762 50 12978 4 37893 document 12978 Fig.2 (SANS).zip application/zip 62a09b107fe5d979e154caacd4a9be85 MD5 23261 2020-01-08 11:52:51 https://researchdata.bath.ac.uk/762/1/Fig.2%20%28SANS%29.zip 762 1 1 application/zip other The zip file named “Fig.2 (SANS)” contains txt files for each sample measured in Small angle neutron scattering (SANS). en public cc_by

Fig.2 (SANS).zip

data 12979 4 37895 document 12979 Fig.5_FigS3_FigS4.zip application/zip a3a0ee8899c58ecdd28e66f1706dd94c MD5 82938 2020-01-08 11:52:57 https://researchdata.bath.ac.uk/762/2/Fig.5_FigS3_FigS4.zip 762 2 2 application/zip other (i) Gamma_vs_time: Data for the sinusoidal deformation (gamma in (%) as function of time (s) (ii) Lissajous_sigma_vs_shear: Data for the Lissajous-plots as stress (Sigma in (Pa) as function of shear rate (1/s) (iii) Lissajous_sigma_vs_strain: Data for the Lissajous-plots as stress (Sigma in (Pa) as function of strain (gamma in (%)) (iv) Sigma_vs_time: Data for the sinusoidal deformation as stress (Sigma (Pa) as function of time (s) en public cc_by

Fig.5_FigS3_FigS4.zip

data 12980 4 37897 document 12980 Data_filler_Size_Fibrillated_Network.xlsx application/vnd.openxmlformats-officedocument.spreadsheetml.sheet 9d09d665196977dfedd6c647c12924af MD5 213010 2020-01-08 11:53:02 https://researchdata.bath.ac.uk/762/3/Data_filler_Size_Fibrillated_Network.xlsx 762 3 3 application/vnd.openxmlformats-officedocument.spreadsheetml.sheet other Fig. 1(a) shows the Small Angle X-rays Scattering (SAXS) data of the Silica Nanoparticles used in the study Fig. 1(b) contains the data of size distributions for the Silica Nanoparticles used in the study. Fig. 3 contains the rheological data for the time sweep of the OCNF-based gels (data presented as G’, G’’ and tand_delta vs time. Fig.4-6-S5 Show the Oscillatory strain sweep as G’, G’’ and tand_delta vs strain Fig. S1 contains the data for the contrast match experiment. en public cc_by

Data_filler_Size_Fibrillated_Network.xlsx

data archive 7774 disk0/00/00/07/62 2020-02-05 11:11:28 2024-07-15 10:59:20 2020-02-05 11:11:28 data_collection show Calabrese Vincenzo V.Calabrese@bath.ac.uk 0000-0001-5974-9217 University of Bath TRUE Alves Da Silva Marcelo M.Alves.da.Silva@bath.ac.uk 0000-0002-1413-4021 University of Bath FALSE Porcar Lionel 0000-0003-4674-7591 Institut Laue-Langevin FALSE Bryant Saffron S.J.Bryant@bath.ac.uk 0000-0002-7202-3004 University of Bath FALSE Hossain Kazi M. Zakir zh603@bath.ac.uk 0000-0002-4178-7271 University of Bath FALSE Scott Janet L J.L.Scott@bath.ac.uk 0000-0001-8021-2860 University of Bath FALSE Edler Karen K.Edler@bath.ac.uk 0000-0001-5822-0127 University of Bath TRUE CG0030 CP0070 dept_chem In the Excel file named “Data_filler_Size_Fibrillated_Network”, the data are presented in separate sheets, each of which is labelled as for the figure presented in the manuscript. The spreadsheet named: Fig. 1(a) shows the Small Angle X-rays Scattering (SAXS) data of the Silica Nanoparticles used in the study Fig. 1(b) contains the data of size distributions for the Silica Nanoparticles used in the study. Fig. 3 contains the rheological data for the time sweep of the OCNF-based gels (data presented as G’, G’’ and tand_delta vs time). Fig.4-6-S5 Show the Oscillatory strain sweep as G’, G’’ and tand_delta vs strain. Fig. S1 contains the data for the contrast match experiment as SQR(I(q)) vs q . The zip file named “Fig.2 (SANS)” contains txt files for each sample measured in Small angle neutron scattering (SANS). The zip file named “Fig.5_FigS3_FigS4” contains subfolder as: (i) Gamma_vs_time: which contains the data for the sinusoidal deformation (gamma in (%) (left Column)) as function of time (s, (right Column)) for each sample and each amplitude displayed in the Manuscript. The files are named as “NameY-axe_vs_NameX-axe,_sample name_applied amplitude” as for instance “Gamma_vs_time_1wt%OCNF_5wt%SiNp5_gamma=5%” (ii) Lissajous_sigma_vs_shear: which contains the data for the Lissajous-plots as stress (Sigma in (Pa) (right Column)) as function of shear rate (1/s (left Column)) for each sample and each amplitude displayed in the Manuscript. The files are named as “Lissajous_NameY-axe_vs_NameX-axe,_sample name_applied amplitude” as for instance “Lissajous_Sigma_vs_ShearRate_1wt%OCNF_5wt%SiNp5_gamma=5%” (iii) Lissajous_sigma_vs_strain: which contains the data for the Lissajous-plots as stress (Sigma in (Pa) (right Column)) as function of strain (gamma in (%) (left Column)) for each sample and each amplitude displayed in the Manuscript. The files are named as “Lissajous_NameY-axe_vs_NameX-axe,_sample name_applied amplitude” as for instance “Lissajous_Sigma_vs_strain_1wt%OCNF_5wt%SiNp5_gamma=5%” (iv) Sigma_vs_time: which contains the data for the sinusoidal deformation as stress (Sigma (Pa) (left Column)) as function of time (s, (right Column)) for each sample and each amplitude displayed in the Manuscript. The files are named as “NameY-axe_vs_NameX-axe,_sample name_applied amplitude” as for instance “Sigma_vs_time_1wt%OCNF_5wt%SiNp5_gamma=5%” The dataset for "Filler size effect in an attractive fibrillated network: a structural and rheological perspective" contains data, in the form of excel and txt files, for the figures shown in the main manuscript and the electronic supplementary information (ESI). Each excel sheet is specific for a set of data acquired utilising the same protocol. Rheological and scattering data are provided and specifications regarding each dataset can be found in the dataset description. This study is conducted to unravel how the size of colloidal fillers modulates the structure-property relationship of hydrogels composed by a fibrillated network. Specification of the materials and methods employed throughout the data collection are available in the main manuscript. 2020-02-05 University of Bath public RightsHolder University of Bath University of Bath https://doi.org/10.13039/501100000835 Engineering and Physical Sciences Research Council https://doi.org/10.13039/501100000266 EP/N033310/1 New Enzymatically Produced Interpenetrating Starch-Cellulose Gels Detailed description of materials and methods used for the data collection is described in the main Manuscript. en 1 10.15125/BATH-00762 https://doi.org/10.1039/C9SM02175B pub