376 27 6583 2 16516 document 6583 Data.zip application/zip 24853ad8828815877bea35bcc671c17a MD5 8010628 2017-06-06 13:51:31 https://researchdata.bath.ac.uk/376/1/Data.zip 376 1 1 application/zip other en public cc_by

Data.zip

data archive 5553 disk0/00/00/03/76 2017-06-26 11:55:52 2024-07-16 15:37:09 2017-06-26 11:55:52 data_collection show Hammond Oliver O.S.Hammond@bath.ac.uk 0000-0002-5612-9343 University of Bath TRUE Edler Karen K.Edler@bath.ac.uk 0000-0001-5822-0127 University of Bath FALSE Eslava Salvador S.Eslava@bath.ac.uk 0000-0002-2416-3205 University of Bath FALSE dept_chem_eng dept_chem Nanostructures, Sustainable Chemistry, Water Splitting, Hydrogen Evolution, Deep Eutectic Solvents, Ionic Liquids, Iron oxide, Photoelectrochemistry This dataset contains freely-available raw data in support of the named article (10.1039/C7TA02078C), including data from powder X-Ray diffraction, magnetometry measurements, Raman spectroscopy, wide-angle X-Ray scattering performed at the I22 beamline of Diamond Light Source, and photoelectrochemical measurements. 2017-06-05 University of Bath public Data from measurements of the physical and chemical properties of some prepared nanomaterials are provided here, and openly-accessible, for interested researchers. RightsHolder University of Bath Science and Technology Facilities Council https://doi.org/10.13039/501100000271 3578 ISIS Studentship Agreement Engineering and Physical Sciences Research Council https://doi.org/10.13039/501100000266 EP/P008097/1 Nanostructured Metal Oxides for Solar Fuels Engineering and Physical Sciences Research Council https://doi.org/10.13039/501100000266 EP/L016354/1 EPSRC Centre for Doctoral Training in Sustainable Chemical Technologies WAXS: Data were collected on pure, and heat-treated DES samples, using the wide-angle detector at the I22 instrument of Diamond Light Source, UK. Samples were measured in glass capillaries at 30 C. XRD: Diffraction data of the prepared powders were collected using a Bruker D8-ADVANCE instrument provided by the University of Bath CCAF. Magnetometry: M(H) and M(T) measurements of the prepared solids were made using either a Quantum Design PPMS Vibrating Sample Magnetometer, or a Quantum Design MPMS-XL SQUID Magnetometer. Photoelectrochemistry: PEC measurements were made of the prepared photoanodes using an in-house solar simulator and a three-electrode cell. Full details of data collection methodology are given in the article. WAXS data were treated using the DAWN software suite, with the following processing steps performed: - Detector calibration - Masking - Calculation of errors - Azimuthal reduction (I vs q reduction) - Division by I(t) (Transmitted intensity) - Multiplication by I(0) (Primary beam intensity) - Background subtraction No significant processing steps can be reported for the other data givenhere, other than basic background subtraction (XRD), and normalisation to either the sample mass (magnetometry measurements) or the sample area (PEC measurements) Where possible, all data has been provided as tab-delimited text files. Due to the large volume of data, the magnetometry data has been provided as a collection of Microsoft Excel sheets. 2016-10-01 2017-03-03 en 1 10.15125/BATH-00376 https://doi.org/10.1039/C7TA02078C pub open