data_240k_smz-f1_a _audit_creation_method 'SHELXL-2014/7' _shelx_SHELXL_version_number '2014/7' _chemical_name_systematic ' 4-amino-N-(4-methylpyrimidin-2-yl) ' _chemical_name_common ' Sulfamerazine ' _chemical_melting_point ? _chemical_formula_moiety 'C11 H12 N4 O2 S' _chemical_formula_sum 'C11 H12 N4 O2 S' _chemical_formula_weight 264.31 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_H-M_alt 'P n a 21' _space_group_name_Hall 'P 2c -2n' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' _cell_length_a 14.48520(10) _cell_length_b 8.20200(10) _cell_length_c 21.9002(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 2601.91(5) _cell_formula_units_Z 8 _cell_measurement_temperature 240 _cell_measurement_reflns_used 10719 _cell_measurement_theta_min 1.8010 _cell_measurement_theta_max 29.4920 _exptl_crystal_description Parallelepiped _exptl_crystal_colour Colourless _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.349 _exptl_crystal_F_000 1104 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.50 _exptl_crystal_size_mid 0.40 _exptl_crystal_size_min 0.20 _exptl_absorpt_coefficient_mu 0.249 _shelx_estimated_absorpt_T_min 0.886 _shelx_estimated_absorpt_T_max 0.952 _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min 0.98405 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_process_details ; CrysAlisPro, Agilent Technologies, Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _diffrn_ambient_temperature 240 _diffrn_radiation_wavelength 0.68890 _diffrn_radiation_type 'Synchrotron' _diffrn_radiation_source 'Diamond Light Source Beamline I19' _diffrn_radiation_monochromator 'double crystal Silicon 111' _diffrn_measurement_specimen_support 'MiTeGen loop' _diffrn_measurement_device 'CrystalLogic Kappa (3 circle)' _diffrn_measurement_device_type 'Rigaku Saturn724+ (2x2 bin mode)' _diffrn_measurement_method ; omega rotation with 1 degree frames ; _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 23512 _diffrn_reflns_av_unetI/netI 0.0447 _diffrn_reflns_av_R_equivalents 0.0455 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_theta_min 1.803 _diffrn_reflns_theta_max 29.474 _diffrn_reflns_theta_full 24.415 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.969 _diffrn_reflns_point_group_measured_fraction_full 0.988 _reflns_number_total 7694 _reflns_number_gt 6081 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.896 _reflns_Friedel_fraction_max 0.938 _reflns_Friedel_fraction_full 0.977 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_cell_refinement ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_data_reduction ; CrysAlisPro, Agilent Technologies, Version 1.171.37.35 (release 13-08-2014 CrysAlis171 .NET) (compiled Aug 13 2014,18:06:01) ; _computing_structure_solution 'SHELXT' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_molecular_graphics 'OSCAIL' _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0541P)^2^+0.3587P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Flack x determined using 2253 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.02(5) _chemical_absolute_configuration ad _refine_ls_number_reflns 7694 _refine_ls_number_parameters 344 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0644 _refine_ls_R_factor_gt 0.0473 _refine_ls_wR_factor_ref 0.1250 _refine_ls_wR_factor_gt 0.1115 _refine_ls_goodness_of_fit_ref 1.035 _refine_ls_restrained_S_all 1.035 _refine_ls_shift/su_max 0.087 _refine_ls_shift/su_mean 0.003 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.64592(5) 0.49539(9) 0.34416(5) 0.03225(19) Uani 1 1 d . . . . . S2 S 0.57779(6) 0.49602(9) 0.65262(5) 0.03139(19) Uani 1 1 d . . . . . O1 O 0.68918(18) 0.3709(3) 0.30872(13) 0.0422(6) Uani 1 1 d . . . . . O2 O 0.54884(17) 0.5223(3) 0.33757(14) 0.0417(6) Uani 1 1 d . . . . . O3 O 0.67526(16) 0.4684(3) 0.65896(14) 0.0403(6) Uani 1 1 d . . . . . O4 O 0.53551(18) 0.6231(3) 0.68742(13) 0.0414(6) Uani 1 1 d . . . . . N1 N 0.8422(2) 1.1165(4) 0.31230(19) 0.0484(9) Uani 1 1 d . . . . . N2 N 0.6551(2) 0.4487(4) 0.41708(16) 0.0370(7) Uani 1 1 d . . . . . N3 N 0.8145(2) 0.4091(4) 0.41746(15) 0.0380(7) Uani 1 1 d . . . . . N4 N 0.7280(2) 0.4292(5) 0.50951(16) 0.0519(9) Uani 1 1 d . . . . . N5 N 0.3802(3) -0.1197(4) 0.6954(2) 0.0612(11) Uani 1 1 d . . . . . H5A H 0.3237 -0.1182 0.7074 0.080 Uiso 1 1 calc R U . . . H5B H 0.4076 -0.2113 0.6891 0.080 Uiso 1 1 calc R U . . . N6 N 0.5682(2) 0.5384(4) 0.57939(16) 0.0393(7) Uani 1 1 d . . . . . N7 N 0.4098(2) 0.5857(4) 0.57989(15) 0.0387(7) Uani 1 1 d . . . . . N8 N 0.4960(2) 0.5660(5) 0.48762(17) 0.0513(9) Uani 1 1 d . . . . . C1 C 0.7046(2) 0.6777(4) 0.33417(18) 0.0309(7) Uani 1 1 d . . . . . C2 C 0.7946(2) 0.6796(4) 0.31059(16) 0.0314(7) Uani 1 1 d . . . . . H2 H 0.8236 0.5826 0.2997 0.041 Uiso 1 1 calc R U . . . C3 C 0.8398(2) 0.8255(4) 0.30360(18) 0.0325(7) Uani 1 1 d . . . . . H3 H 0.8998 0.8264 0.2884 0.042 Uiso 1 1 calc R U . . . C4 C 0.7973(2) 0.9727(4) 0.31888(17) 0.0333(7) Uani 1 1 d . . . . . C5 C 0.7067(2) 0.9694(4) 0.3426(2) 0.0372(8) Uani 1 1 d . . . . . H5 H 0.6775 1.0663 0.3533 0.048 Uiso 1 1 calc R U . . . C6 C 0.6613(2) 0.8229(4) 0.35001(19) 0.0372(8) Uani 1 1 d . . . . . H6 H 0.6016 0.8212 0.3657 0.048 Uiso 1 1 calc R U . . . C7 C 0.7370(2) 0.4287(4) 0.44924(17) 0.0350(8) Uani 1 1 d . . . . . C8 C 0.8065(3) 0.4045(8) 0.5406(2) 0.0716(16) Uani 1 1 d . . . . . H8 H 0.8042 0.4024 0.5831 0.093 Uiso 1 1 calc R U . . . C9 C 0.8896(3) 0.3825(7) 0.5125(2) 0.0661(14) Uani 1 1 d . . . . . H9 H 0.9429 0.3640 0.5351 0.086 Uiso 1 1 calc R U . . . C10 C 0.8922(3) 0.3885(5) 0.4499(2) 0.0468(10) Uani 1 1 d . . . . . C11 C 0.9790(3) 0.3695(6) 0.4141(2) 0.0625(12) Uani 1 1 d . . . . . H11A H 0.9819 0.2614 0.3974 0.081 Uiso 1 1 calc R U . . . H11B H 1.0312 0.3873 0.4403 0.081 Uiso 1 1 calc R U . . . H11C H 0.9799 0.4476 0.3814 0.081 Uiso 1 1 calc R U . . . C12 C 0.5189(2) 0.3160(4) 0.66585(16) 0.0303(7) Uani 1 1 d . . . . . C13 C 0.5634(2) 0.1680(4) 0.6556(2) 0.0404(9) Uani 1 1 d . . . . . H13 H 0.6241 0.1671 0.6418 0.053 Uiso 1 1 calc R U . . . C14 C 0.5181(3) 0.0236(4) 0.6657(2) 0.0459(10) Uani 1 1 d . . . . . H14 H 0.5485 -0.0746 0.6588 0.060 Uiso 1 1 calc R U . . . C15 C 0.4265(3) 0.0231(4) 0.68633(19) 0.0396(8) Uani 1 1 d . . . . . C16 C 0.3822(2) 0.1724(4) 0.69654(17) 0.0340(7) Uani 1 1 d . . . . . H16 H 0.3213 0.1739 0.7101 0.044 Uiso 1 1 calc R U . . . C17 C 0.4282(2) 0.3175(4) 0.68663(18) 0.0322(8) Uani 1 1 d . . . . . H17 H 0.3985 0.4161 0.6939 0.042 Uiso 1 1 calc R U . . . C18 C 0.4866(2) 0.5651(4) 0.54828(17) 0.0355(7) Uani 1 1 d . . . . . C19 C 0.4183(3) 0.5975(8) 0.4570(2) 0.0699(16) Uani 1 1 d . . . . . H19 H 0.4207 0.6008 0.4146 0.091 Uiso 1 1 calc R U . . . C20 C 0.3356(3) 0.6251(7) 0.4850(2) 0.0693(15) Uani 1 1 d . . . . . H20 H 0.2831 0.6501 0.4624 0.090 Uiso 1 1 calc R U . . . C21 C 0.3323(3) 0.6149(5) 0.5478(2) 0.0471(9) Uani 1 1 d . . . . . C22 C 0.2457(3) 0.6354(7) 0.5837(3) 0.0669(13) Uani 1 1 d . . . . . H22A H 0.2476 0.7371 0.6053 0.087 Uiso 1 1 calc R U . . . H22B H 0.2398 0.5474 0.6123 0.087 Uiso 1 1 calc R U . . . H22C H 0.1937 0.6350 0.5565 0.087 Uiso 1 1 calc R U . . . H1N1 H 0.891(3) 1.121(5) 0.292(2) 0.055(13) Uiso 1 1 d . . . . . H2N1 H 0.812(3) 1.200(6) 0.315(2) 0.060(14) Uiso 1 1 d . . . . . H1N2 H 0.618(3) 0.480(4) 0.438(2) 0.031(11) Uiso 1 1 d . . . . . H1N6 H 0.617(4) 0.501(6) 0.561(3) 0.076(18) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0302(4) 0.0346(4) 0.0319(4) 0.0029(3) -0.0017(3) -0.0021(3) S2 0.0292(3) 0.0343(4) 0.0307(5) 0.0035(3) -0.0010(3) -0.0019(3) O1 0.0483(14) 0.0347(12) 0.0435(16) -0.0047(11) 0.0014(12) -0.0018(11) O2 0.0318(12) 0.0519(14) 0.0414(16) 0.0077(13) -0.0062(13) -0.0053(10) O3 0.0307(12) 0.0509(14) 0.0392(15) 0.0067(12) -0.0055(12) -0.0029(10) O4 0.0454(15) 0.0346(12) 0.0440(16) -0.0038(11) -0.0007(12) -0.0021(10) N1 0.0434(18) 0.0352(16) 0.067(2) -0.0085(16) 0.0197(18) -0.0061(13) N2 0.0272(14) 0.0493(17) 0.0345(18) 0.0079(14) 0.0007(13) 0.0001(12) N3 0.0305(14) 0.0412(15) 0.0422(19) 0.0038(13) -0.0003(13) 0.0030(12) N4 0.0367(16) 0.084(3) 0.035(2) 0.0073(18) -0.0014(15) 0.0125(17) N5 0.053(2) 0.0361(16) 0.094(3) -0.0041(18) 0.018(2) -0.0087(14) N6 0.0288(14) 0.0562(18) 0.0329(18) 0.0111(15) 0.0016(13) 0.0023(13) N7 0.0304(14) 0.0440(16) 0.0417(19) 0.0020(14) 0.0024(13) 0.0043(12) N8 0.0385(16) 0.077(2) 0.038(2) 0.0069(17) -0.0029(15) 0.0130(16) C1 0.0293(15) 0.0347(14) 0.0286(18) 0.0021(13) -0.0005(13) 0.0008(11) C2 0.0305(15) 0.0345(15) 0.0292(18) 0.0009(13) 0.0019(14) 0.0039(11) C3 0.0285(15) 0.0382(17) 0.031(2) -0.0011(14) 0.0043(14) 0.0000(12) C4 0.0326(16) 0.0355(16) 0.0317(18) -0.0037(13) 0.0010(14) -0.0023(12) C5 0.0346(17) 0.0349(15) 0.042(2) -0.0025(16) 0.0049(18) 0.0042(12) C6 0.0312(15) 0.0396(16) 0.041(2) -0.0009(16) 0.0073(15) 0.0032(12) C7 0.0294(16) 0.0369(16) 0.039(2) 0.0074(14) -0.0015(15) 0.0022(12) C8 0.049(3) 0.126(5) 0.040(3) 0.003(3) -0.007(2) 0.025(3) C9 0.038(2) 0.108(4) 0.052(3) -0.002(3) -0.012(2) 0.020(2) C10 0.0334(18) 0.049(2) 0.058(3) 0.0015(19) 0.0004(18) 0.0075(15) C11 0.036(2) 0.076(3) 0.076(3) -0.005(3) 0.005(2) 0.0093(19) C12 0.0283(14) 0.0311(14) 0.0316(18) -0.0002(12) 0.0023(13) -0.0004(11) C13 0.0323(17) 0.0343(16) 0.055(3) 0.0005(17) 0.0082(18) 0.0045(12) C14 0.0408(19) 0.0333(16) 0.064(3) -0.0023(17) 0.0088(19) 0.0053(13) C15 0.043(2) 0.0341(16) 0.042(2) -0.0016(14) 0.0031(17) -0.0025(13) C16 0.0332(16) 0.0378(16) 0.0309(19) -0.0037(14) 0.0054(14) -0.0015(12) C17 0.0312(16) 0.0315(15) 0.034(2) -0.0019(13) 0.0020(14) 0.0015(12) C18 0.0325(16) 0.0414(17) 0.033(2) 0.0038(15) -0.0001(14) 0.0018(13) C19 0.048(3) 0.124(5) 0.038(3) 0.003(3) -0.008(2) 0.026(3) C20 0.041(2) 0.112(4) 0.055(3) -0.004(3) -0.012(2) 0.028(2) C21 0.0347(18) 0.057(2) 0.050(3) -0.0054(19) -0.0033(17) 0.0098(16) C22 0.035(2) 0.089(3) 0.077(3) -0.004(3) 0.004(2) 0.012(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 O1 1.427(3) . ? S1 O2 1.431(2) . ? S1 N2 1.648(4) . ? S1 C1 1.733(3) . ? S2 O4 1.429(3) . ? S2 O3 1.437(2) . ? S2 N6 1.647(4) . ? S2 C12 1.729(3) . ? N1 C4 1.354(4) . ? N1 H1N1 0.83(5) . ? N1 H2N1 0.82(5) . ? N2 C7 1.389(4) . ? N2 H1N2 0.75(4) . ? N3 C7 1.330(4) . ? N3 C10 1.341(5) . ? N4 C7 1.326(5) . ? N4 C8 1.341(5) . ? N5 C15 1.365(5) . ? N5 H5A 0.8600 . ? N5 H5B 0.8600 . ? N6 C18 1.382(5) . ? N6 H1N6 0.87(6) . ? N7 C18 1.321(4) . ? N7 C21 1.345(5) . ? N8 C19 1.335(5) . ? N8 C18 1.335(5) . ? C1 C6 1.390(5) . ? C1 C2 1.403(4) . ? C2 C3 1.373(5) . ? C2 H2 0.9300 . ? C3 C4 1.396(5) . ? C3 H3 0.9300 . ? C4 C5 1.411(5) . ? C5 C6 1.380(5) . ? C5 H5 0.9300 . ? C6 H6 0.9300 . ? C8 C9 1.364(6) . ? C8 H8 0.9300 . ? C9 