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    <title>Dataset for Investigation of InGaN facet-dependent non-polar growth rates and composition for core-shell LEDs</title>
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      <item>GE0030</item>
      <item>GE0040</item>
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    <abstract>This dataset contains the results of scanning electron microscopy (SEM) and transmission electron microscopy (TEM) measurements carried out on core-shell nanostructures. The samples are highly regular arrays of GaN plasma etched cores onto which thick InGaN layers were grown using different metal organic vapour phase epitaxy (MOVPE) growth parameters. 
 
Three different InGaN growth conditions were considered with the following parameters: 750°C at 300 mbar, 700°C at 300 mbar and 750°C at 100 mbar. Statistical growth rates were determined on the non-polar crystal planes from measurements of increase in diameter using SEM images. TEM analysis was carried out on a single nanorod for greater detail.</abstract>
    <date>2016-01-27</date>
    <publisher>University of Bath</publisher>
    <full_text_status>public</full_text_status>
    <lay_summary>Core-shell InGaN/GaN structures are attractive as light emitters due to their potential for emission on large non-polar surface area and flexibility in achieving different emission wavelengths with changing growth parameters. The morphology and dimensional dependence of InGaN layers with growth parameters were investigated by scanning electron microscopy (SEM) and transmission electron microscopy (TEM).  Growth rates for InGaN under different growth parameters for the non-polar a- and m-planes were determined.</lay_summary>
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    <funding>
      <item>
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        <funder_id>https://doi.org/10.13039/501100004963</funder_id>
        <grant_id>228999</grant_id>
        <project_name>SMASH: Smart Nanostructured Semiconductors for Energy-Saving Light Solutions</project_name>
      </item>
      <item>
        <funder_name>Engineering and Physical Sciences Research Council</funder_name>
        <funder_id>https://doi.org/10.13039/501100000266</funder_id>
        <grant_id>EP/I012591/1</grant_id>
        <project_name>Lighting the Future</project_name>
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    <collection_method>Secondary electron images were captured using a Hitachi S-4300 scanning electron microscope (SEM).  An accelerating voltage of 5 kV was used to collect the images at constant magnification of 6000x from 5 samples, corresponding to a plasma etched GaN template, a GaN regrowth and three InGaN growths. Approximately 80 individual nanorods and their diameters are identified in each image. 

Each image was processed by binary threshold and low pass filter in Vision Assistant 2011 to obtain individual nanorod dimensions as detailed in the *.xls files. Each xls file contains separate columns for object number, calibrated area, equivalent disk diameter and image area. Statistical distributions of diameters were determined. 

A planar cross section was prepared for TEM measurements using a focused ion beam to thin down the cross section to 100-200 nm thickness. 
A Tecnai Osiris scanning-TEM (STEM) operating at 200 kV was used to obtain a high-angle annular dark-field (HAADF) Z-contrast image. The same image processing as in the SEM images was used to determine diameters and InGaN shell thickness.</collection_method>
    <techinfo>Hitachi S-4300 scanning electron microscope (SEM) 
Focused Ion Beam (FIB) etching and platinum deposition 
Tecnai Osiris scanning transmission electron microscope (STEM)</techinfo>
    <language>en</language>
    <version>1</version>
    <doi>10.15125/BATH-00172</doi>
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    <access_arrangements>All data are available under a Creative Commons Attribution 4.0 (CC-BY) licence.</access_arrangements>
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