.uk University of Cambridge FALSE Bowen Chris C.R.Bowen@bath.ac.uk 0000-0002-5880-9131 University of Bath FALSE Allsopp Duncan D.Allsopp@bath.ac.uk 0000-0003-4197-9852 University of Bath FALSE Shields Philip P.Shields@bath.ac.uk 0000-0003-0517-132X University of Bath FALSE Researcher Shields Philip P.Shields@bath.ac.uk 0000-0003-0517-132X University of Bath Researcher Allsopp Duncan D.Allsopp@bath.ac.uk 0000-0003-4197-9852 University of Bath Researcher Martin Robert W. r.w.martin@strath.ac.uk 0000-0002-6119-764X University of Strathclyde Researcher Edwards Paul 0000-0001-7671-7698 University of Strathclyde Researcher Cherns David d.cherns@bristol.ac.uk University of Bristol Dataset for Structural and optical emission uniformity of m-plane InGaN single quantum wells in core-shell nanorods EA0040 GE0030 GE0040 HH0050 KF0010 dept_elec_eng This dataset contains the results of scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Energy Dispersive X-ray (EDX) measurements carried out on InGaN/GaN core-shell nanostructures. The samples are highly regular arrays of GaN plasma etched cores onto which wide InGaN layer capped with a GaN layer were grown using different metal organic vapour phase epitaxy (MOVPE) growth parameters. Three different growth temperature were used to grow the InGaN layer: 750°C, 700°C and 650°C. SEM images were used to characterize the describe the fabrication, growth and assess nanorod morphologies. TEM were used to investigate the structural properties and assess the InGaN thickness along the entire length of the m-plane facets. EDX measurements were used to assess the homogeneity of the InGaN layer composition at different position along the m-plane facet and on the semi-polar facets. 2016-03-03 University of Bath public Controlling the long-range homogeneity of core-shell InGaN/GaN layers is essential for their use in light-emitting devices. Understanding the impact of the crystallographic arrangement and material composition on light emission at a nanometer scale is a key feature for the fabrication of efficient light emitting devices. We investigated the structural quality and composition of the material via Transmission Electron microscopy (TEM) and Energy Dispersive X-ray (EDX) spectroscopy. The light emission were qualitatively assessed via Hyperspectral Cathodolumiscence (CL) spectroscopy. We use these information to determine the impact of the composition inhomogeneities on light emission. We have found that a homegeneous long-range light emission can be achieved on InGaN/GaN core-shell structure despite the presence of nano-scale alloy compositional fluctuations. RightsHolder University of Bath Engineering and Physical Sciences Research Council https://doi.org/10.13039/501100000266 EP/M022862/1 Manufacturing of Nano-Engineered III-N Semiconductors - Equipment Engineering and Physical Sciences Research Council https://doi.org/10.13039/501100000266 EP/I012591/1 Lighting the Future Seventh Framework Programme https://doi.org/10.13039/501100004963 320963 NEMESIS - Novel Energy Materials: Engineering Science and Integrated Systems Secondary electron images were captured using a Hitachi S-4300 scanning electron microscope (SEM). An accelerating voltage of 5 kV was used to collect the images. Atomic resolution STEM images were acquired using a FEI TITAN 80-300 microscope that was equipped with a CEOS CESCOR spherical aberration (Cs) corrector in the probe forming lens and high-brightness FEI XFEG electron source. Atomic resolution HAADF STEM images were acquired at an accelerating voltage of 300 keV and probe convergence semi-angle of 17.9 mrad and col-lection semi-angle of 55-200 mrad. Energy dispersive X-Ray spectroscopy analyses were carried out using FEI Tecnai Osiris. This microscope was equipped with XFEG and Super X system EDS detectors. This detector comprises 4 Bruker silicon detectors (SDD) arranged symmetrically around the optic axis of the microscope for high collection efficiency and high count rate. Spectrum images were acquired at a spatial sampling of 2 nm/pixel and 1 s/pixel dwell times with a probe current of approximately 0.5 nA, at an accelerating voltage of 200 keV. Samples for TEM were prepared by a dual beam focused ion beam system. The nanorods were protected by a platinum layer prior to etching to reduce damage that could occur with the use of ion beam system. The samples for EDX measurements and atomic resolution STEM were prepared by a tripod polishing method using an Allied Tech Multiprep unit. Specimens were then ion-milled with a Gatan Precision Ion Polishing System (PIPS) using 1.5–5 keV argon ions for further thinning and removing the residue of polishing contamination from the specimens. Using principal component analysis and independent component analysis (implemented in HyperSpy46), two independent and uncorrelated components were identified in the spectrum images. The first component contains Ga and N X-ray peaks and the second component contain Ga, In, and N X-ray peaks. To obtain the composition of the InGaN shell, the intensities of Ga Kalpha and In Lalpha peaks were quantified using the Cliff-Lorimer method and the k-factor provided by the manufacturer of the EDX system (Bruker). The errors were also estimated from Poisson statistics. Hitachi S-4300 scanning electron microscope (SEM) en 1 10.15125/BATH-00150 https://doi.org/10.1021/acs.cgd.5b01438 pub open