C10 1.373(7) . ? C9 H9 0.9300 . ? C10 C11 1.490(6) . ? C11 H11A 0.9600 . ? C11 H11B 0.9600 . ? C11 H11C 0.9600 . ? C12 C17 1.391(4) . ? C12 C13 1.392(4) . ? C13 C14 1.371(5) . ? C13 H13 0.9300 . ? C14 C15 1.402(5) . ? C14 H14 0.9300 . ? C15 C16 1.400(5) . ? C16 C17 1.381(5) . ? C16 H16 0.9300 . ? C17 H17 0.9300 . ? C19 C20 1.365(7) . ? C19 H19 0.9300 . ? C20 C21 1.380(7) . ? C20 H20 0.9300 . ? C21 C22 1.490(6) . ? C22 H22A 0.9600 . ? C22 H22B 0.9600 . ? C22 H22C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 S1 O2 119.15(17) . . ? O1 S1 N2 108.97(18) . . ? O2 S1 N2 102.32(17) . . ? O1 S1 C1 109.45(17) . . ? O2 S1 C1 109.63(15) . . ? N2 S1 C1 106.43(18) . . ? O4 S2 O3 118.98(17) . . ? O4 S2 N6 109.24(17) . . ? O3 S2 N6 102.13(17) . . ? O4 S2 C12 108.78(17) . . ? O3 S2 C12 109.50(15) . . ? N6 S2 C12 107.55(18) . . ? C4 N1 H1N1 120(3) . . ? C4 N1 H2N1 118(3) . . ? H1N1 N1 H2N1 117(4) . . ? C7 N2 S1 126.0(3) . . ? C7 N2 H1N2 111(3) . . ? S1 N2 H1N2 116(3) . . ? C7 N3 C10 116.5(3) . . ? C7 N4 C8 115.0(4) . . ? C15 N5 H5A 120.0 . . ? C15 N5 H5B 120.0 . . ? H5A N5 H5B 120.0 . . ? C18 N6 S2 125.8(3) . . ? C18 N6 H1N6 122(4) . . ? S2 N6 H1N6 107(4) . . ? C18 N7 C21 116.9(3) . . ? C19 N8 C18 114.5(4) . . ? C6 C1 C2 120.1(3) . . ? C6 C1 S1 119.1(3) . . ? C2 C1 S1 120.8(2) . . ? C3 C2 C1 119.6(3) . . ? C3 C2 H2 120.2 . . ? C1 C2 H2 120.2 . . ? C2 C3 C4 121.2(3) . . ? C2 C3 H3 119.4 . . ? C4 C3 H3 119.4 . . ? N1 C4 C3 121.0(3) . . ? N1 C4 C5 120.2(3) . . ? C3 C4 C5 118.8(3) . . ? C6 C5 C4 120.2(3) . . ? C6 C5 H5 119.9 . . ? C4 C5 H5 119.9 . . ? C5 C6 C1 120.2(3) . . ? C5 C6 H6 119.9 . . ? C1 C6 H6 119.9 . . ? N4 C7 N3 127.2(3) . . ? N4 C7 N2 114.8(3) . . ? N3 C7 N2 118.0(3) . . ? N4 C8 C9 122.6(5) . . ? N4 C8 H8 118.7 . . ? C9 C8 H8 118.7 . . ? C8 C9 C10 118.1(4) . . ? C8 C9 H9 121.0 . . ? C10 C9 H9 121.0 . . ? N3 C10 C9 120.7(4) . . ? N3 C10 C11 116.3(4) . . ? C9 C10 C11 123.0(4) . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C17 C12 C13 119.8(3) . . ? C17 C12 S2 120.9(2) . . ? C13 C12 S2 119.3(2) . . ? C14 C13 C12 120.4(3) . . ? C14 C13 H13 119.8 . . ? C12 C13 H13 119.8 . . ? C13 C14 C15 120.4(3) . . ? C13 C14 H14 119.8 . . ? C15 C14 H14 119.8 . . ? N5 C15 C16 120.1(3) . . ? N5 C15 C14 121.0(3) . . ? C16 C15 C14 118.9(3) . . ? C17 C16 C15 120.4(3) . . ? C17 C16 H16 119.8 . . ? C15 C16 H16 119.8 . . ? C16 C17 C12 120.0(3) . . ? C16 C17 H17 120.0 . . ? C12 C17 H17 120.0 . . ? N7 C18 N8 127.4(3) . . ? N7 C18 N6 118.8(3) . . ? N8 C18 N6 113.8(3) . . ? N8 C19 C20 123.1(5) . . ? N8 C19 H19 118.5 . . ? C20 C19 H19 118.5 . . ? C19 C20 C21 117.9(4) . . ? C19 C20 H20 121.1 . . ? C21 C20 H20 121.1 . . ? N7 C21 C20 120.2(4) . . ? N7 C21 C22 116.6(4) . . ? C20 C21 C22 123.2(4) . . ? C21 C22 H22A 109.5 . . ? C21 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C21 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 S1 N2 C7 60.7(4) . . . . ? O2 S1 N2 C7 -172.3(3) . . . . ? C1 S1 N2 C7 -57.3(4) . . . . ? O4 S2 N6 C18 -57.4(4) . . . . ? O3 S2 N6 C18 175.8(3) . . . . ? C12 S2 N6 C18 60.5(4) . . . . ? O1 S1 C1 C6 162.3(3) . . . . ? O2 S1 C1 C6 29.8(4) . . . . ? N2 S1 C1 C6 -80.1(3) . . . . ? O1 S1 C1 C2 -17.9(4) . . . . ? O2 S1 C1 C2 -150.3(3) . . . . ? N2 S1 C1 C2 99.7(3) . . . . ? C6 C1 C2 C3 0.4(5) . . . . ? S1 C1 C2 C3 -179.5(3) . . . . ? C1 C2 C3 C4 -0.8(5) . . . . ? C2 C3 C4 N1 179.6(4) . . . . ? C2 C3 C4 C5 0.8(6) . . . . ? N1 C4 C5 C6 -179.2(4) . . . . ? C3 C4 C5 C6 -0.4(6) . . . . ? C4 C5 C6 C1 0.0(6) . . . . ? C2 C1 C6 C5 0.0(6) . . . . ? S1 C1 C6 C5 179.9(3) . . . . ? C8 N4 C7 N3 -1.0(6) . . . . ? C8 N4 C7 N2 177.9(4) . . . . ? C10 N3 C7 N4 -0.4(6) . . . . ? C10 N3 C7 N2 -179.4(3) . . . . ? S1 N2 C7 N4 164.9(3) . . . . ? S1 N2 C7 N3 -16.0(5) . . . . ? C7 N4 C8 C9 0.7(8) . . . . ? N4 C8 C9 C10 1.0(9) . . . . ? C7 N3 C10 C9 2.3(6) . . . . ? C7 N3 C10 C11 -178.9(4) . . . . ? C8 C9 C10 N3 -2.5(8) . . . . ? C8 C9 C10 C11 178.8(5) . . . . ? O4 S2 C12 C17 22.4(4) . . . . ? O3 S2 C12 C17 154.0(3) . . . . ? N6 S2 C12 C17 -95.8(3) . . . . ? O4 S2 C12 C13 -157.4(3) . . . . ? O3 S2 C12 C13 -25.9(4) . . . . ? N6 S2 C12 C13 84.4(3) . . . . ? C17 C12 C13 C14 0.2(6) . . . . ? S2 C12 C13 C14 -179.9(4) . . . . ? C12 C13 C14 C15 0.1(7) . . . . ? C13 C14 C15 N5 178.7(4) . . . . ? C13 C14 C15 C16 -0.1(6) . . . . ? N5 C15 C16 C17 -179.1(4) . . . . ? C14 C15 C16 C17 -0.2(6) . . . . ? C15 C16 C17 C12 0.6(6) . . . . ? C13 C12 C17 C16 -0.6(5) . . . . ? S2 C12 C17 C16 179.6(3) . . . . ? C21 N7 C18 N8 -1.8(6) . . . . ? C21 N7 C18 N6 178.6(4) . . . . ? C19 N8 C18 N7 2.6(7) . . . . ? C19 N8 C18 N6 -177.7(4) . . . . ? S2 N6 C18 N7 11.9(5) . . . . ? S2 N6 C18 N8 -167.8(3) . . . . ? C18 N8 C19 C20 -0.6(8) . . . . ? N8 C19 C20 C21 -2.0(10) . . . . ? C18 N7 C21 C20 -1.2(6) . . . . ? C18 N7 C21 C22 179.0(4) . . . . ? C19 C20 C21 N7 2.9(8) . . . . ? C19 C20 C21 C22 -177.3(5) . . . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N5 H5B O4 0.86 2.30 3.089(5) 152.9 1_545 N1 H1N1 O4 0.83(5) 2.53(5) 3.259(5) 148(4) 4_654 N1 H2N1 O1 0.82(5) 2.26(5) 3.045(4) 160(4) 1_565 N2 H1N2 N8 0.75(4) 2.19(4) 2.937(5) 173(4) . N6 H1N6 N4 0.87(6) 2.05(6) 2.916(5) 173(6) . _refine_diff_density_max 0.256 _refine_diff_density_min -0.307 _refine_diff_density_rms 0.046 _shelx_res_file ; 240k_smz-f1_a.res created by SHELXL-2014/7 TITL 240k_smz-f1_a.res in Pna2(1) REM Old TITL 008_240K_SulfamerazineF1_ in Pna2(1) REM SHELXT solution in Pna2(1) REM R1 0.102, Rweak 0.018, Alpha 0.003, Orientation as input REM Flack x = 0.096 ( 0.041 ) from Parsons' quotients REM Formula found by SHELXT: C26 N4 O4 S2 CELL 0.68890 14.4852 8.2020 21.9002 90.000 90.000 90.000 ZERR 8.000 0.0001 0.0001 0.0003 0.000 0.000 0.000 REM SG 33 4 4 Pna21 PGmm2 Orthorhombic LATT -1 REM SG ASUN 1 .5 .5 1. REM SG ORGN on 2(1) SYMM -X,-Y,0.5+Z SYMM 0.5+X,0.5-Y,Z SYMM 0.5-X,0.5+Y,0.5+Z SFAC C H N O S UNIT 88.00 96.00 32.00 16.00 8.00 L.S. 10 SIZE 0.50 0.40 0.20 BOND $H FMAP 2 PLAN 20 ACTA CONF EQIV $1 x, y-1, z HTAB N5 O4_$1 EQIV $2 -x+3/2, y+1/2, z-1/2 HTAB N1 O4_$2 EQIV $3 x, y+1, z HTAB N1 O1_$3 HTAB N2 N8 HTAB N6 N4 LIST 4 WGHT 0.054100 0.358700 FVAR 0.51921 0.35344 S1 5 0.645917 0.495395 0.344157 11.00000 0.03025 0.03460 = 0.03191 0.00290 -0.00166 -0.00206 S2 5 0.577794 0.496023 0.652622 11.00000 0.02915 0.03427 = 0.03075 0.00350 -0.00103 -0.00193 O1 4 0.689182 0.370897 0.308725 11.00000 0.04834 0.03472 = 0.04350 -0.00473 0.00144 -0.00175 O2 4 0.548844 0.522325 0.337567 11.00000 0.03175 0.05187 = 0.04143 0.00770 -0.00621 -0.00528 O3 4 0.675261 0.468448 0.658964 11.00000 0.03068 0.05090 = 0.03924 0.00674 -0.00552 -0.00294 O4 4 0.535505 0.623051 0.687424 11.00000 0.04537 0.03465 = 0.04404 -0.00377 -0.00070 -0.00206 N1 3 0.842196 1.116457 0.312299 11.00000 0.04336 0.03517 = 0.06661 -0.00845 0.01972 -0.00605 N2 3 0.655146 0.448715 0.417076 11.00000 0.02716 0.04925 = 0.03449 0.00787 0.00071 0.00009 N3 3 0.814502 0.409075 0.417463 11.00000 0.03046 0.04118 = 0.04222 0.00380 -0.00032 0.00300 N4 3 0.727995 0.429198 0.509514 11.00000 0.03671 0.08403 = 0.03488 0.00731 -0.00138 0.01246 N5 3 0.380219 -0.119738 0.695412 11.00000 0.05311 0.03610 = 0.09436 -0.00405 0.01783 -0.00875 AFIX 93 H5A 2 0.323703 -0.118244 0.707430 11.00000 -1.30000 H5B 2 0.407569 -0.211273 0.689118 11.00000 -1.30000 AFIX 0 N6 3 0.568212 0.538358 0.579390 11.00000 0.02876 0.05618 = 0.03285 0.01111 0.00159 0.00225 N7 3 0.409776 0.585730 0.579891 11.00000 0.03044 0.04405 = 0.04175 0.00203 0.00242 0.00432 N8 3 0.495984 0.565986 0.487615 11.00000 0.03852 0.07738 = 0.03815 0.00691 -0.00285 0.01298 C1 1 0.704591 0.677651 0.334172 11.00000 0.02927 0.03468 = 0.02860 0.00214 -0.00050 0.00079 C2 1 0.794650 0.679588 0.310585 11.00000 0.03053 0.03445 = 0.02916 0.00092 0.00186 0.00388 AFIX 43 H2 2 0.823572 0.582581 0.299749 11.00000 -1.30000 AFIX 0 C3 1 0.839796 0.825527 0.303605 11.00000 0.02849 0.03815 = 0.03091 -0.00108 0.00434 -0.00001 AFIX 43 H3 2 0.899760 0.826357 0.288433 11.00000 -1.30000 AFIX 0 C4 1 0.797294 0.972725 0.318876 11.00000 0.03265 0.03545 = 0.03173 -0.00367 0.00098 -0.00229 C5 1 0.706707 0.969422 0.342593 11.00000 0.03458 0.03490 = 0.04200 -0.00253 0.00488 0.00424 AFIX 43 H5 2 0.677522 1.066326 0.353250 11.00000 -1.30000 AFIX 0 C6 1 0.661329 0.822851 0.350012 11.00000 0.03118 0.03962 = 0.04066 -0.00089 0.00730 0.00323 AFIX 43 H6 2 0.601645 0.821219 0.365651 11.00000 -1.30000 AFIX 0 C7 1 0.737015 0.428720 0.449242 11.00000 0.02939 0.03688 = 0.03877 0.00742 -0.00150 0.00224 C8 1 0.806496 0.404534 0.540639 11.00000 0.04875 0.12591 = 0.04018 0.00340 -0.00749 0.02521 AFIX 43 H8 2 0.804190 0.402352 0.583069 11.00000 -1.30000 AFIX 0 C9 1 0.889600 0.382518 0.512512 11.00000 0.03773 0.10822 = 0.05241 -0.00216 -0.01175 0.01990 AFIX 43 H9 2 0.942943 0.364021 0.535107 11.00000 -1.30000 AFIX 0 C10 1 0.892208 0.388460 0.449863 11.00000 0.03336 0.04860 = 0.05831 0.00155 0.00036 0.00747 C11 1 0.979030 0.369514 0.414060 11.00000 0.03568 0.07600 = 0.07580 -0.00513 0.00546 0.00931 AFIX 137 H11A 2 0.981939 0.261371 0.397403 11.00000 -1.30000 H11B 2 1.031171 0.387317 0.440285 11.00000 -1.30000 H11C 2 0.979913 0.447650 0.381428 11.00000 -1.30000 AFIX 0 C12 1 0.518944 0.315997 0.665846 11.00000 0.02825 0.03115 = 0.03160 -0.00019 0.00229 -0.00035 C13 1 0.563381 0.168012 0.655608 11.00000 0.03226 0.03431 = 0.05466 0.00054 0.00824 0.00449 AFIX 43 H13 2 0.624116 0.167063 0.641844 11.00000 -1.30000 AFIX 0 C14 1 0.518148 0.023612 0.665693 11.00000 0.04082 0.03332 = 0.06351 -0.00235 0.00878 0.00531 AFIX 43 H14 2 0.548453 -0.074641 0.658801 11.00000 -1.30000 AFIX 0 C15 1 0.426499 0.023135 0.686330 11.00000 0.04270 0.03409 = 0.04199 -0.00160 0.00309 -0.00252 C16 1 0.382169 0.172404 0.696536 11.00000 0.03324 0.03781 = 0.03093 -0.00367 0.00542 -0.00152 AFIX 43 H16 2 0.321321 0.173852 0.710075 11.00000 -1.30000 AFIX 0 C17 1 0.428194 0.317461 0.686633 11.00000 0.03120 0.03147 = 0.03387 -0.00194 0.00201 0.00149 AFIX 43 H17 2 0.398520 0.416140 0.693862 11.00000 -1.30000 AFIX 0 C18 1 0.486565 0.565118 0.548276 11.00000 0.03248 0.04137 = 0.03266 0.00384 -0.00013 0.00184 C19 1 0.418330 0.597495 0.456969 11.00000 0.04825 0.12403 = 0.03751 0.00296 -0.00797 0.02636 AFIX 43 H19 2 0.420714 0.600768 0.414551 11.00000 -1.30000 AFIX 0 C20 1 0.335583 0.625138 0.484970 11.00000 0.04116 0.11159 = 0.05523 -0.00431 -0.01182 0.02824 AFIX 43 H20 2 0.283067 0.650054 0.462394 11.00000 -1.30000 AFIX 0 C21 1 0.332339 0.614933 0.547848 11.00000 0.03473 0.05681 = 0.04973 -0.00538 -0.00326 0.00982 C22 1 0.245659 0.635423 0.583668 11.00000 0.03482 0.08908 = 0.07683 -0.00432 0.00378 0.01223 AFIX 137 H22A 2 0.247629 0.737088 0.605349 11.00000 -1.30000 H22B 2 0.239797 0.547357 0.612280 11.00000 -1.30000 H22C 2 0.193705 0.635024 0.556453 11.00000 -1.30000 AFIX 0 H1N1 2 0.890524 1.120650 0.291833 11.00000 0.05482 H2N1 2 0.811647 1.200289 0.314700 11.00000 0.05971 H1N2 2 0.617611 0.479627 0.437569 11.00000 0.03139 H1N6 2 0.617440 0.500931 0.561374 11.00000 0.07601 HKLF 4 REM 240k_smz-f1_a.res in Pna2(1) REM R1 = 0.0473 for 6081 Fo > 4sig(Fo) and 0.0644 for all 7694 data REM 344 parameters refined using 1 restraints END WGHT 0.0484 0.4605 REM Highest difference peak 0.256, deepest hole -0.307, 1-sigma level 0.046 Q1 1 0.5453 0.3981 0.6552 11.00000 0.05 0.26 Q2 1 0.6804 0.5922 0.3444 11.00000 0.05 0.23 Q3 1 0.8078 0.7698 0.3006 11.00000 0.05 0.20 Q4 1 0.6847 0.3849 0.5281 11.00000 0.05 0.18 Q5 1 0.5419 0.2559 0.6516 11.00000 0.05 0.18 Q6 1 0.6989 0.4305 0.3388 11.00000 0.05 0.18 Q7 1 0.5882 0.4963 0.3421 11.00000 0.05 0.18 Q8 1 0.2705 0.5694 0.4706 11.00000 0.05 0.18 Q9 1 0.5927 0.5428 0.3422 11.00000 0.05 0.18 Q10 1 0.4226 0.2311 0.6980 11.00000 0.05 0.18 Q11 1 0.7578 0.9655 0.3416 11.00000 0.05 0.17 Q12 1 0.4767 0.0287 0.6914 11.00000 0.05 0.17 Q13 1 0.4672 0.5204 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145.80 8.96 5 -2 2 144.23 9.43 5 2 2 155.10 9.28 5 -2 3 327.25 13.98 5 2 3 290.81 12.99 5 2 4 69.32 6.01 5 2 4 67.59 6.30 5 -2 4 72.38 6.62 5 2 5 91.87 7.65 5 -2 5 108.48 8.16 5 2 5 106.06 7.61 5 2 6 363.11 14.17 5 -2 6 351.51 14.91 5 2 6 377.91 15.64 5 2 7 604.33 18.02 5 -2 7 604.64 19.70 5 2 7 593.65 20.29 5 2 8 86.14 6.88 5 -2 8 97.46 8.04 5 2 8 92.09 8.09 5 2 9 7.07 2.22 5 2 9 11.78 2.68 5 -2 9 10.11 2.70 5 2 10 0.89 1.02 5 2 10 1.24 1.21 5 -2 10 1.52 0.97 5 2 11 88.78 7.04 5 2 11 83.38 8.07 5 -2 11 83.41 7.62 5 2 12 14.01 3.47 5 2 12 19.92 3.54 5 -2 12 15.39 3.14 5 -2 13 335.30 15.91 5 2 13 304.39 16.55 5 2 13 321.55 13.63 5 -2 14 110.13 9.52 5 2 14 133.14 8.75 5 2 14 127.37 10.80 5 2 15 713.36 20.39 5 2 15 660.15 25.20 5 -2 15 679.07 23.63 5 2 16 86.32 9.15 5 -2 16 76.74 8.02 5 2 16 84.68 6.92 5 2 17 49.02 7.45 5 -2 17 34.26 5.78 5 2 18 38.16 6.76 5 -2 18 38.60 5.82 5 2 19 152.65 12.89 5 -2 19 153.72 12.33 5 2 20 14.76 3.86 5 2 21 1.64 2.26 5 2 22 9.91 3.69 5 2 23 37.14 7.17 5 2 24 13.55 4.86 5 -3 -29 5.94 4.14 5 -3 -28 22.01 6.15 5 -3 -27 56.88 9.08 5 -3 -26 23.47 5.97 5 -3 -25 139.12 14.03 5 -3 -24 5.22 1.97 5 -3 -23 1.08 1.55 5 -3 -22 117.39 12.35 5 -3 -21 145.73 13.93 5 -3 -20 75.10 9.65 5 -3 -19 137.73 12.17 5 -3 -19 134.65 12.79 5 -3 -18 23.67 5.81 5 -3 -18 24.26 5.11 5 -3 -17 19.41 4.54 5 -3 -17 25.92 5.34 5 3 -17 25.41 4.55 5 -3 -16 143.29 11.74 5 3 -16 170.86 12.19 5 3 -15 555.59 19.83 5 -3 -15 530.61 24.48 5 3 -15 567.48 22.68 5 -3 -15 541.39 22.90 5 3 -14 107.15 8.22 5 -3 -14 118.03 11.17 5 -3 -14 105.00 9.95 5 3 -13 23.64 4.90 5 3 -13 19.98 3.40 5 -3 -13 22.98 4.85 5 -3 -13 22.36 4.49 5 3 -12 65.43 5.98 5 -3 -12 63.53 7.53 5 -3 -12 64.85 8.23 5 3 -12 59.85 7.10 5 -3 -11 129.98 10.72 5 -3 -11 116.70 10.93 -5 3 -11 121.85 7.07 5 3 -11 114.25 7.28 5 3 -11 115.80 9.66 -5 3 -10 204.43 9.51 5 3 -10 220.14 9.58 5 3 -10 208.26 6.84 5 -3 -10 231.91 13.92 5 -3 -10 236.82 14.53 5 3 -9 59.77 4.14 5 3 -9 60.59 4.94 5 -3 -9 73.21 8.40 5 -3 -9 50.71 6.71 5 3 -9 70.97 7.13 5 3 -8 14.91 2.28 5 3 -8 14.31 3.36 5 3 -8 17.47 2.55 5 -3 -8 21.11 4.19 5 -3 -8 17.12 4.27 5 3 -7 125.49 9.58 5 -3 -7 133.16 10.67 5 3 -7 131.14 7.06 5 -3 -7 136.09 10.25 5 3 -7 141.17 6.56 5 -3 -6 601.13 22.02 5 3 -6 573.51 20.28 5 3 -6 588.64 13.25 5 3 -6 565.95 15.22 5 -3 -6 533.83 20.26 5 -3 -5 519.90 20.37 5 3 -5 524.94 19.39 5 3 -5 524.23 15.27 5 3 -5 533.76 12.33 5 -3 -5 529.59 19.94 5 3 -4 259.99 13.64 5 -3 -4 240.96 13.26 5 -3 -4 240.42 13.31 5 3 -4 269.64 8.80 5 3 -4 268.56 11.18 5 3 -3 167.50 10.70 5 -3 -3 195.49 11.94 5 3 -3 178.36 9.55 5 3 -3 186.69 7.68 5 -3 -3 173.05 11.21 5 -3 -2 441.97 17.96 5 -3 -2 436.50 17.67 5 3 -2 414.65 14.84 5 -3 -1 1445.10 31.83 5 3 -1 1460.32 31.52 5 3 -1 1439.59 28.15 5 -3 -1 1544.38 32.85 5 3 0 1056.54 26.57 5 -3 0 1026.01 27.15 5 -3 0 1033.82 26.88 5 3 0 1007.91 24.51 5 -3 1 1408.81 31.15 5 -3 1 1458.91 31.65 5 3 1 1406.72 29.48 5 3 1 1485.37 31.88 5 -3 2 442.25 17.29 5 -3 2 439.74 17.36 5 3 2 433.08 17.06 5 3 2 402.27 16.05 5 3 3 180.90 11.17 5 -3 3 176.83 11.01 5 3 3 182.88 11.22 5 -3 3 199.45 11.57 5 -3 4 237.79 12.81 5 3 4 286.11 13.95 5 -3 4 265.55 13.60 5 3 4 248.84 13.24 5 -3 5 510.29 18.88 5 3 5 533.85 19.37 5 3 5 540.38 19.12 5 3 6 601.56 21.26 5 3 6 588.62 19.96 5 -3 6 572.97 19.94 5 3 7 153.82 10.10 5 -3 7 140.62 9.93 5 3 7 133.65 10.33 5 3 8 13.57 2.98 5 -3 8 18.16 3.67 5 3 8 11.89 3.31 5 3 9 40.23 5.43 5 -3 9 58.50 6.40 5 3 9 47.60 6.33 5 -3 10 250.12 13.67 5 3 10 228.36 14.00 5 3 10 231.59 12.70 5 3 11 116.01 9.02 5 -3 11 124.47 9.66 5 3 11 129.28 10.80 5 3 12 69.92 7.15 5 -3 12 66.94 7.31 5 3 12 63.29 7.55 5 3 13 19.79 3.83 5 3 13 21.02 4.89 5 -3 13 14.82 3.99 5 3 14 104.04 8.89 5 -3 14 108.80 9.50 5 3 14 114.22 10.74 5 3 15 564.04 20.86 5 -3 15 519.15 21.12 5 3 15 544.02 23.95 5 3 16 160.36 12.96 5 -3 16 165.46 12.25 5 3 16 146.68 10.86 5 3 17 23.79 4.67 5 -3 17 25.81 5.24 5 3 17 21.92 4.97 5 3 18 27.99 5.60 5 -3 18 22.97 4.10 5 3 19 153.27 13.39 5 3 20 67.40 9.25 5 3 21 132.15 13.14 5 3 22 114.52 12.74 5 3 23 0.37 1.34 5 3 24 9.22 4.02 5 3 25 120.59 14.00 5 -4 -28 4.64 2.20 5 -4 -27 -4.72 4.27 5 -4 -26 0.66 1.97 5 -4 -25 13.36 5.03 5 -4 -24 57.76 9.42 5 -4 -23 17.50 4.39 5 -4 -22 1.35 1.47 5 -4 -21 29.85 6.70 5 -4 -20 70.68 9.78 5 -4 -20 67.30 9.43 5 -4 -19 9.28 3.61 5 -4 -19 4.10 3.13 -5 -4 -18 8.27 3.77 5 -4 -18 10.59 3.30 5 -4 -18 10.98 4.34 -5 -4 -17 288.71 18.51 5 -4 -17 234.26 16.78 5 -4 -17 258.27 17.70 5 -4 -16 116.62 11.62 5 4 -16 100.09 9.84 5 -4 -16 98.75 10.39 -5 -4 -16 95.45 10.38 -5 -4 -15 51.63 7.89 5 -4 -15 45.24 7.01 5 4 -15 38.77 6.11 5 -4 -15 33.18 6.30 5 4 -14 17.84 4.49 5 -4 -14 18.77 5.65 5 -4 -14 23.24 5.20 -5 -4 -14 17.01 4.37 5 4 -13 101.98 9.77 5 -4 -13 102.23 10.65 5 -4 -13 118.05 11.11 -5 -4 -13 106.49 10.30 -5 -4 -12 152.71 12.23 5 4 -12 140.58 11.25 5 -4 -12 160.26 12.88 5 -4 -12 172.68 13.04 5 -4 -11 38.39 6.02 5 -4 -11 47.35 7.11 5 4 -11 34.59 5.31 -5 4 -11 35.21 4.57 5 -4 -10 14.71 4.33 5 4 -10 15.67 4.51 -5 4 -10 14.13 3.09 5 -4 -10 12.28 3.12 -5 4 -9 133.11 8.92 5 -4 -9 148.43 11.81 5 4 -9 129.46 10.47 5 4 -9 114.93 6.77 5 -4 -9 129.28 11.16 5 4 -8 26.57 5.04 5 4 -8 33.82 3.95 -5 4 -8 32.34 4.64 5 -4 -8 27.33 4.91 5 -4 -8 25.48 4.64 5 4 -7 57.03 7.11 5 4 -7 65.60 5.67 -5 4 -7 75.73 7.05 5 -4 -7 78.79 8.26 5 -4 -7 68.83 7.92 5 4 -6 230.61 13.80 5 -4 -6 227.68 14.28 5 4 -6 225.04 10.82 5 -4 -6 226.59 14.20 5 -4 -5 76.47 8.26 5 4 -5 70.78 7.97 5 4 -5 80.86 6.59 5 -4 -5 76.73 8.12 5 4 -4 108.70 9.25 5 -4 -4 99.63 9.43 5 4 -4 100.34 4.40 5 4 -4 104.35 7.82 5 -4 -4 124.67 10.29 5 -4 -3 9.27 3.09 5 4 -3 4.06 2.33 5 4 -3 8.50 2.58 5 -4 -3 3.37 1.47 5 4 -3 7.26 1.38 5 4 -2 28.90 5.07 5 4 -2 33.94 4.67 5 -4 -2 28.55 5.01 5 -4 -2 26.74 4.49 5 -4 -1 6.27 2.80 5 4 -1 3.85 1.06 5 4 -1 6.67 2.43 5 -4 -1 4.73 1.90 5 4 0 112.85 8.97 5 4 0 98.88 9.08 5 -4 0 109.34 9.00 5 -4 0 131.80 10.47 5 -4 1 7.55 2.69 5 4 1 7.39 2.94 5 4 1 2.99 1.99 5 -4 1 7.19 2.44 5 -4 2 33.40 5.59 5 4 2 30.56 4.64 5 4 2 39.88 5.99 5 -4 2 32.74 4.90 5 -4 3 8.77 2.94 5 4 3 5.85 2.89 5 4 3 4.08 1.77 5 -4 3 9.64 3.12 5 -4 4 98.11 8.78 5 4 4 92.25 8.59 5 -4 4 120.66 9.39 5 4 4 126.74 10.13 5 -4 5 78.46 7.99 5 4 5 76.07 7.80 5 4 5 78.54 8.05 5 -4 5 73.72 7.40 5 4 6 218.70 13.76 5 4 6 237.02 13.75 5 -4 6 223.30 13.46 5 4 7 72.28 7.98 5 -4 7 58.15 7.03 5 4 7 73.57 7.77 5 4 8 24.19 4.84 5 4 8 26.28 4.71 5 -4 8 27.80 4.91 5 4 9 133.88 11.00 5 4 9 128.93 10.46 5 -4 9 115.46 9.85 5 4 10 13.84 3.56 5 4 10 17.13 3.98 5 -4 10 18.67 3.86 5 4 11 50.28 6.57 5 -4 11 50.86 6.45 5 4 11 45.82 6.56 5 -4 12 174.18 12.28 5 4 12 155.09 11.83 5 -4 13 101.19 9.64 5 4 13 102.15 9.67 5 4 13 92.88 9.82 5 4 14 11.42 3.13 5 -4 14 19.94 4.37 5 4 14 28.27 5.82 5 4 15 35.06 5.97 5 -4 15 30.12 5.30 5 4 15 43.43 6.76 5 4 16 87.89 9.47 5 -4 16 88.78 9.31 5 4 16 89.29 10.35 5 4 17 269.88 17.91 5 -4 17 255.24 15.81 5 4 17 285.26 16.93 5 4 18 5.30 3.66 5 4 19 7.38 3.34 5 4 20 70.30 9.48 5 4 21 24.20 5.92 5 4 22 5.17 3.66 5 4 23 13.68 3.18 5 4 24 42.32 7.99 5 4 25 17.28 5.66 5 4 26 2.38 3.17 5 -5 -27 5.58 3.09 5 -5 -26 19.81 5.21 5 -5 -25 17.97 5.88 5 -5 -24 54.24 8.92 5 -5 -23 5.80 3.72 5 -5 -22 4.35 2.68 5 -5 -21 64.77 9.44 5 -5 -20 87.79 10.85 -5 -5 -20 93.19 11.53 5 -5 -20 112.05 12.63 -5 -5 -19 6.71 2.87 5 -5 -19 13.64 5.09 5 -5 -19 8.76 3.48 5 -5 -18 4.05 3.50 5 -5 -18 7.11 3.47 -5 -5 -18 5.88 2.22 -5 -5 -17 54.82 8.81 5 -5 -17 58.22 8.84 5 -5 -17 42.13 7.17 5 5 -16 1.45 1.16 -5 -5 -16 -2.21 1.32 5 -5 -16 -1.66 2.38 5 -5 -16 -0.24 2.17 5 -5 -15 157.20 14.07 -5 -5 -15 144.42 12.83 5 -5 -15 153.23 13.71 5 5 -14 51.68 7.65 -5 -5 -14 56.89 7.64 5 -5 -14 68.24 8.56 5 -5 -14 54.52 8.20 5 5 -13 -2.00 1.87 5 -5 -13 0.89 2.64 -5 -5 -13 3.26 3.34 5 -5 -13 2.38 1.79 5 5 -12 17.21 4.11 -5 -5 -12 23.07 5.01 5 -5 -12 22.51 5.39 5 -5 -12 26.38 5.05 -5 5 -11 157.93 11.46 -5 -5 -11 173.32 13.05 5 -5 -11 190.15 14.24 5 5 -11 186.09 13.91 5 -5 -11 179.24 14.11 5 5 -10 53.34 7.46 5 -5 -10 57.97 8.19 -5 5 -10 53.75 6.66 5 -5 -10 46.09 7.13 -5 -5 -10 61.48 7.57 5 5 -9 101.67 10.05 -5 5 -9 99.21 9.15 5 -5 -9 87.35 9.95 5 -5 -9 110.96 10.94 -5 5 -8 28.52 5.16 5 5 -8 22.12 4.68 5 5 -8 20.83 3.55 5 -5 -8 32.49 5.75 5 -5 -8 22.43 4.75 5 -5 -7 25.85 5.66 5 5 -7 18.51 3.91 5 5 -7 26.04 4.32 -5 5 -7 24.80 4.40 5 -5 -7 28.53 5.57 5 5 -6 297.41 16.79 -5 5 -6 342.02 17.04 5 -5 -6 274.44 16.39 5 -5 -6 313.13 17.90 5 5 -6 305.86 14.38 5 -5 -5 163.46 12.40 5 5 -5 172.65 13.00 -5 5 -5 175.60 12.05 5 5 -5 186.28 11.23 5 -5 -5 189.06 13.73 5 5 -4 17.28 4.11 -5 5 -4 6.56 2.30 5 5 -4 16.64 3.69 5 -5 -4 11.60 3.79 5 -5 -4 8.55 2.82 5 5 -3 42.76 6.32 5 5 -3 38.32 5.45 -5 5 -3 40.94 5.70 5 -5 -3 48.89 6.62 5 -5 -3 39.91 6.39 5 5 -2 35.87 5.88 5 5 -2 35.84 5.20 5 -5 -2 43.03 6.47 5 -5 -2 34.82 5.97 5 5 -1 69.18 8.30 5 5 -1 54.89 6.76 5 -5 -1 56.24 7.04 5 -5 -1 52.49 7.16 5 5 0 187.78 13.31 5 5 0 206.50 13.00 5 -5 0 196.27 13.05 5 -5 0 204.49 13.72 5 5 1 73.45 8.56 5 5 1 63.21 7.11 5 -5 1 70.79 7.61 5 -5 1 63.06 7.73 5 5 2 30.69 5.26 5 5 2 35.46 5.49 5 -5 2 34.19 5.88 5 -5 2 25.25 4.63 5 5 3 50.97 6.71 5 -5 3 39.94 6.11 5 5 3 36.98 5.55 5 -5 3 52.10 6.41 5 -5 4 12.39 3.31 5 5 4 10.91 3.31 5 5 4 12.67 3.70 5 -5 4 23.10 4.72 5 -5 5 176.93 12.21 5 5 5 151.10 11.91 5 5 5 184.49 13.04 5 -5 5 157.29 12.07 5 5 6 318.72 17.65 5 -5 6 342.05 17.91 5 5 6 358.56 18.24 5 -5 6 306.82 16.13 5 -5 7 24.30 4.59 5 5 7 33.19 5.71 5 5 7 24.35 5.43 5 -5 7 25.34 5.10 5 5 8 30.76 5.50 5 -5 8 23.04 5.03 5 5 8 26.51 5.46 5 -5 8 23.75 4.55 5 -5 9 116.30 10.51 5 5 9 97.38 10.27 5 5 9 106.60 10.29 5 -5 9 108.54 9.75 5 -5 10 44.64 6.31 5 5 10 51.09 7.40 5 5 10 55.52 7.76 5 -5 11 200.30 14.01 5 5 11 175.03 13.71 5 5 11 207.98 14.54 5 -5 12 26.40 5.17 5 5 12 20.56 4.53 5 5 12 22.66 5.66 5 -5 13 7.24 3.32 5 5 13 3.05 2.14 5 5 13 2.17 2.16 5 5 14 48.02 7.27 5 -5 14 65.83 8.31 5 5 14 60.64 8.06 5 -5 15 138.21 12.05 5 5 15 156.85 13.18 5 5 15 152.93 13.53 5 5 16 -1.25 2.16 5 5 16 2.95 2.49 5 5 17 64.50 8.76 5 5 17 41.62 7.09 5 5 18 11.34 4.00 5 5 18 10.51 3.59 5 5 19 10.84 3.81 5 5 20 112.55 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-11 17.99 5.12 5 -6 -10 7.15 2.76 5 6 -10 3.19 1.42 -5 -6 -10 7.22 3.26 -5 6 -10 8.33 3.94 5 -6 -10 15.99 4.82 5 6 -9 42.12 6.87 -5 6 -9 32.96 5.76 5 -6 -9 33.19 6.29 5 -6 -9 44.95 7.32 5 6 -8 37.48 6.22 -5 6 -8 37.18 6.57 5 -6 -8 24.35 4.69 5 -6 -8 31.32 5.81 5 6 -7 96.38 8.71 -5 6 -7 91.90 9.40 5 -6 -7 84.93 9.63 5 6 -7 84.14 9.33 5 -6 -7 99.65 11.02 5 6 -6 6.93 2.81 5 6 -6 8.35 2.63 5 -6 -6 8.39 4.21 5 -6 -6 7.38 3.46 -5 6 -6 1.71 1.64 5 6 -5 14.02 3.45 -5 6 -5 11.88 3.27 5 6 -5 12.22 4.28 5 -6 -5 14.77 4.30 5 -6 -5 14.39 4.20 5 6 -4 102.89 9.40 -5 6 -4 112.10 10.47 5 -6 -4 115.35 10.75 5 6 -4 105.61 10.82 5 -6 -4 107.81 10.99 5 6 -3 23.56 4.51 -5 6 -3 24.78 5.08 5 6 -3 31.08 5.72 5 -6 -3 28.66 5.37 5 -6 -3 21.89 4.52 5 -6 -2 49.75 7.29 5 6 -2 76.09 8.44 -5 6 -2 56.18 7.61 5 -6 -2 66.85 8.60 5 6 -2 64.04 8.24 5 6 -1 79.65 9.20 5 6 -1 72.57 8.19 -5 6 -1 58.66 7.84 5 -6 -1 64.74 8.55 5 -6 -1 74.62 8.43 5 6 0 63.34 8.37 5 6 0 54.40 7.30 -5 6 0 63.26 8.14 5 -6 0 61.89 7.49 5 -6 0 61.20 8.27 5 6 1 68.67 8.79 5 6 1 71.33 8.02 -5 6 1 71.58 8.64 5 -6 1 66.24 7.89 5 -6 1 88.78 9.66 5 6 2 71.88 8.49 5 6 2 57.61 7.24 -5 6 2 54.62 7.54 5 -6 2 53.99 7.34 5 -6 2 65.32 8.31 5 -6 3 33.50 6.09 5 6 3 23.58 5.39 5 6 3 19.39 4.25 -5 6 3 22.49 5.30 5 -6 3 27.08 5.14 5 6 4 134.28 12.21 5 6 4 112.92 10.83 -5 6 4 121.88 11.40 5 -6 4 120.74 11.25 5 -6 4 99.09 9.78 5 -6 5 3.39 1.06 5 6 5 20.35 4.67 5 -6 5 16.82 4.38 5 6 5 18.46 4.40 5 -6 6 6.27 2.09 5 6 6 5.49 1.96 5 -6 6 5.05 2.44 5 6 6 7.97 2.06 5 6 7 95.15 10.45 5 6 7 94.08 10.11 5 -6 7 79.37 9.00 5 -6 7 101.38 10.07 5 6 8 22.84 4.86 5 6 8 34.03 6.16 5 -6 8 29.09 4.96 5 -6 8 41.32 6.71 5 6 9 42.44 7.20 5 6 9 31.81 6.17 5 -6 9 38.05 6.32 5 -6 9 47.07 7.16 5 -6 10 11.06 3.42 5 6 10 11.47 3.94 5 -6 10 10.62 3.29 5 6 10 8.13 3.24 5 -6 11 13.20 3.31 5 6 11 10.42 3.48 5 6 11 15.73 4.25 5 -6 11 17.84 4.80 5 6 12 67.89 8.87 -5 6 12 68.63 9.49 5 -6 12 86.21 9.89 5 -6 12 68.92 8.46 5 6 12 82.40 9.70 5 -6 13 17.68 4.49 5 6 13 20.44 4.87 5 6 13 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25.38 6.38 5 -7 -14 27.77 6.12 -5 -7 -13 38.56 6.73 5 -7 -13 19.93 5.46 5 7 -13 31.51 6.70 5 -7 -13 23.74 6.26 5 7 -12 30.82 6.48 -5 -7 -12 32.02 6.78 5 -7 -12 24.89 5.68 5 -7 -12 23.72 5.12 5 7 -11 90.54 10.93 -5 -7 -11 90.39 10.15 5 -7 -11 102.45 11.63 5 -7 -11 107.98 12.11 5 7 -10 148.83 13.71 -5 7 -10 125.21 11.91 5 -7 -10 155.02 14.00 5 -7 -10 127.64 13.12 5 -7 -9 87.53 10.06 5 7 -9 90.62 10.53 -5 7 -9 89.34 10.31 5 -7 -9 89.36 10.96 5 7 -8 86.21 10.50 -5 7 -8 81.19 9.71 5 -7 -8 94.44 10.59 5 -7 -8 86.10 10.59 5 -7 -7 112.89 11.12 5 7 -7 102.09 11.27 -5 7 -7 111.53 11.27 5 -7 -7 104.32 11.44 5 7 -6 43.35 7.75 5 7 -6 49.78 7.70 5 -7 -6 32.90 5.98 -5 7 -6 57.04 8.20 5 -7 -6 44.30 7.06 5 7 -5 112.83 11.80 5 -7 -5 111.49 11.62 5 7 -5 106.34 10.19 -5 7 -5 143.08 12.66 5 -7 -5 94.33 10.27 5 7 -4 41.22 7.47 5 7 -4 40.14 6.73 -5 7 -4 44.72 7.32 5 -7 -4 42.12 7.44 5 -7 -4 43.69 7.29 5 -7 -3 6.21 2.44 5 7 -3 9.04 2.97 -5 7 -3 5.08 3.30 5 -7 -3 8.60 3.63 5 7 -3 3.64 2.52 5 7 -2 41.12 6.96 5 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3 5 436.81 18.21 6 -3 5 419.30 18.11 6 3 6 336.43 15.73 6 -3 6 346.33 16.51 6 3 6 342.80 16.58 6 3 7 330.00 15.53 6 3 7 331.53 16.70 6 -3 7 342.31 16.59 6 3 8 62.33 7.08 6 3 8 68.32 7.24 6 -3 8 58.39 7.00 6 3 9 69.21 7.19 6 -3 9 64.64 7.19 6 3 10 25.68 4.32 6 -3 10 27.89 4.81 6 3 10 18.34 3.24 6 3 11 172.22 11.59 6 -3 11 154.10 11.44 6 3 11 155.34 11.78 6 3 12 63.29 7.01 6 -3 12 69.70 7.87 6 3 12 81.82 8.85 6 3 13 61.85 6.99 6 -3 13 62.22 7.29 6 3 13 74.97 8.54 6 3 14 186.88 12.20 6 -3 14 185.52 13.26 6 3 14 178.34 13.55 6 3 15 24.58 5.52 6 3 15 31.12 4.91 6 -3 15 26.85 4.89 6 3 16 46.60 6.20 6 -3 16 39.45 6.25 6 3 16 48.66 7.63 6 -3 17 126.91 11.46 6 3 17 115.18 11.78 6 -3 18 53.03 7.82 6 3 18 47.72 7.68 6 -3 19 121.46 11.40 6 3 19 110.30 12.20 6 3 20 33.41 7.09 6 3 21 10.28 3.47 6 3 22 4.22 3.26 6 3 23 6.03 3.44 6 3 24 9.73 3.80 6 3 25 36.43 7.46 6 3 26 13.34 5.30 6 -4 -27 3.99 4.40 6 -4 -26 10.70 4.01 6 -4 -25 5.71 2.54 6 -4 -24 53.84 9.94 6 -4 -23 23.25 6.23 6 -4 -22 33.83 6.99 6 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72.45 8.32 6 4 -5 519.54 21.53 6 -4 -5 531.85 22.48 6 4 -5 497.31 17.79 6 4 -5 506.63 12.23 6 -4 -5 519.83 21.86 6 -4 -4 1.88 1.15 6 4 -4 2.93 1.37 6 4 -4 3.63 1.25 6 -4 -4 -1.35 0.83 6 4 -4 1.04 2.02 6 4 -3 184.32 12.66 6 4 -3 201.62 8.67 6 -4 -3 187.24 13.23 6 4 -3 208.13 11.73 6 -4 -3 196.69 13.22 6 4 -2 108.40 9.50 6 -4 -2 121.97 10.44 6 4 -2 95.44 8.26 6 -4 -2 105.77 9.96 6 4 -1 73.21 7.59 6 -4 -1 67.75 7.60 6 4 -1 86.42 7.72 6 -4 -1 79.37 8.42 6 -4 0 133.75 11.08 6 4 0 143.69 10.89 6 -4 0 140.47 10.91 6 4 0 156.08 10.82 6 4 1 83.83 8.58 6 -4 1 88.48 8.65 6 4 1 89.11 8.21 6 -4 1 74.82 8.06 6 4 2 100.57 8.78 6 -4 2 114.99 9.95 6 4 2 112.37 9.97 6 -4 2 106.19 9.67 6 -4 3 188.21 12.96 6 4 3 198.34 13.00 6 4 3 201.44 12.64 6 -4 3 219.89 13.63 6 -4 4 2.11 0.76 6 4 4 1.14 2.61 6 -4 4 1.56 1.16 6 4 4 1.86 1.53 6 -4 5 490.36 20.75 6 4 5 510.49 21.24 6 -4 5 494.13 20.55 6 -4 6 69.58 7.79 6 4 6 66.55 7.71 6 -4 6 78.62 8.29 6 4 6 70.53 8.10 6 -4 7 27.13 5.15 6 4 7 33.39 5.48 6 4 7 18.79 3.63 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8.94 6 -5 -3 77.12 8.74 6 5 -3 89.15 8.37 6 5 -2 74.47 8.39 6 -5 -2 58.54 7.68 6 -5 -2 64.82 7.52 6 5 -2 63.97 7.18 6 5 -1 18.40 3.66 6 5 -1 25.47 5.42 6 -5 -1 20.17 4.13 6 -5 -1 23.94 5.38 6 -5 0 17.86 4.05 6 5 0 18.12 3.77 6 5 0 19.69 4.56 6 -5 0 20.61 4.02 6 -5 1 20.81 4.86 6 5 1 21.20 5.09 6 5 1 22.61 4.45 6 -5 1 23.75 4.89 6 5 2 59.65 7.49 6 5 2 56.77 7.71 6 -5 2 64.59 7.80 6 -5 2 60.92 7.98 6 5 3 73.00 8.16 6 5 3 86.30 9.22 6 -5 3 80.43 8.77 6 -5 3 69.97 8.10 6 5 4 82.01 8.81 6 5 4 75.62 8.56 6 -5 4 86.81 9.19 6 -5 4 75.11 8.57 6 -5 5 38.56 5.94 6 -5 5 35.79 6.13 6 5 5 34.28 5.73 6 5 5 33.44 5.54 6 -5 6 6.10 2.32 6 5 6 7.60 1.87 6 5 6 8.80 2.91 6 -5 6 9.23 3.62 6 -5 7 12.71 3.84 6 5 7 9.84 3.46 6 5 7 23.98 5.07 6 -5 7 13.28 3.76 6 -5 8 20.50 4.46 6 5 8 28.77 5.14 6 5 8 30.77 5.66 6 -5 8 18.75 4.69 6 5 9 27.38 5.03 6 5 9 26.65 5.20 6 -5 9 22.40 5.42 6 -5 9 32.44 5.19 6 5 10 7.10 3.14 6 -5 10 4.95 1.71 6 5 10 9.61 3.09 6 5 11 3.85 3.16 6 5 11 3.04 2.23 6 -5 11 1.63 1.15 6 5 12 6.24 3.52 6 5 12 12.22 3.79 6 -5 12 7.22 3.11 6 -5 13 66.17 8.56 6 5 13 56.60 7.49 6 5 13 78.22 9.61 6 5 14 12.06 3.20 6 -5 14 19.47 5.27 6 5 14 16.11 4.70 6 5 15 10.26 3.68 6 -5 15 16.01 5.31 6 5 15 13.28 5.12 6 5 16 4.95 1.73 6 -5 16 13.48 4.82 6 5 16 11.41 4.25 6 5 17 30.15 6.06 6 5 17 22.80 5.71 6 5 18 12.95 4.50 6 5 18 8.46 3.39 6 5 19 6.74 4.05 6 5 20 2.13 2.22 6 5 21 12.64 4.14 6 5 22 13.47 3.85 6 5 23 -0.61 2.33 -6 5 23 -1.38 2.06 6 5 24 -1.53 2.38 6 5 25 16.68 6.24 6 5 26 2.88 2.76 6 -6 -25 14.07 4.83 6 -6 -24 46.06 9.02 6 -6 -23 -1.38 3.46 6 -6 -22 102.47 12.34 6 -6 -21 21.48 5.92 6 -6 -21 24.49 5.55 6 -6 -20 -2.39 1.98 6 -6 -20 10.36 5.15 6 -6 -19 26.34 6.16 6 -6 -19 29.15 7.04 6 -6 -18 187.20 16.13 6 -6 -18 160.22 15.90 6 -6 -17 16.54 4.73 6 -6 -17 18.93 5.21 6 6 -16 -0.08 1.89 6 -6 -16 3.97 2.09 6 -6 -16 0.05 1.75 6 6 -15 7.60 2.99 6 -6 -15 10.59 3.82 6 -6 -15 11.97 4.43 6 6 -14 2.87 1.28 6 -6 -14 5.46 4.11 6 -6 -14 6.37 3.74 6 6 -13 14.99 5.22 6 -6 -13 16.42 4.02 6 -6 -13 12.78 4.77 6 -6 -12 132.53 12.84 6 6 -12 159.64 13.90 6 -6 -12 136.56 13.30 6 -6 -11 33.61 6.17 6 6 -11 31.48 6.33 6 -6 -11 17.72 4.82 6 6 -10 0.64 2.48 -6 6 -10 6.69 4.08 6 -6 -10 0.77 2.09 6 -6 -10 2.11 2.10 6 6 -9 32.51 6.11 -6 6 -9 35.37 6.43 6 -6 -9 28.17 5.81 6 -6 -9 36.46 6.77 6 6 -8 359.10 20.13 -6 6 -8 330.08 18.66 6 -6 -8 393.05 21.48 6 -6 -8 360.28 20.98 6 6 -7 67.47 8.81 -6 6 -7 78.38 9.13 6 -6 -7 72.62 9.40 6 6 -7 71.86 8.07 6 -6 -7 67.16 9.34 6 6 -6 -0.19 2.62 6 -6 -6 3.69 2.49 6 6 -6 0.85 0.80 -6 6 -6 0.14 2.10 6 -6 -6 -1.59 1.62 6 6 -5 49.78 6.62 6 6 -5 51.92 7.68 -6 6 -5 51.62 7.48 6 -6 -5 54.26 8.34 6 -6 -5 55.66 8.08 6 6 -4 160.65 13.42 6 6 -4 165.73 12.25 -6 6 -4 173.82 13.38 6 -6 -4 177.26 13.93 6 -6 -4 153.84 13.42 6 6 -3 -1.71 2.59 6 6 -3 4.36 2.68 6 -6 -3 0.47 1.66 -6 6 -3 2.97 2.61 6 -6 -3 5.41 2.63 6 6 -2 307.20 16.91 6 6 -2 308.07 18.44 -6 6 -2 304.11 17.72 6 -6 -2 318.70 18.88 6 -6 -2 322.89 18.55 6 6 -1 76.64 8.65 6 6 -1 60.28 8.41 6 -6 -1 72.63 8.78 -6 6 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12.36 4.59 6 -6 13 16.60 4.68 6 6 14 3.04 2.70 6 -6 14 2.04 1.75 6 6 14 1.00 2.67 6 6 15 10.83 4.37 6 -6 15 17.60 4.49 6 6 15 16.94 3.98 6 6 16 1.78 3.01 6 6 16 0.90 1.25 6 6 17 26.35 5.41 6 6 17 13.97 4.11 6 6 18 198.12 16.50 -6 6 18 145.51 14.24 6 6 18 186.59 16.11 -6 6 19 30.05 7.54 6 6 19 11.48 4.55 -6 6 20 3.34 4.39 6 6 20 -3.32 3.52 6 6 21 20.34 6.59 -6 6 21 32.28 7.09 -6 6 22 96.14 12.71 6 6 22 85.87 11.77 -6 6 23 9.71 3.90 6 6 23 4.92 3.94 6 6 24 39.80 8.44 6 6 25 23.05 7.09 6 -7 -23 6.85 3.29 6 -7 -22 0.15 1.71 6 -7 -21 43.98 8.45 6 -7 -21 28.33 6.60 6 -7 -20 10.89 4.64 6 -7 -20 6.46 2.85 6 -7 -19 18.71 5.66 6 -7 -19 18.50 5.56 6 -7 -18 37.90 7.77 6 -7 -18 28.92 6.77 6 -7 -17 6.86 3.69 6 -7 -17 10.26 3.83 6 -7 -16 11.95 4.28 6 -7 -16 19.78 6.23 6 7 -15 25.14 5.68 6 -7 -15 21.17 5.50 6 -7 -15 22.96 5.40 6 -7 -14 3.26 1.96 6 7 -14 8.77 4.78 6 -7 -14 10.66 4.22 6 7 -13 46.01 8.36 6 -7 -13 27.89 6.49 6 -7 -13 36.07 7.61 6 -7 -12 14.48 5.31 6 -7 -12 12.63 5.39 6 7 -12 15.58 4.61 6 7 -11 9.17 3.83 6 -7 -11 14.10 5.10 6 -7 -11 6.25 3.18 6 -7 -10 57.35 8.81 6 7 -10 49.35 8.28 6 -7 -10 44.76 8.27 6 7 -9 3.04 1.32 6 -7 -9 6.85 3.36 6 -7 -9 8.36 3.94 -6 7 -9 6.13 2.96 6 7 -8 68.40 9.48 -6 7 -8 64.07 8.46 6 -7 -8 70.92 9.26 6 -7 -8 75.66 9.74 6 7 -7 29.02 6.90 -6 7 -7 15.01 4.68 6 -7 -7 14.69 5.76 6 -7 -7 22.72 6.03 6 7 -6 5.31 1.95 -6 7 -6 8.36 3.15 6 -7 -6 9.68 4.23 6 -7 -6 5.83 3.25 6 7 -5 28.34 6.48 6 7 -5 25.92 5.54 6 -7 -5 17.66 5.31 -6 7 -5 33.37 6.37 6 -7 -5 23.84 5.97 6 7 -4 100.75 10.39 6 7 -4 110.15 11.48 -6 7 -4 93.86 10.73 6 -7 -4 85.52 10.25 6 -7 -4 95.17 10.77 6 7 -3 48.55 7.53 6 7 -3 38.33 6.79 -6 7 -3 39.32 6.69 6 -7 -3 46.27 7.02 6 -7 -3 42.60 7.35 6 7 -2 107.51 10.92 6 7 -2 119.45 12.28 -6 7 -2 128.43 12.47 6 -7 -2 129.11 12.54 6 -7 -2 122.02 12.24 -6 7 -1 18.41 5.52 6 7 -1 15.31 4.03 6 7 -1 16.29 4.67 6 -7 -1 12.56 4.15 6 -7 -1 16.32 5.23 6 -7 0 3.01 2.22 6 7 0 8.53 4.19 6 -7 0 7.00 4.38 -6 7 0 4.98 2.98 6 7 0 4.00 2.36 6 -7 1 11.91 4.14 6 7 1 7.83 2.81 6 7 1 19.57 4.38 -6 7 1 16.14 4.41 6 -7 1 14.52 4.92 6 7 2 141.19 12.60 6 7 2 118.65 11.55 -6 7 2 102.87 11.29 6 -7 2 145.67 12.98 6 -7 2 137.54 12.82 6 -7 3 32.88 6.11 6 7 3 48.57 7.88 6 7 3 25.59 5.65 6 -7 3 26.49 5.18 -6 7 3 34.56 6.51 6 7 4 99.89 11.09 6 7 4 110.96 11.28 -6 7 4 90.45 10.53 6 -7 4 74.44 9.54 6 -7 4 73.41 9.02 6 -7 5 16.81 4.61 6 -7 5 28.84 6.51 -6 7 5 22.07 6.10 6 7 5 18.08 4.78 6 7 5 17.68 4.81 6 -7 6 3.40 2.10 6 7 6 4.30 3.43 6 7 6 7.69 1.81 -6 7 6 8.45 3.66 6 -7 6 4.03 1.13 6 7 7 14.69 4.88 6 -7 7 17.08 4.56 -6 7 7 19.42 4.90 6 -7 7 17.16 5.46 6 7 7 11.31 4.29 6 7 8 67.51 8.84 6 7 8 69.91 9.55 6 -7 8 78.50 9.76 6 -7 8 72.73 9.53 -6 7 8 57.54 8.46 6 -7 9 13.92 5.07 -6 7 9 9.34 2.84 6 7 9 7.17 3.97 6 7 9 3.48 2.15 6 -7 9 0.62 2.97 6 7 10 35.99 6.57 6 7 10 40.78 6.95 -6 7 10 46.73 7.65 6 -7 10 50.87 8.16 6 7 11 14.76 4.40 6 7 11 16.29 4.37 6 -7 11 19.22 5.49 -6 7 11 6.92 2.68 6 -7 12 12.01 4.92 6 7 12 11.19 3.89 6 7 12 4.59 2.56 -6 7 12 13.63 4.47 6 7 13 44.85 8.16 6 7 13 48.27 8.10 -6 7 13 36.55 6.96 6 -7 13 40.24 7.94 -6 7 14 8.11 3.74 6 7 14 10.94 4.35 6 7 14 12.84 5.29 -6 7 15 19.84 5.58 6 7 15 11.45 3.96 6 7 15 11.17 4.64 6 7 16 13.63 3.70 6 7 16 13.62 5.43 -6 7 16 22.10 5.94 6 7 17 9.47 4.46 6 7 17 14.61 5.16 -6 7 17 6.25 3.22 6 7 18 50.91 9.20 -6 7 18 28.29 7.33 6 7 18 42.91 7.87 6 7 19 9.37 3.26 -6 7 19 19.61 5.56 -6 7 20 11.23 5.40 6 7 20 15.40 5.56 6 7 21 18.49 5.37 -6 7 21 37.21 8.33 6 7 22 1.65 2.58 -6 7 22 -2.41 2.75 -6 7 23 0.26 2.65 6 7 23 2.91 4.23 6 -8 -20 15.39 5.30 6 -8 -20 3.45 3.46 6 -8 -19 21.00 5.38 6 -8 -19 15.45 5.56 6 -8 -18 44.79 8.53 6 -8 -18 44.18 8.93 6 -8 -17 13.04 5.09 6 -8 -17 13.39 4.10 6 -8 -16 18.01 4.86 6 -8 -16 14.40 4.53 6 -8 -15 22.35 5.90 6 -8 -15 19.48 5.46 6 8 -14 36.62 8.08 6 -8 -14 31.46 7.23 6 -8 -14 35.26 6.78 6 -8 -13 44.04 8.05 6 8 -13 55.36 9.04 6 -8 -13 47.33 8.78 6 8 -12 39.76 7.34 6 -8 -12 44.42 7.55 6 -8 -12 37.87 8.00 6 8 -11 20.42 5.23 6 -8 -11 33.90 6.45 6 -8 -11 27.70 7.25 6 8 -10 25.96 6.12 6 -8 -10 24.27 5.75 6 8 -9 10.76 3.69 -6 8 -9 23.84 6.78 6 -8 -9 14.63 5.05 6 -8 -9 17.10 5.27 6 8 -8 103.99 11.82 -6 8 -8 115.97 12.84 6 -8 -8 91.54 11.27 6 -8 -8 97.60 11.67 6 8 -7 50.24 8.33 -6 8 -7 49.33 8.39 6 -8 -7 54.28 8.88 6 -8 -7 34.74 6.77 6 -8 -6 13.81 4.20 6 8 -6 10.78 3.63 -6 8 -6 16.87 4.86 6 -8 -6 15.55 5.37 6 8 -5 40.52 7.38 -6 8 -5 34.19 7.37 6 -8 -5 49.25 8.08 6 -8 -5 36.20 7.44 6 8 -4 58.65 8.97 -6 8 -4 68.16 9.40 6 8 -4 42.28 7.15 6 -8 -4 51.15 8.15 6 -8 -4 70.81 9.60 6 8 -3 2.64 1.29 6 8 -3 -0.28 1.88 -6 8 -3 6.37 3.60 6 -8 -3 -0.84 1.48 6 -8 -3 3.32 3.50 6 8 -2 60.80 9.11 6 8 -2 77.32 9.57 -6 8 -2 86.21 10.44 6 -8 -2 65.19 10.14 6 -8 -2 69.04 9.33 6 -8 -1 11.33 3.66 6 8 -1 12.38 4.22 -6 8 -1 15.43 4.54 6 8 -1 15.08 4.57 6 -8 -1 22.07 5.53 6 -8 0 1.80 3.06 6 8 0 0.56 1.65 -6 8 0 4.81 3.67 6 8 0 4.40 2.38 6 -8 0 -3.17 3.66 6 8 1 31.98 6.75 -6 8 1 21.54 5.25 6 -8 1 17.29 4.63 6 8 1 26.26 5.53 6 -8 1 16.99 5.17 6 8 2 82.52 10.67 6 8 2 69.35 9.29 -6 8 2 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2.46 6 -9 -3 1.11 1.71 6 9 -2 4.06 2.61 -6 9 -2 3.59 4.12 6 9 -2 0.93 1.88 6 -9 -2 3.13 3.27 6 9 -1 11.80 4.42 -6 9 -1 14.44 5.32 6 9 -1 9.77 4.03 6 -9 -1 20.77 5.51 -6 9 0 7.68 3.68 6 9 0 12.00 4.36 6 9 0 15.80 5.32 6 -9 0 12.21 5.05 6 9 1 20.17 5.36 6 9 1 9.67 3.70 6 -9 1 20.28 5.26 -6 9 1 7.84 2.70 6 9 2 0.58 1.70 6 9 2 2.56 2.75 -6 9 2 0.91 2.97 6 -9 2 -0.83 2.93 6 9 3 5.38 2.94 -6 9 3 4.09 3.21 6 9 3 5.99 2.94 6 -9 3 12.03 4.71 6 9 4 1.62 3.71 6 9 4 3.01 3.47 -6 9 4 2.12 2.78 6 -9 4 3.62 2.97 6 9 5 13.18 4.16 -6 9 5 16.22 4.93 6 9 5 14.13 3.85 6 -9 5 16.32 5.39 6 9 6 16.06 4.97 -6 9 6 14.25 5.00 6 -9 6 23.70 6.39 6 9 6 17.20 5.12 6 9 7 4.25 3.44 6 9 7 11.65 4.54 -6 9 7 11.00 4.41 6 -9 7 14.40 5.07 6 9 8 10.99 3.90 6 9 8 8.38 2.56 -6 9 8 17.31 5.41 6 -9 8 7.62 3.96 6 9 9 3.73 1.98 6 9 9 10.54 4.71 -6 9 9 12.07 3.89 6 9 10 2.35 2.38 6 -9 10 6.82 3.53 6 9 10 4.24 3.27 -6 9 10 12.34 5.05 6 9 11 4.71 3.76 6 9 11 0.10 2.69 -6 9 11 -1.58 2.93 6 9 12 21.79 6.94 6 9 12 12.90 4.71 -6 9 12 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4.08 2.92 7 -5 -13 -0.45 2.77 7 -5 -13 2.39 2.61 7 -5 -12 241.43 17.41 7 -5 -12 209.16 16.09 7 5 -12 230.75 16.11 7 5 -11 55.71 8.10 7 -5 -11 37.66 7.19 7 -5 -11 38.57 6.82 7 5 -10 7.77 2.76 7 -5 -10 7.93 2.62 -7 5 -10 4.87 2.47 7 -5 -10 6.32 2.97 7 5 -9 24.39 5.69 7 -5 -9 8.18 3.49 7 -5 -9 18.37 4.20 -7 5 -9 11.75 3.40 7 5 -8 260.70 16.72 -7 5 -8 276.56 15.57 7 -5 -8 251.76 17.05 7 -5 -8 266.82 17.49 7 5 -7 64.13 7.91 7 5 -7 63.28 6.85 7 -5 -7 55.71 8.36 7 -5 -7 63.00 8.55 7 -5 -6 16.21 3.72 7 5 -6 17.52 4.35 7 5 -6 14.66 3.39 7 -5 -6 7.94 2.79 7 5 -5 33.19 5.76 7 -5 -5 43.86 6.97 7 5 -5 43.59 5.81 7 -5 -5 36.04 6.21 7 5 -4 57.29 7.66 7 -5 -4 62.03 8.17 7 5 -4 50.91 6.22 7 -5 -4 48.14 7.18 7 -5 -3 61.66 8.49 7 5 -3 61.30 7.30 7 5 -3 61.09 7.87 7 -5 -3 55.04 7.83 7 5 -2 291.68 17.37 7 5 -2 258.23 14.81 7 -5 -2 296.78 17.81 7 -5 -1 14.94 4.41 7 5 -1 6.08 2.49 7 -5 -1 12.65 2.93 7 5 -1 12.44 3.49 7 5 0 1.20 1.79 7 -5 0 -0.29 2.25 7 5 0 1.70 2.78 7 -5 0 1.40 1.57 7 -5 1 9.39 3.19 7 5 1 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191.22 16.43 -9 7 -5 174.57 15.11 9 -7 -5 161.42 15.02 9 -7 -4 2.72 2.04 9 7 -4 2.94 2.50 9 7 -4 -0.30 1.97 -9 7 -4 3.47 3.12 9 -7 -4 3.74 2.11 9 -7 -3 11.28 3.17 9 7 -3 30.07 6.18 9 7 -3 25.22 5.44 -9 7 -3 29.67 6.33 9 -7 -3 26.54 6.90 9 -7 -2 1.49 1.98 9 7 -2 1.91 2.94 9 7 -2 3.09 2.30 9 -7 -2 4.77 2.93 9 7 -1 137.48 13.70 9 7 -1 120.08 12.10 9 -7 -1 106.69 11.96 9 -7 -1 125.66 13.28 9 7 0 222.04 17.17 9 7 0 210.27 16.43 9 -7 0 176.38 15.53 9 -7 0 200.81 16.43 9 7 1 119.08 12.36 9 7 1 124.20 12.52 9 -7 1 137.44 14.19 9 -7 1 101.89 12.42 9 -7 2 4.41 4.15 9 7 2 -1.66 2.55 9 7 2 3.78 2.53 9 -7 2 7.56 5.29 9 7 3 27.31 5.92 9 -7 3 17.37 5.68 9 7 3 28.81 6.16 9 -7 3 19.74 5.82 9 -7 4 1.67 2.35 9 7 4 2.69 2.44 9 7 4 1.54 2.59 9 -7 4 -0.68 2.48 9 7 5 183.42 15.74 9 7 5 182.43 15.34 9 -7 5 167.46 15.78 9 -7 5 144.73 14.35 9 7 6 54.40 8.40 9 -7 6 54.02 8.98 9 7 6 37.10 7.88 9 -7 6 54.48 8.58 9 -7 7 3.30 1.41 9 7 7 2.23 2.50 9 7 7 7.95 3.53 9 -7 7 9.04 4.20 9 -7 8 21.04 6.17 9 7 8 5.78 4.14 9 7 8 11.79 4.15 9 -7 8 8.59 4.17 9 -7 9 38.65 7.63 9 7 9 42.22 7.65 9 7 9 41.40 7.30 9 -7 9 39.78 7.84 9 -7 10 19.95 5.69 9 7 10 15.61 4.53 9 7 10 11.54 4.01 9 -7 10 15.81 3.91 9 7 11 159.50 14.77 9 7 11 160.77 15.31 9 -7 11 138.68 14.61 9 -7 11 158.34 15.16 9 -7 12 8.64 4.58 9 7 12 11.78 4.52 9 7 12 6.17 3.41 9 -7 12 10.60 5.48 9 -7 13 11.18 4.44 9 7 13 1.28 3.75 9 7 13 7.50 3.79 9 -7 14 4.44 3.41 9 7 14 1.52 3.82 9 7 14 1.27 2.34 9 7 15 107.33 12.94 9 7 15 107.99 12.74 9 -7 15 144.45 15.05 9 7 16 2.69 2.99 9 7 16 5.04 3.85 9 7 17 16.94 3.93 9 7 17 19.77 6.87 9 7 18 -1.41 1.76 9 7 19 3.24 2.24 9 7 20 15.34 5.62 -9 7 20 7.66 1.95 9 7 21 22.32 7.27 -9 7 21 30.50 8.35 9 -8 -18 5.19 3.13 9 -8 -18 3.33 4.08 9 -8 -17 -1.27 4.13 9 -8 -17 -2.43 1.57 9 8 -16 -3.13 2.48 9 -8 -16 -2.13 3.85 9 -8 -16 -2.45 3.05 9 8 -15 0.84 2.38 9 -8 -15 3.02 2.24 9 -8 -15 5.66 4.17 9 8 -14 1.65 2.18 9 -8 -14 2.04 3.12 9 -8 -14 1.79 2.05 9 8 -13 4.67 3.91 9 -8 -13 -1.92 2.45 9 -8 -13 -0.28 2.29 9 -8 -12 -0.52 1.50 9 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9.33 4.89 9 10 7 15.28 5.91 9 -10 7 11.82 6.32 9 10 8 55.54 9.98 -9 10 8 30.83 7.75 9 10 8 50.82 9.37 9 -10 8 36.25 8.39 10 0 -25 28.07 6.27 10 0 -24 46.43 8.31 10 0 -23 104.88 12.54 10 0 -22 32.17 7.09 10 0 -21 142.26 14.14 10 0 -20 40.10 8.35 10 0 -19 59.98 9.48 10 0 -18 174.74 15.05 10 0 -17 217.20 16.83 10 0 -16 81.11 10.45 10 0 -15 255.19 17.48 10 0 -14 118.22 12.56 10 0 -13 208.80 15.64 10 0 -12 261.99 15.61 10 0 -12 285.03 18.29 10 0 -11 241.40 14.77 10 0 -11 273.61 17.66 10 0 -10 82.23 8.50 10 0 -10 89.63 10.14 10 0 -9 209.63 13.47 10 0 -9 213.82 14.91 10 0 -8 218.47 13.76 10 0 -8 176.00 13.68 10 0 -7 125.01 10.45 10 0 -7 132.75 12.04 10 0 -7 144.13 12.04 10 0 -6 57.46 7.05 10 0 -6 63.57 7.93 10 0 -6 56.84 7.75 10 0 -5 205.60 13.44 10 0 -5 203.77 14.31 10 0 -5 236.51 14.86 10 0 -4 279.86 15.74 10 0 -4 267.22 16.60 10 0 -4 246.64 15.31 10 0 -3 210.82 13.61 10 0 -3 224.43 15.17 10 0 -3 237.53 14.66 10 0 -2 187.68 12.75 10 0 -2 195.78 13.97 10 0 -2 187.47 13.28 10 0 -1 110.99 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13.33 3.83 10 1 -6 26.56 5.22 10 -1 -5 0.77 1.43 10 -1 -5 0.37 1.25 10 1 -5 0.41 0.87 10 1 -5 2.28 1.97 10 1 -5 0.07 1.48 10 -1 -4 3.33 2.13 10 -1 -4 4.62 1.77 10 1 -4 5.21 2.66 10 1 -4 1.72 1.20 10 1 -4 3.95 1.53 10 -1 -3 8.24 2.82 10 -1 -3 9.63 3.02 10 1 -3 6.44 3.02 10 1 -3 6.07 2.25 10 1 -3 4.26 2.83 10 1 -2 8.40 2.86 10 -1 -2 5.53 2.39 10 -1 -2 2.70 1.96 10 1 -2 4.50 2.61 10 1 -2 5.66 1.45 10 -1 -1 44.30 6.62 10 1 -1 30.11 5.08 10 1 -1 31.85 5.28 10 -1 -1 32.44 5.61 10 1 -1 28.59 5.24 10 1 0 24.79 4.60 10 -1 0 23.27 5.19 10 -1 0 23.69 5.16 10 1 0 19.36 4.57 10 1 0 10.23 3.54 10 -1 1 27.05 5.17 10 1 1 29.51 5.09 10 -1 1 30.30 5.79 10 1 1 31.82 5.22 10 1 2 9.32 2.92 10 1 2 10.13 2.78 10 -1 2 7.23 2.47 10 -1 2 7.21 2.64 10 1 3 3.20 1.97 10 1 3 8.21 3.60 10 -1 3 5.56 3.19 10 1 4 3.93 2.73 10 1 4 1.66 1.43 10 -1 4 3.31 0.84 10 1 5 0.63 1.43 10 1 5 0.72 1.21 10 -1 5 1.76 1.31 10 1 6 17.67 4.18 10 1 6 22.50 4.70 10 -1 6 19.37 4.66 10 1 7 35.07 6.12 10 1 7 27.66 5.02 10 -1 7 30.91 5.56 10 1 8 1.02 1.21 10 1 8 -1.98 2.19 10 -1 8 -0.62 2.29 10 1 9 10.09 3.38 10 1 9 8.67 4.02 10 -1 9 11.28 3.68 10 1 10 7.24 2.62 10 1 10 4.79 2.94 10 -1 10 1.72 1.52 10 1 11 1.29 2.53 10 -1 11 0.12 1.85 10 1 11 0.93 1.17 10 1 12 20.82 5.12 10 1 12 28.47 5.21 10 -1 12 19.40 4.64 10 1 13 24.26 5.40 10 1 13 30.73 5.16 10 -1 13 27.64 6.02 10 1 14 -0.04 1.87 10 -1 14 0.74 1.85 10 -1 15 15.65 4.88 10 1 15 10.72 3.21 10 1 16 11.31 4.75 10 -1 16 2.10 1.86 10 1 17 9.53 3.41 10 -1 17 8.99 4.29 10 1 18 6.76 3.34 10 -1 18 6.09 4.05 10 1 19 4.90 2.73 10 -1 19 9.61 3.86 10 1 20 0.92 3.42 10 -1 20 5.89 2.55 10 1 21 1.82 1.37 10 -1 21 3.98 3.18 10 1 22 9.32 3.94 10 -1 22 -0.52 3.79 10 1 23 -0.34 2.68 10 -1 23 3.18 2.64 10 1 24 4.19 2.71 10 1 25 10.04 2.34 10 -2 -26 11.91 5.02 10 -2 -25 13.55 5.11 10 -2 -24 28.35 7.02 10 -2 -23 22.99 6.55 10 -2 -22 22.60 6.58 10 -2 -21 36.02 7.82 10 -2 -20 11.81 4.11 10 -2 -19 40.43 7.30 10 -2 -18 114.10 12.31 10 -2 -17 115.27 12.31 10 -2 -16 58.76 8.98 10 2 -16 43.78 7.38 10 2 -15 127.16 12.02 10 -2 -15 137.85 13.45 10 2 -15 129.05 12.71 10 2 -14 91.85 10.08 10 -2 -14 105.04 12.04 10 -2 -14 93.61 10.64 10 2 -14 91.56 10.44 10 2 -13 87.63 9.46 10 -2 -13 76.05 10.26 10 2 -13 91.20 9.95 10 -2 -13 68.12 8.83 10 2 -12 184.21 13.66 10 -2 -12 196.49 15.87 10 2 -12 185.45 14.55 10 -2 -12 168.85 13.71 10 2 -11 356.65 18.88 10 -2 -11 366.26 21.39 10 2 -11 361.19 19.86 10 -2 -11 349.70 19.34 10 2 -10 86.11 8.83 10 2 -10 94.72 9.82 10 -2 -10 102.00 11.04 10 2 -10 116.65 11.32 10 -2 -10 101.17 10.40 10 -2 -9 155.66 13.15 10 2 -9 158.53 11.13 10 -2 -9 158.39 13.73 10 2 -9 181.08 13.22 10 2 -9 183.67 13.85 10 -2 -8 214.02 15.15 10 2 -8 171.31 12.00 10 -2 -8 178.47 14.39 10 2 -8 190.29 13.46 10 2 -8 201.86 14.83 10 -2 -7 74.19 8.52 10 2 -7 86.83 8.35 10 -2 -7 86.30 9.97 10 2 -7 78.84 8.57 10 2 -7 90.66 9.59 10 -2 -6 73.53 8.57 10 2 -6 81.97 8.11 10 -2 -6 72.17 9.19 10 2 -6 94.82 9.70 10 2 -6 98.65 10.09 10 2 -5 248.25 14.34 10 -2 -5 254.99 16.93 10 2 -5 254.10 15.38 10 2 -5 226.39 15.03 10 -2 -4 135.43 11.50 10 -2 -4 139.67 12.55 10 2 -4 160.51 11.43 10 2 -4 149.65 11.86 10 2 -4 143.34 12.20 10 -2 -3 241.59 15.40 10 -2 -3 228.02 16.16 10 2 -3 215.51 13.68 10 2 -3 227.55 14.38 10 2 -3 232.62 15.26 10 -2 -2 386.19 19.97 10 -2 -2 367.47 19.99 10 2 -2 405.35 19.12 10 2 -2 379.66 18.22 10 2 -2 387.03 20.31 10 -2 -1 265.72 16.21 10 -2 -1 262.44 16.91 10 2 -1 258.69 15.46 10 2 -1 253.48 15.19 10 2 -1 252.05 16.66 10 -2 0 52.97 7.24 10 -2 0 50.11 7.77 10 2 0 52.67 7.14 10 2 0 59.00 8.31 10 -2 1 242.55 15.83 10 -2 1 274.49 17.21 10 2 1 268.14 15.57 10 2 1 271.82 15.83 10 -2 2 369.90 19.39 10 -2 2 362.25 20.00 10 2 2 336.16 18.12 10 2 2 384.03 18.91 10 -2 3 216.62 14.80 10 -2 3 238.96 16.19 10 2 3 255.25 15.37 10 2 3 224.47 14.68 10 -2 4 154.27 12.34 10 -2 4 144.09 12.69 10 2 4 148.98 11.86 10 2 4 141.32 11.87 10 2 5 224.15 15.24 10 -2 5 261.72 16.74 10 2 6 77.65 8.89 10 -2 6 77.96 9.02 10 2 6 84.71 8.94 10 2 7 69.25 8.74 10 -2 7 70.62 8.49 10 2 7 73.19 8.29 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9 12.83 4.29 10 3 9 5.97 2.51 10 3 10 30.27 5.75 10 -3 10 24.77 5.56 10 3 10 24.06 5.61 10 3 11 3.18 3.51 10 -3 11 2.67 2.38 10 3 11 3.83 2.22 10 3 12 12.36 4.20 10 -3 12 2.35 2.64 10 3 12 10.29 3.69 10 3 13 9.59 4.04 10 -3 13 18.84 4.32 10 3 13 8.62 3.38 10 3 14 -0.11 1.22 10 -3 14 0.81 2.75 10 3 14 -1.95 2.08 10 -3 15 -0.22 2.15 10 3 15 1.49 3.10 10 -3 16 4.00 3.82 10 3 16 6.49 2.61 10 -3 17 0.51 2.38 10 3 17 2.63 2.20 10 -3 18 0.18 2.07 10 3 18 1.48 2.58 10 3 19 -0.50 2.45 10 -3 19 -3.28 2.85 10 3 20 0.44 3.13 10 -3 20 -3.71 3.90 10 3 21 -1.20 3.39 10 3 22 2.62 3.84 10 3 23 4.16 1.94 10 3 24 5.51 2.98 10 3 25 3.38 2.68 10 3 26 3.85 2.23 10 -4 -25 29.29 7.76 10 -4 -24 26.01 5.69 10 -4 -23 7.42 4.25 10 -4 -22 25.18 6.72 10 -4 -21 38.60 7.59 10 -4 -20 6.29 4.08 10 -4 -19 34.25 7.11 10 4 -19 33.59 8.71 10 -4 -18 76.33 10.66 10 4 -18 60.35 9.46 10 -4 -17 49.88 8.50 10 -4 -17 61.91 9.22 10 4 -17 50.05 8.08 10 -4 -16 46.33 7.64 10 4 -16 43.21 8.24 10 -4 -16 27.60 6.84 10 -4 -15 72.69 10.33 10 -4 -15 77.23 10.48 10 4 -15 90.94 10.86 10 -4 -14 85.78 11.15 10 -4 -14 81.95 10.58 10 4 -14 84.34 10.47 10 -4 -13 55.62 9.07 10 -4 -13 57.92 8.88 10 4 -13 62.49 9.04 10 -4 -12 110.82 12.34 10 -4 -12 112.56 12.03 10 4 -12 135.37 13.42 10 -4 -11 223.09 17.10 10 -4 -11 197.63 16.15 10 4 -11 217.46 16.54 10 -4 -10 62.45 8.71 10 4 -10 59.49 8.76 10 -4 -9 70.92 9.61 10 -4 -9 72.68 9.65 10 4 -9 66.75 9.16 10 -4 -8 90.27 11.11 10 -4 -8 109.35 11.58 10 4 -8 97.60 11.20 10 4 -7 25.38 5.94 10 -4 -7 23.05 5.51 10 4 -7 26.10 4.94 10 -4 -7 29.16 6.36 10 -4 -6 40.21 7.62 10 4 -6 38.14 5.61 10 4 -6 41.79 7.45 10 -4 -6 48.38 7.61 10 -4 -5 147.48 13.17 10 -4 -5 156.52 14.05 10 4 -5 137.06 11.37 10 4 -5 146.81 12.56 10 4 -4 69.09 8.05 10 -4 -4 56.49 8.31 10 -4 -4 66.69 9.42 10 4 -4 69.76 8.47 10 -4 -3 74.22 9.26 10 4 -3 69.27 8.07 10 -4 -3 52.49 8.09 10 4 -3 58.76 7.19 10 4 -3 72.04 8.99 10 -4 -2 218.67 16.03 10 4 -2 190.02 13.61 10 -4 -2 229.31 16.81 10 4 -2 218.73 13.62 10 4 -2 240.70 16.60 10 4 -1 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42.80 7.35 10 5 3 14.27 4.10 10 5 3 13.07 4.39 10 -5 3 11.18 3.28 10 -5 3 15.91 5.48 10 5 4 39.82 7.51 10 -5 4 42.27 7.36 10 5 4 46.13 7.25 10 -5 4 32.78 6.85 10 5 5 13.05 4.16 10 5 5 9.24 2.99 10 -5 5 12.74 4.32 10 -5 5 11.41 4.00 10 5 6 3.38 2.60 10 5 6 6.18 2.85 10 -5 6 6.48 3.17 10 -5 6 8.32 3.99 10 5 7 21.27 5.34 10 5 7 15.64 5.00 10 -5 7 14.25 3.90 10 -5 7 22.38 5.50 10 5 8 27.17 5.32 10 5 8 20.70 5.51 10 -5 8 32.54 6.38 10 -5 8 31.00 6.97 10 5 9 4.24 2.68 10 5 9 2.86 1.59 10 -5 9 4.94 3.68 10 -5 9 5.39 3.81 10 5 10 6.78 3.31 10 5 10 25.99 5.74 10 -5 10 12.16 4.00 10 -5 10 24.66 5.36 10 5 11 6.05 3.98 10 5 11 10.58 4.88 10 -5 11 7.15 3.16 10 -5 11 5.16 3.62 10 5 12 5.50 3.32 10 5 12 6.87 4.26 10 -5 12 4.42 2.89 10 -5 12 3.41 4.11 10 5 13 0.50 2.09 10 5 13 -1.50 3.41 10 -5 13 -0.67 1.65 10 5 14 1.35 2.86 10 5 14 0.96 1.95 10 -5 14 6.23 3.82 10 5 15 14.92 4.69 10 5 15 20.95 5.60 10 -5 15 10.41 3.06 10 5 16 11.60 4.02 10 -5 16 9.50 3.85 10 -5 17 1.32 4.02 10 5 17 1.57 2.53 10 -5 18 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11.79 10 6 -5 92.73 10.19 10 -6 -5 88.17 11.51 10 -6 -5 88.70 11.37 10 6 -4 47.44 7.67 10 6 -4 67.15 8.71 10 -6 -4 69.97 9.32 10 -6 -4 45.38 8.59 10 -6 -3 10.30 4.27 10 6 -3 4.76 3.32 10 -6 -3 4.34 3.61 10 6 -3 1.60 2.08 10 6 -2 46.75 8.62 10 -6 -2 34.09 6.65 10 6 -2 33.69 6.30 10 -6 -2 48.95 9.00 10 6 -1 83.83 10.74 10 6 -1 100.17 10.45 10 -6 -1 95.14 11.15 10 -6 -1 93.72 10.98 10 6 0 93.79 11.01 10 6 0 89.33 10.49 10 -6 0 99.52 11.80 10 -6 0 73.16 10.19 10 6 1 90.10 10.62 10 -6 1 93.54 11.09 10 6 1 101.64 10.94 10 -6 1 101.11 11.56 10 6 2 50.27 7.83 10 -6 2 48.32 7.50 10 6 2 44.11 7.38 10 -6 2 50.68 8.60 10 6 3 3.77 2.21 10 6 3 3.46 2.13 10 -6 3 6.07 3.43 10 -6 3 5.65 3.41 10 -6 4 59.32 9.16 10 6 4 66.19 9.47 10 6 4 46.70 8.04 10 -6 4 47.29 8.52 10 -6 5 93.05 11.36 10 6 5 100.66 11.21 10 6 5 79.94 10.25 10 -6 5 105.30 12.40 10 6 6 33.35 6.61 10 6 6 31.31 6.37 10 -6 6 28.29 6.11 10 -6 6 50.03 8.40 10 6 7 9.82 4.01 10 6 7 9.98 3.60 10 -6 7 13.06 4.12 10 -6 7 16.98 5.05 10 6 8 62.07 9.53 10 -6 8 46.92 8.04 10 6 8 55.14 8.74 10 -6 8 75.99 11.05 10 -6 9 53.67 9.13 10 6 9 65.72 9.76 10 6 9 61.44 9.51 10 -6 9 52.33 8.92 10 6 10 41.69 7.99 10 6 10 30.13 6.99 10 -6 10 41.26 7.18 10 -6 10 46.40 8.74 10 -6 11 42.44 8.42 10 6 11 58.59 9.00 10 6 11 45.06 8.03 10 -6 11 40.81 8.88 10 6 12 39.09 7.91 10 6 12 39.90 7.48 10 -6 12 37.16 7.03 10 -6 12 43.73 8.30 10 6 13 60.32 8.66 10 6 13 43.25 7.58 10 -6 13 35.81 7.40 10 -6 13 63.26 10.21 10 -6 14 89.72 11.84 10 6 14 68.88 10.12 10 6 14 70.04 9.97 10 -6 14 63.25 9.55 10 -6 15 99.14 12.70 10 6 15 105.38 12.41 10 6 15 98.51 12.30 10 6 16 51.21 9.47 10 -6 16 42.39 8.71 10 6 16 50.48 8.81 10 -6 16 25.82 6.98 10 6 17 33.21 8.24 10 6 18 28.94 6.35 10 6 19 14.31 4.51 10 6 20 19.63 5.36 10 6 21 61.44 10.00 10 6 22 11.76 5.02 10 -7 -20 3.12 3.15 10 -7 -20 4.77 4.16 10 -7 -19 5.13 3.36 10 -7 -19 1.42 2.13 10 -7 -18 15.50 5.82 10 -7 -18 7.60 3.54 10 -7 -17 2.51 2.30 10 -7 -17 4.91 1.55 10 7 -16 9.13 3.04 10 -7 -16 15.99 5.35 10 -7 -16 5.02 3.33 10 7 -15 7.83 4.18 10 -7 -15 10.88 4.16 10 -7 -15 4.27 2.06 10 7 -14 12.74 4.39 10 -7 -14 21.81 5.60 10 -7 -14 15.94 4.83 10 7 -13 0.30 1.91 10 -7 -13 9.11 4.40 10 -7 -13 10.07 4.44 10 7 -12 4.41 3.81 10 -7 -12 5.45 2.61 10 -7 -12 10.59 4.84 10 7 -11 27.08 5.86 10 -7 -11 31.37 7.60 10 -7 -11 16.78 5.56 10 7 -10 34.29 7.42 10 -7 -10 27.99 6.29 10 -7 -10 25.97 6.43 10 7 -9 30.61 6.82 10 -7 -9 21.97 5.75 10 -7 -9 27.20 6.80 10 7 -8 12.21 4.50 10 -7 -8 20.58 5.18 10 -7 -8 13.24 5.07 10 -7 -7 0.28 1.78 10 7 -7 2.72 1.40 -10 7 -7 2.63 3.74 10 -7 -7 1.23 2.50 10 -7 -6 5.47 1.52 10 7 -6 8.85 3.14 10 -7 -6 15.21 5.30 -10 7 -6 7.79 3.22 10 -7 -5 5.26 3.83 10 7 -5 10.25 4.44 -10 7 -5 5.95 2.11 10 -7 -5 5.95 3.37 10 7 -4 -5.48 2.63 10 -7 -4 4.02 3.16 10 7 -4 4.48 4.32 10 -7 -4 5.88 4.03 10 -7 -3 5.90 2.37 10 7 -3 10.89 4.37 10 7 -3 11.14 3.25 10 -7 -3 3.62 2.47 10 -7 -2 7.71 4.64 10 7 -2 20.12 5.28 10 7 -2 14.14 4.27 10 -7 -2 25.38 6.49 10 7 -1 58.05 8.82 10 -7 -1 30.09 6.93 10 7 -1 49.77 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4.45 2.60 11 2 -4 5.72 3.09 11 -2 -4 3.57 2.36 11 -2 -4 0.76 2.23 11 2 -4 4.57 2.44 11 -2 -3 352.21 19.35 11 2 -3 322.24 17.51 11 -2 -3 346.70 20.47 11 2 -3 353.83 19.04 11 2 -3 358.08 19.30 11 2 -2 6.18 2.84 11 2 -2 9.99 3.45 11 -2 -2 14.34 4.08 11 -2 -2 8.63 2.25 11 2 -2 9.10 2.25 11 -2 -1 247.16 16.14 11 -2 -1 235.22 16.51 11 2 -1 238.86 15.56 11 2 -1 227.77 15.54 11 2 -1 255.23 16.30 11 2 0 0.44 2.76 11 2 0 -0.06 1.90 11 -2 0 -0.06 0.98 11 -2 0 1.03 2.61 11 2 0 0.08 1.09 11 -2 1 251.51 16.70 11 -2 1 277.03 17.80 11 2 1 252.68 16.00 11 2 1 237.78 15.78 11 2 2 9.48 3.05 11 2 2 9.31 3.50 11 -2 2 12.95 4.13 11 -2 2 9.53 3.73 11 -2 3 339.66 19.19 11 -2 3 367.98 20.99 11 2 3 372.62 19.58 11 2 3 381.59 19.93 11 2 4 -0.50 1.70 11 2 4 1.16 1.29 11 -2 4 2.01 1.00 11 -2 4 1.69 1.87 11 2 5 26.15 5.09 11 -2 5 24.84 5.24 11 2 5 36.21 6.13 11 2 6 5.25 3.02 11 2 6 2.59 0.97 11 -2 6 0.58 2.36 11 2 7 26.67 5.61 11 2 7 21.83 4.78 11 -2 7 22.82 4.84 11 -2 8 57.33 8.13 11 2 8 64.11 8.55 11 2 8 64.23 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7.82 11 3 -15 26.37 6.35 11 -3 -14 89.22 11.28 11 -3 -14 78.74 10.34 11 3 -14 67.77 9.74 11 -3 -13 85.42 10.86 11 -3 -13 92.48 10.86 11 3 -13 82.28 10.41 11 -3 -12 72.57 9.78 11 3 -12 98.67 11.23 11 -3 -12 99.29 11.13 11 -3 -11 171.71 15.45 11 3 -11 159.46 14.22 11 -3 -11 142.62 13.33 11 -3 -10 26.68 5.91 11 -3 -10 34.44 6.58 11 3 -10 37.48 7.49 11 3 -9 690.90 28.48 11 -3 -9 718.52 29.44 11 -3 -8 210.51 16.16 11 3 -8 194.23 13.40 11 -3 -8 210.60 16.33 11 3 -8 221.95 16.16 11 -3 -7 59.33 8.50 11 3 -7 82.90 8.76 11 -3 -7 74.58 9.61 11 3 -7 69.11 8.12 11 3 -7 75.00 9.32 11 -3 -6 46.61 7.46 11 -3 -6 55.40 8.26 11 3 -6 44.84 6.47 11 3 -6 42.75 6.22 11 3 -6 55.31 8.58 11 -3 -5 436.38 22.80 11 -3 -5 407.52 22.82 11 3 -5 440.48 20.87 11 3 -5 426.49 20.57 11 3 -5 473.52 23.63 11 -3 -4 231.21 16.41 11 3 -4 205.70 14.31 11 3 -4 209.07 14.50 11 3 -4 233.74 16.32 11 -3 -3 1554.75 42.69 11 -3 -3 1586.26 45.22 11 3 -3 1623.60 40.24 11 3 -3 1554.93 42.05 11 -3 -2 275.48 18.31 11 -3 -2 290.34 19.39 11 3 -2 271.26 16.71 11 3 -2 312.04 17.35 11 3 -2 312.67 18.59 11 -3 -1 1416.17 40.42 11 -3 -1 1374.18 40.95 11 3 -1 1357.49 37.34 11 3 -1 1451.88 38.32 11 -3 0 42.10 6.73 11 -3 0 46.42 7.91 11 3 0 67.29 8.69 11 3 0 56.41 7.77 11 -3 1 1432.64 40.66 11 -3 1 1369.83 41.55 11 3 1 1422.73 39.13 11 3 1 1472.80 39.20 11 3 2 266.48 16.82 11 -3 2 292.35 18.32 11 -3 2 252.45 17.79 11 3 2 284.91 17.42 11 3 3 1555.81 40.88 11 -3 3 1634.27 43.87 11 -3 3 1585.70 44.24 11 3 3 1496.95 40.76 11 3 4 214.61 15.38 11 -3 4 232.72 16.80 11 -3 4 213.79 16.36 11 3 4 200.30 14.92 11 3 5 468.98 22.81 11 -3 5 432.99 22.36 11 -3 5 428.12 23.27 11 3 5 437.62 21.63 11 3 6 43.98 7.04 11 -3 6 46.87 7.93 11 -3 6 47.22 8.75 11 3 7 101.50 10.77 11 -3 7 79.32 9.35 11 3 7 74.69 9.09 11 3 8 193.41 14.86 11 -3 8 205.53 15.76 11 3 8 211.74 15.15 11 3 9 644.91 27.82 11 -3 9 715.67 29.66 11 3 9 651.68 26.67 11 3 10 16.07 4.56 11 -3 10 26.35 5.71 11 3 10 25.34 5.63 11 3 11 115.23 12.04 11 -3 11 129.41 12.80 11 3 11 151.08 13.85 11 3 12 82.18 10.17 11 -3 12 93.37 10.79 11 3 12 103.53 11.07 11 3 13 109.94 11.83 11 -3 13 85.87 10.97 11 3 13 97.41 10.58 11 3 14 78.96 10.05 11 -3 14 75.80 10.14 11 3 14 83.74 10.06 11 3 15 21.11 4.29 11 -3 15 18.03 5.29 11 3 16 1.22 2.55 11 -3 16 5.07 2.80 11 3 17 49.40 8.33 11 -3 17 49.72 8.86 11 3 18 110.05 12.88 11 -3 18 87.71 11.46 11 3 19 23.79 5.62 11 -3 19 23.20 6.84 11 3 20 25.14 6.78 11 -3 20 27.98 7.12 11 3 21 9.56 4.04 11 -3 21 1.47 2.49 11 3 22 15.45 5.59 11 3 23 47.50 9.13 11 3 24 42.74 8.65 11 3 25 51.81 9.79 11 -4 -24 8.72 3.89 11 -4 -23 6.79 3.91 11 -4 -22 28.38 7.15 11 -4 -21 7.93 2.40 11 -4 -20 2.49 2.25 11 -4 -19 7.11 4.38 11 4 -19 2.30 3.12 11 -4 -18 -0.95 1.99 11 4 -18 -4.61 4.31 11 -4 -17 2.37 2.29 11 -4 -17 3.65 2.37 11 4 -17 4.91 4.29 11 -4 -16 1.91 4.22 11 -4 -16 3.34 2.67 11 4 -16 1.46 1.47 11 -4 -15 1.75 2.79 11 4 -15 3.93 1.50 11 -4 -14 4.62 3.60 11 -4 -14 1.91 3.21 11 4 -14 0.95 1.27 11 4 -13 -1.54 2.10 11 -4 -13 0.60 1.42 11 -4 -13 -0.04 2.20 11 4 -12 34.51 7.14 11 -4 -12 31.94 6.78 11 -4 -12 38.16 7.03 11 4 -11 8.82 3.44 11 -4 -11 9.47 3.71 11 -4 -11 8.85 4.76 11 -4 -10 33.88 7.69 11 -4 -10 36.69 6.95 11 4 -10 52.50 7.99 11 4 -9 8.75 3.17 11 -4 -9 11.84 4.54 11 -4 -9 -1.44 1.45 11 -4 -8 111.50 12.38 11 4 -8 124.04 12.28 11 -4 -8 98.92 11.25 11 4 -7 18.84 4.60 11 4 -7 9.98 3.38 11 -4 -7 17.11 4.09 11 -4 -7 9.44 4.31 11 4 -6 9.37 3.53 11 -4 -6 9.31 3.41 11 4 -6 7.65 3.14 11 -4 -6 10.27 4.53 11 4 -5 7.97 4.23 11 -4 -5 2.91 2.99 11 4 -5 2.47 1.51 11 -4 -5 4.40 3.46 11 -4 -4 621.91 28.11 11 -4 -4 691.32 30.40 11 4 -4 659.69 26.40 11 4 -4 709.79 29.19 11 -4 -3 78.17 9.78 11 -4 -3 73.38 10.18 11 4 -3 68.64 9.13 11 4 -3 65.56 8.27 11 4 -2 168.79 13.58 11 -4 -2 182.49 15.26 11 -4 -2 154.06 14.56 11 4 -2 175.43 13.20 11 4 -2 166.09 13.75 11 4 -1 213.65 15.05 11 -4 -1 195.44 15.44 11 -4 -1 238.81 17.95 11 4 -1 209.17 14.71 11 4 -1 240.03 16.75 11 4 0 5.61 3.46 11 -4 0 -0.92 2.51 11 4 0 1.16 1.56 11 -4 0 -1.08 2.41 11 -4 1 228.07 16.44 11 4 1 243.45 16.40 11 -4 1 245.12 17.95 11 4 1 253.29 16.92 11 -4 2 152.85 13.39 11 4 2 161.22 13.24 11 -4 2 149.21 14.17 11 4 2 160.29 13.22 11 4 3 59.96 8.46 11 4 3 54.86 7.95 11 -4 3 67.77 8.58 11 -4 3 56.28 8.41 11 4 4 657.71 27.95 11 4 4 604.02 26.08 11 -4 4 673.61 28.87 11 -4 4 683.15 29.81 11 4 5 0.34 2.46 11 -4 5 6.83 2.94 11 4 5 3.28 1.80 11 -4 5 2.18 2.32 11 4 6 12.26 4.16 11 -4 6 10.76 3.65 11 4 6 9.34 3.90 11 -4 6 0.90 2.59 11 4 7 13.72 4.33 11 -4 7 14.30 3.83 11 4 7 16.77 4.88 11 -4 7 13.69 5.45 11 4 8 88.18 9.94 11 4 8 125.61 11.95 11 -4 8 85.12 10.06 11 -4 8 102.72 12.31 11 4 9 7.40 3.75 11 -4 9 4.03 3.36 11 4 9 4.40 3.29 11 -4 9 9.25 3.79 11 4 10 55.21 8.32 11 4 10 61.80 8.80 11 -4 10 34.54 6.96 11 4 11 12.23 3.79 11 -4 11 7.25 3.07 11 4 11 8.07 3.87 11 4 12 29.80 6.26 11 -4 12 33.08 6.66 11 4 12 35.81 6.73 11 4 13 0.19 2.66 11 -4 13 0.19 2.11 11 4 13 1.74 3.38 11 4 14 0.68 3.18 11 -4 14 0.38 2.15 11 4 14 6.22 4.61 11 4 15 7.15 3.20 11 -4 15 9.83 3.51 11 4 15 5.11 3.66 11 -4 16 2.33 1.99 11 4 16 -0.01 1.28 11 -4 17 -1.46 3.10 11 4 17 -0.17 1.79 11 -4 18 -2.21 3.95 11 4 18 1.02 2.33 11 -4 19 -0.12 2.24 11 4 19 9.40 5.22 11 4 20 4.34 3.27 11 4 21 2.85 2.07 11 4 22 24.50 6.37 11 4 23 17.62 5.26 11 4 24 5.70 1.84 11 -5 -22 27.71 6.29 11 -5 -21 4.05 2.47 11 -5 -20 28.96 6.78 11 -5 -19 15.51 4.87 11 5 -19 -6.19 3.10 11 -5 -18 26.75 6.47 11 -5 -18 32.61 7.91 11 5 -18 28.92 6.96 11 -5 -17 17.44 5.77 11 -5 -17 12.02 4.83 11 5 -17 23.65 6.37 11 5 -16 4.75 2.02 11 -5 -16 12.85 4.49 11 -5 -16 4.18 3.62 11 5 -15 19.38 6.19 11 -5 -15 29.22 7.29 11 -5 -15 29.33 6.42 11 -5 -14 64.03 9.85 11 -5 -14 78.89 10.90 11 5 -14 61.85 10.05 11 -5 -13 66.82 10.17 11 5 -13 76.31 10.49 11 -5 -12 10.33 4.00 11 5 -12 20.60 5.75 11 -5 -12 9.32 4.27 11 -5 -11 0.99 1.89 11 5 -11 3.56 1.96 11 -5 -11 5.21 3.54 11 5 -10 0.26 1.48 11 -5 -10 -0.53 1.81 11 -5 -10 2.94 1.49 11 -5 -9 62.68 9.53 11 -5 -9 69.78 9.60 11 5 -9 73.45 10.16 11 -5 -8 219.98 17.76 11 -5 -8 240.86 18.25 11 5 -8 281.73 19.45 11 -5 -7 47.20 8.57 11 -5 -7 58.77 8.88 11 5 -7 43.65 7.99 11 5 -6 26.72 6.11 11 -5 -6 31.29 6.58 11 -5 -6 25.75 6.30 11 5 -5 5.11 3.33 11 -5 -5 3.86 3.08 11 5 -5 6.01 2.93 11 -5 -5 5.13 2.88 11 5 -4 229.56 16.09 11 -5 -4 268.22 18.85 11 -5 -4 283.63 19.33 11 5 -4 285.41 19.06 11 5 -3 54.36 7.46 11 -5 -3 43.01 8.01 11 -5 -3 38.42 7.30 11 5 -3 60.14 8.33 11 5 -2 104.94 11.71 11 -5 -2 87.47 11.04 11 5 -2 90.53 9.85 11 -5 -2 105.61 12.17 11 5 -1 155.10 13.79 11 -5 -1 154.45 14.40 11 5 -1 134.68 12.74 11 -5 -1 164.83 14.96 11 5 0 4.52 3.39 11 -5 0 2.73 2.19 11 5 0 1.75 3.12 11 -5 0 1.49 1.94 11 5 1 153.58 13.94 11 -5 1 136.47 13.57 11 5 1 149.48 13.18 11 -5 1 154.40 14.88 11 5 2 103.16 11.49 11 -5 2 99.77 11.56 11 5 2 91.17 10.52 11 -5 2 93.07 11.58 11 5 3 50.15 8.17 11 -5 3 45.90 7.46 11 5 3 48.90 7.69 11 -5 3 59.02 9.19 11 5 4 257.27 18.16 11 -5 4 276.64 18.59 11 5 4 295.66 19.08 11 -5 4 268.45 19.67 11 5 5 4.81 2.20 11 -5 5 3.35 2.59 11 -5 5 7.74 3.28 11 5 5 6.59 3.55 11 5 6 27.70 6.12 11 -5 6 24.66 5.24 11 -5 6 28.58 6.32 11 5 6 26.05 5.93 11 5 7 50.45 8.66 11 -5 7 46.94 7.72 11 5 7 41.98 7.35 11 -5 7 42.84 8.07 11 5 8 275.32 18.80 11 -5 8 263.37 18.71 11 5 8 273.89 18.86 11 -5 8 246.54 19.15 11 5 9 63.22 8.97 11 -5 9 52.37 8.75 11 5 9 64.51 8.80 11 -5 9 72.15 10.50 11 5 10 3.63 4.16 11 -5 10 2.29 3.47 11 -5 10 3.74 3.64 11 5 10 -1.33 2.34 11 5 11 2.69 2.40 11 -5 11 4.54 2.09 11 -5 11 5.06 4.08 11 5 11 3.07 2.20 11 5 12 16.49 5.14 11 -5 12 10.98 4.64 11 -5 12 10.37 3.80 11 5 12 13.78 4.23 11 5 13 60.37 9.28 11 5 13 72.18 10.00 11 -5 13 43.36 7.79 11 -5 13 51.40 9.37 11 5 14 69.89 10.21 11 -5 14 54.34 9.29 11 5 14 64.81 9.69 11 5 15 14.03 5.02 11 -5 15 17.54 4.31 11 5 15 23.07 6.00 11 -5 16 4.15 2.77 11 5 16 2.06 3.03 11 -5 17 18.83 5.61 11 5 17 13.19 3.95 11 5 18 43.45 8.65 11 -5 18 27.77 7.66 11 5 19 18.26 5.31 11 5 20 22.97 6.32 11 5 21 4.93 3.58 11 5 22 23.58 6.62 11 -6 -21 1.60 2.19 11 -6 -20 28.74 7.21 11 -6 -19 2.09 2.76 11 -6 -19 5.23 5.33 11 -6 -18 0.14 1.75 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28.83 7.17 11 -7 -9 22.23 6.09 11 -7 -8 83.72 11.76 11 7 -8 90.07 11.25 11 7 -7 110.75 12.86 -11 7 -7 125.57 14.33 11 -7 -7 106.06 12.67 11 -7 -7 104.96 13.21 11 7 -6 48.27 8.81 11 -7 -6 33.55 7.59 -11 7 -6 36.48 7.19 11 -7 -6 50.42 9.09 11 -7 -5 7.28 3.87 11 7 -5 1.28 2.08 11 -7 -5 2.01 2.48 11 7 -4 50.08 8.64 11 -7 -4 54.86 9.31 11 -7 -4 46.23 8.35 11 7 -3 97.12 11.76 11 7 -3 86.79 11.05 11 -7 -3 103.17 12.91 11 -7 -3 105.74 12.60 11 -7 -2 22.65 6.08 11 7 -2 16.61 4.93 11 -7 -2 23.33 6.30 11 7 -2 22.59 6.25 11 -7 -1 4.89 3.12 11 7 -1 6.03 3.90 11 -7 -1 2.50 1.64 11 7 -1 1.28 2.33 11 7 0 0.38 1.83 11 -7 0 2.98 2.16 11 7 0 3.53 3.13 11 -7 0 -1.30 3.16 11 7 1 -0.78 2.31 11 -7 1 1.87 2.64 11 7 1 -0.89 2.37 11 -7 1 2.64 2.50 11 7 2 25.68 6.34 11 -7 2 23.07 5.52 11 7 2 20.55 5.76 11 -7 2 25.32 5.50 11 7 3 106.24 11.78 11 7 3 106.27 12.32 11 -7 3 84.94 11.80 11 -7 3 95.19 12.28 11 7 4 53.88 9.11 11 -7 4 42.19 8.22 11 7 4 43.63 8.31 11 -7 4 40.26 7.23 11 7 5 4.12 3.23 11 7 5 4.30 3.61 11 -7 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11 9 6 12.24 4.57 11 9 6 24.45 6.74 -11 9 6 19.62 6.56 11 9 7 62.58 10.67 11 9 7 34.51 7.48 -11 9 7 55.05 9.23 11 -9 7 67.93 10.57 11 -9 8 31.24 7.77 11 9 8 29.13 6.67 11 9 8 17.55 5.75 -11 9 8 8.20 2.56 11 -9 9 16.45 5.64 11 9 9 31.54 7.08 11 9 9 18.38 5.66 -11 9 9 25.87 6.68 11 -9 10 1.05 2.48 11 9 10 -1.48 4.61 11 9 10 6.20 4.18 -11 9 10 0.22 1.43 11 -9 11 -2.41 3.82 11 9 11 4.89 2.91 11 9 11 2.26 2.72 -11 9 11 6.03 3.70 12 0 -23 6.96 4.16 12 0 -22 12.74 5.03 12 0 -21 4.75 3.62 12 0 -20 41.01 8.49 12 0 -19 81.97 10.81 12 0 -18 56.65 9.49 12 0 -17 169.16 15.60 12 0 -16 101.16 12.49 12 0 -15 4.95 1.70 12 0 -14 243.96 18.25 12 0 -13 440.41 24.47 12 0 -12 -5.80 2.50 12 0 -12 216.24 17.24 12 0 -11 144.69 12.73 12 0 -11 230.19 17.43 12 0 -10 270.47 17.40 12 0 -10 238.83 17.77 12 0 -9 36.87 6.10 12 0 -9 48.26 7.79 12 0 -8 174.74 13.71 12 0 -8 172.81 14.61 12 0 -7 29.75 5.50 12 0 -7 21.58 5.26 12 0 -6 146.09 12.72 12 0 -6 125.55 12.31 12 0 -5 219.72 15.32 12 0 -5 254.37 17.62 12 0 -5 232.87 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0.73 2.19 12 -6 -15 4.63 3.35 12 -6 -15 8.60 3.70 12 -6 -14 53.69 9.57 12 -6 -14 51.81 9.20 12 6 -14 46.85 8.62 12 -6 -13 83.17 11.70 12 -6 -13 67.97 10.71 12 6 -13 80.85 11.10 12 6 -12 4.14 2.25 12 -6 -12 2.79 3.26 12 -6 -12 6.26 2.64 12 -6 -11 29.65 6.89 12 6 -11 44.32 8.33 12 -6 -11 29.78 6.09 12 6 -10 41.40 7.59 12 -6 -10 47.07 8.85 12 -6 -10 40.28 8.55 12 -6 -9 10.14 3.75 12 6 -9 11.20 5.37 12 -6 -9 21.09 6.18 12 -6 -8 107.40 13.23 12 -6 -8 96.70 12.21 12 6 -8 102.35 12.58 12 -6 -7 121.88 13.58 12 -6 -7 167.14 15.51 12 6 -7 167.09 15.53 12 6 -6 30.33 7.29 12 -6 -6 31.34 7.64 12 -6 -6 17.71 5.23 12 6 -5 45.82 7.81 12 -6 -5 40.12 7.66 12 -6 -5 41.29 8.09 12 6 -4 92.44 11.52 12 -6 -4 88.98 12.12 12 -6 -4 80.05 10.78 12 6 -4 104.35 12.09 12 6 -3 146.02 13.81 12 -6 -3 130.80 13.74 12 -6 -3 148.67 14.45 12 6 -3 136.74 13.98 12 6 -2 120.13 12.74 12 6 -2 121.92 12.62 12 -6 -2 134.89 14.56 12 -6 -2 118.68 12.95 12 -6 -1 18.14 5.06 12 6 -1 23.03 4.64 12 -6 -1 33.33 8.06 12 6 0 0.45 2.36 12 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7 -6 1.68 2.73 12 -7 -6 1.81 2.72 12 -7 -5 4.00 4.31 12 7 -5 -2.46 2.13 12 -7 -5 0.28 1.52 12 7 -4 30.16 7.16 12 -7 -4 33.33 6.98 12 -7 -4 34.71 7.92 12 -7 -3 16.08 5.44 12 7 -3 14.01 5.06 12 -7 -3 11.72 4.01 12 -7 -2 8.85 4.95 12 7 -2 11.46 4.09 12 -7 -2 21.84 6.10 12 7 -2 14.46 5.02 12 -7 -1 40.62 7.91 12 7 -1 26.17 5.53 12 -7 -1 33.42 8.26 12 7 -1 30.02 6.08 12 7 0 17.70 5.58 12 -7 0 14.31 4.55 12 -7 0 13.98 4.83 12 7 0 16.90 4.04 12 7 1 37.90 8.27 12 -7 1 28.69 6.60 12 -7 1 34.13 6.92 12 7 1 37.22 7.20 12 7 2 15.89 5.11 12 -7 2 12.33 3.84 12 -7 2 15.11 5.57 12 7 2 19.37 5.25 12 7 3 7.54 2.69 12 -7 3 10.28 5.05 12 7 3 10.49 4.05 12 7 4 49.78 9.08 12 -7 4 36.31 7.83 12 -7 4 27.15 6.56 12 7 4 37.66 6.75 12 7 5 1.82 3.60 12 -7 5 7.39 3.59 12 -7 5 5.18 4.56 12 7 5 4.84 2.48 12 7 6 7.24 4.62 12 -7 6 1.38 1.53 12 -7 6 1.80 3.77 12 7 6 5.84 2.92 12 7 7 18.22 5.31 12 7 7 19.02 4.78 12 -7 7 33.81 7.22 12 -7 7 25.24 6.39 12 7 8 10.53 4.17 12 7 8 11.51 3.19 12 -7 8 11.13 4.63 12 -7 8 6.88 3.94 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18.79 6.35 13 5 -14 22.70 6.45 13 5 -13 2.76 2.06 13 -5 -13 3.68 2.45 13 -5 -13 2.97 2.26 13 5 -12 11.72 5.27 13 -5 -12 14.48 4.85 13 -5 -12 18.95 6.03 13 5 -11 53.85 8.33 13 -5 -11 62.38 9.89 13 -5 -11 64.91 9.86 13 -5 -10 26.48 5.69 13 -5 -10 18.80 6.34 13 5 -10 37.06 8.28 13 5 -9 7.26 4.80 13 -5 -9 1.37 1.94 13 -5 -9 -0.64 2.80 13 5 -8 10.13 4.60 13 -5 -8 2.60 1.94 13 -5 -8 9.62 2.57 13 -5 -7 38.15 8.08 13 5 -7 43.11 7.81 13 -5 -7 41.90 8.45 13 -5 -6 95.22 12.04 13 5 -6 77.41 10.39 13 -5 -6 60.22 9.79 13 5 -5 23.18 5.80 13 -5 -5 34.00 7.23 13 -5 -5 13.90 5.65 13 -5 -4 83.19 10.84 13 5 -4 72.64 9.50 13 5 -4 74.07 10.16 13 -5 -4 83.87 11.12 13 -5 -3 45.82 7.81 13 -5 -3 41.57 7.50 13 5 -3 47.19 8.11 13 5 -3 48.70 8.00 13 -5 -2 163.38 15.46 13 -5 -2 164.12 15.89 13 5 -2 154.48 14.48 13 5 -2 162.54 15.17 13 5 -1 124.83 12.71 13 -5 -1 113.33 13.04 13 -5 -1 128.40 14.10 13 5 -1 124.45 12.67 13 5 0 15.39 5.35 13 -5 0 7.07 1.57 13 5 0 18.52 5.33 13 -5 0 20.44 6.30 13 5 1 122.82 12.57 13 -5 1 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63.86 9.35 14 2 -10 61.45 9.58 14 -2 -9 81.36 10.91 14 -2 -9 82.08 11.31 14 2 -9 78.84 10.53 14 2 -9 74.26 10.55 14 -2 -8 18.73 5.40 14 2 -8 23.24 5.53 14 -2 -8 19.24 5.61 14 2 -8 29.81 7.20 14 2 -8 17.35 4.22 14 -2 -7 11.24 3.48 14 -2 -7 17.90 5.68 14 2 -7 13.50 4.04 14 2 -7 16.59 4.59 14 2 -7 27.90 6.30 14 -2 -6 58.70 9.29 14 2 -6 74.38 9.39 14 -2 -6 82.60 10.70 14 2 -6 67.21 9.53 14 2 -6 81.59 10.46 14 -2 -5 65.61 9.47 14 2 -5 88.10 10.49 14 -2 -5 85.94 11.30 14 2 -5 71.24 10.10 14 2 -5 80.80 10.06 14 -2 -4 103.16 11.67 14 2 -4 84.29 10.04 14 -2 -4 108.47 12.64 14 2 -4 102.77 11.58 14 2 -4 93.69 11.09 14 -2 -3 26.35 5.41 14 -2 -3 16.77 4.96 14 2 -3 27.48 6.19 14 2 -3 21.14 5.65 14 2 -3 33.92 6.58 14 -2 -2 14.98 4.63 14 -2 -2 13.39 4.70 14 2 -2 14.16 4.45 14 2 -2 12.16 3.77 14 2 -2 12.95 4.55 14 2 -1 11.43 4.04 14 -2 -1 9.73 3.39 14 -2 -1 9.22 3.72 14 2 -1 17.72 4.81 14 2 -1 12.14 3.79 14 -2 0 193.85 15.98 14 2 0 216.43 16.71 14 -2 0 188.38 16.93 14 2 0 224.23 17.45 14 2 0 206.22 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16.89 5.73 14 -4 -14 29.17 6.96 14 -4 -14 48.18 9.14 14 4 -14 36.36 7.51 14 -4 -13 13.71 4.62 14 -4 -13 9.35 4.29 14 4 -13 8.75 4.41 14 -4 -12 35.56 8.12 14 -4 -12 43.10 8.33 14 4 -12 39.53 7.32 14 -4 -11 38.20 7.81 14 -4 -11 68.62 10.57 14 4 -11 64.07 9.63 14 -4 -10 29.47 7.14 14 -4 -10 41.58 7.83 14 4 -10 25.62 6.32 14 -4 -9 53.45 9.38 14 4 -9 67.52 9.97 14 -4 -9 58.18 9.70 14 4 -8 23.31 6.28 14 -4 -8 25.29 6.21 14 -4 -8 19.78 5.17 14 4 -7 5.45 3.24 14 -4 -7 8.39 4.08 14 -4 -7 13.35 4.72 14 -4 -6 84.92 11.12 14 -4 -6 88.48 11.26 14 4 -6 88.66 11.23 14 4 -5 21.39 5.50 14 4 -5 17.27 4.31 14 -4 -5 21.02 6.35 14 -4 -5 16.73 5.82 14 -4 -4 73.64 10.43 14 -4 -4 71.61 10.26 14 4 -4 77.14 9.90 14 4 -4 73.16 10.07 14 4 -3 40.48 7.44 14 -4 -3 59.25 9.54 14 -4 -3 54.72 9.60 14 4 -3 61.02 9.02 14 4 -2 6.76 2.39 14 4 -2 16.36 4.40 14 -4 -2 10.82 3.63 14 -4 -2 12.60 4.49 14 4 -1 40.02 7.29 14 -4 -1 20.07 6.08 14 -4 -1 26.27 7.12 14 4 -1 42.28 8.63 14 -4 0 466.70 25.66 14 -4 0 471.31 26.93 14 4 0 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4 14 39.76 7.81 14 -4 14 26.52 7.44 14 4 15 13.38 3.41 14 -4 15 22.70 6.56 14 4 16 51.90 9.50 14 -4 16 33.03 7.73 14 4 17 26.55 6.66 14 -4 17 33.18 8.04 14 4 18 10.94 5.37 14 -4 18 -1.45 3.01 14 4 19 2.87 1.45 14 -4 19 5.03 4.60 14 4 20 23.71 6.64 14 -4 20 30.88 7.60 14 -5 -18 1.96 1.15 14 5 -18 1.74 3.05 14 -5 -17 4.18 2.80 14 5 -17 2.71 2.32 14 -5 -16 10.31 4.95 14 5 -16 6.29 3.26 14 -5 -16 4.04 2.17 14 -5 -15 -2.13 3.95 14 5 -15 3.39 3.91 14 -5 -15 -4.64 4.80 14 -5 -14 -0.72 2.71 14 5 -14 3.97 2.38 14 -5 -13 6.48 4.11 14 -5 -13 6.31 4.06 14 5 -13 3.43 2.76 14 5 -12 24.56 5.79 14 -5 -12 19.20 4.71 14 -5 -12 7.98 4.66 14 5 -11 12.00 4.29 14 -5 -11 15.62 4.39 14 -5 -11 1.17 2.01 14 5 -10 13.75 5.54 14 -5 -10 12.55 4.40 14 -5 -10 8.98 4.26 14 5 -9 1.28 2.05 14 -5 -9 15.42 5.49 14 -5 -9 12.88 6.24 14 5 -8 2.47 2.33 14 -5 -8 0.97 1.31 14 -5 -8 5.71 3.48 14 5 -7 7.37 3.95 14 -5 -7 12.16 5.31 14 -5 -7 4.23 3.62 14 5 -6 -0.84 1.78 14 -5 -6 -0.59 1.49 14 -5 -6 -1.31 3.37 14 5 -5 4.02 3.57 14 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12.84 14 -6 -10 80.90 11.95 14 6 -10 62.38 9.69 14 6 -9 33.00 7.64 14 -6 -9 19.28 5.16 14 -6 -9 21.44 6.81 14 6 -8 0.64 1.77 14 -6 -8 10.54 5.14 14 -6 -8 6.50 3.62 14 6 -7 19.01 5.26 14 -6 -7 17.07 5.10 14 -6 -7 18.51 6.22 14 -6 -6 103.11 13.12 14 -6 -6 109.33 13.19 14 6 -6 104.38 12.68 14 6 -5 -2.77 3.41 14 -6 -5 -0.74 1.86 14 -6 -5 1.60 1.74 14 -6 -4 57.90 9.72 14 -6 -4 56.70 9.62 14 6 -4 74.65 11.29 14 6 -3 34.77 8.05 14 -6 -3 36.56 7.25 14 -6 -3 26.01 6.77 14 -6 -2 17.00 5.21 14 6 -2 11.85 4.79 14 -6 -2 31.60 7.39 14 6 -2 38.94 8.62 14 6 -1 32.16 7.01 14 -6 -1 27.25 7.19 14 6 -1 23.04 6.01 14 -6 -1 42.84 8.77 14 -6 0 204.41 17.75 14 6 0 203.79 18.09 14 -6 0 210.30 18.29 14 6 1 28.52 6.87 14 -6 1 16.42 5.38 14 6 1 28.73 6.97 14 6 2 15.20 5.60 14 -6 2 18.16 5.31 14 6 2 19.50 5.35 14 -6 2 31.18 7.27 14 6 3 40.55 8.34 14 6 3 28.07 6.33 14 -6 3 38.56 8.24 14 -6 3 39.57 8.55 14 -6 4 86.50 11.53 14 6 4 49.43 8.90 14 -6 4 65.88 10.97 14 6 4 69.48 10.20 14 6 5 5.97 4.49 14 -6 5 4.78 3.81 14 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5.95 4.28 19 2 4 6.28 2.69 19 2 4 9.19 3.28 19 -2 5 26.55 7.30 19 -2 5 24.56 7.74 19 2 5 29.61 7.76 19 2 5 22.06 6.14 19 2 5 10.43 5.81 19 -2 6 24.60 7.54 19 -2 6 13.55 5.22 19 2 6 26.27 7.48 19 2 6 14.11 4.75 19 2 6 11.45 4.54 19 -2 7 6.29 3.94 19 -2 7 0.97 2.65 19 2 7 11.25 4.69 19 2 7 9.14 3.90 19 2 7 8.97 5.20 19 -2 8 2.65 3.48 19 2 8 -0.79 3.41 19 2 8 -4.20 2.24 19 2 8 4.83 3.10 19 -2 9 2.69 3.32 19 -2 9 5.18 5.05 19 2 9 0.49 2.55 19 -2 10 1.15 2.63 19 2 10 1.94 1.92 19 -2 11 8.45 2.21 19 -2 11 5.42 4.56 19 2 11 7.11 3.70 19 -3 -9 13.98 4.81 19 -3 -9 11.37 4.87 19 3 -9 7.88 2.73 19 -3 -8 20.38 5.81 19 -3 -8 20.22 6.07 19 3 -8 26.59 7.00 19 -3 -7 3.31 2.53 19 -3 -7 5.28 2.30 19 3 -7 3.83 3.40 19 -3 -6 4.32 3.26 19 -3 -6 7.84 4.05 19 3 -6 9.78 5.72 19 -3 -5 8.86 3.19 19 -3 -5 9.68 4.42 19 3 -5 15.49 5.64 19 -3 -4 5.17 3.43 19 -3 -4 6.06 3.34 19 3 -4 4.97 1.60 19 -3 -3 3.38 3.41 19 -3 -3 10.50 4.25 19 3 -3 3.33 3.38 19 3 -3 7.25 4.78 19 -3 -2 6.44 4.84 19 -3 -2 14.17 5.23 19 3 -2 26.79 7.17 19 3 -2 14.97 6.06 19 -3 -1 1.08 2.84 19 -3 -1 11.37 5.40 19 3 -1 7.57 4.71 19 3 -1 2.42 4.13 19 -3 0 -0.35 2.30 19 -3 0 1.63 3.06 19 3 0 3.09 2.68 19 3 0 3.99 3.83 19 -3 1 10.07 4.47 19 -3 1 10.84 5.20 19 3 1 5.61 3.24 19 3 1 11.63 5.06 19 -3 2 10.12 4.32 19 -3 2 23.97 6.38 19 3 2 21.11 6.12 19 3 2 7.49 3.51 19 -3 3 6.13 2.56 19 -3 3 4.16 3.00 19 3 3 14.65 7.62 19 3 3 7.89 4.47 19 3 3 10.07 4.26 19 -3 4 5.28 3.47 19 -3 4 0.56 2.37 19 3 4 1.16 3.81 19 3 4 6.58 4.05 19 3 4 2.59 2.36 19 -3 5 12.42 4.80 19 -3 5 6.77 3.93 19 3 5 13.04 4.47 19 3 5 19.12 5.63 19 3 5 9.21 3.35 19 -3 6 8.13 2.61 19 -3 6 13.45 5.28 19 3 6 -1.17 4.58 19 3 6 5.49 3.00 19 3 6 1.91 2.39 19 3 7 5.84 4.06 19 -3 7 12.33 6.26 19 -3 7 8.32 4.98 19 3 7 9.38 3.41 19 3 7 0.28 2.03 19 3 8 26.57 6.63 19 -3 8 19.49 6.80 19 -3 8 27.62 7.40 19 3 8 9.93 4.50 19 3 8 19.18 5.44 19 3 9 11.57 4.52 19 -3 9 15.10 6.18 19 -3 9 14.92 5.80 19 3 9 14.04 6.81 19 -4 -6 0.56 2.81 19 -4 -6 -0.76 2.93 19 4 -6 6.18 4.93 19 -4 -5 2.10 2.04 19 -4 -5 -2.17 2.61 19 4 -5 -2.34 2.46 19 -4 -4 8.60 3.45 19 -4 -4 13.39 5.67 19 4 -4 12.16 5.14 19 -4 -3 6.06 4.48 19 -4 -3 3.90 2.25 19 4 -3 1.78 4.27 19 -4 -2 6.06 4.31 19 -4 -2 8.11 4.76 19 4 -2 3.66 4.82 19 4 -2 0.43 1.29 19 -4 -1 4.25 3.41 19 -4 -1 0.94 5.03 19 4 -1 -0.14 2.45 19 4 -1 -0.78 3.17 19 -4 0 13.11 4.47 19 -4 0 2.46 3.64 19 4 0 6.12 3.47 19 4 0 3.94 2.24 19 -4 1 -2.33 1.39 19 -4 1 1.86 3.44 19 4 1 3.10 2.26 19 4 1 -5.44 4.94 19 4 2 10.45 4.83 19 -4 2 1.29 2.63 19 -4 2 2.01 2.61 19 4 2 2.29 2.27 19 4 3 3.20 3.76 19 -4 3 10.64 5.07 19 -4 3 1.96 3.35 19 4 3 1.07 3.35 19 4 4 2.79 2.64 19 -4 4 4.33 2.80 19 -4 4 6.74 4.56 19 4 4 13.25 5.86 19 4 5 0.07 1.66 19 -4 5 -2.78 2.80 19 -4 5 0.23 3.09 19 4 5 5.78 5.29 19 4 6 0.34 1.38 19 -4 6 0.02 2.31 19 -4 6 0.85 3.27 19 4 6 -1.41 2.65 20 0 -8 136.19 16.35 20 0 -7 3.88 2.91 20 0 -6 -0.32 2.58 20 0 -6 -1.93 2.20 20 0 -5 66.03 10.76 20 0 -5 63.90 10.74 20 0 -4 187.11 18.44 20 0 -4 224.39 20.86 20 0 -3 0.72 1.70 20 0 -3 -2.58 5.07 20 0 -2 223.99 20.42 20 0 -2 231.85 21.73 20 0 -1 28.27 6.55 20 0 -1 24.88 6.70 20 0 0 0.15 2.31 20 0 0 -1.40 2.86 20 0 1 16.18 4.96 20 0 1 12.37 5.00 20 0 2 208.21 19.20 20 0 2 227.58 21.90 20 0 3 -0.74 3.16 20 0 3 1.74 2.22 20 0 4 197.46 18.87 20 0 4 181.68 19.34 20 0 5 71.40 11.03 20 0 5 50.76 10.34 20 0 6 -1.12 2.84 20 0 6 -0.28 3.25 20 0 7 6.06 3.38 20 0 7 2.49 2.27 20 0 8 174.48 17.02 20 0 8 181.84 18.24 20 -1 -7 3.92 2.58 20 -1 -7 -1.24 1.75 20 -1 -6 -0.24 3.28 20 -1 -6 -0.56 2.15 20 1 -6 0.69 3.95 20 -1 -5 0.50 2.85 20 1 -5 4.13 3.28 20 -1 -5 8.39 3.42 20 1 -5 6.98 3.84 20 -1 -4 -2.26 3.21 20 1 -4 0.64 2.43 20 -1 -4 -3.47 3.48 20 1 -4 4.07 2.95 20 1 -3 10.47 4.29 20 -1 -3 10.64 3.07 20 1 -3 19.30 6.37 20 -1 -2 10.87 3.88 20 1 -2 4.65 3.16 20 -1 -2 9.34 5.12 20 1 -2 7.57 4.03 20 -1 -1 9.92 4.37 20 1 -1 8.05 2.21 20 -1 -1 3.71 2.29 20 1 -1 10.79 4.80 20 -1 0 -1.02 4.04 20 1 0 7.15 5.37 20 -1 0 0.34 2.50 20 1 0 0.53 4.30 20 -1 1 4.77 3.35 20 1 1 1.40 1.16 20 -1 1 -0.80 4.05 20 1 1 4.00 4.08 20 -1 2 3.19 4.58 20 1 2 5.88 3.54 20 -1 2 5.59 3.94 20 1 2 5.44 4.66 20 -1 3 17.35 6.48 20 1 3 15.59 5.20 20 -1 3 12.08 5.87 20 1 3 19.14 6.25 20 -1 4 0.75 1.43 20 1 4 0.73 2.80 20 -1 4 -1.32 4.25 20 1 4 0.28 4.29 20 -1 5 11.48 4.37 20 1 5 9.49 3.29 20 -1 5 6.41 4.83 20 1 5 12.72 5.64 20 -1 6 3.34 3.26 20 1 6 2.19 3.14 20 -1 6 -5.80 5.60 20 1 6 1.60 3.82 20 -1 7 -2.21 3.46 20 1 7 -0.65 2.26 20 -1 7 3.96 3.54 20 1 7 5.72 5.83 20 -2 -5 5.63 2.13 20 -2 -5 -2.19 4.66 20 -2 -4 18.28 5.60 20 -2 -4 31.47 7.37 20 -2 -3 1.46 2.06 20 2 -3 7.52 4.58 20 -2 -3 5.46 5.53 20 2 -3 7.20 2.91 20 -2 -2 66.09 10.88 20 2 -2 82.77 12.46 20 -2 -2 71.65 12.49 20 2 -2 100.89 12.91 20 -2 -1 -0.14 3.05 20 2 -1 6.02 2.75 20 -2 -1 5.05 4.79 20 2 -1 2.31 4.89 20 2 -1 7.96 4.04 20 -2 0 4.35 4.01 20 2 0 2.84 3.87 20 -2 0 -1.22 3.02 20 2 0 -1.99 3.08 20 2 0 -0.88 2.77 20 -2 1 7.19 4.61 20 2 1 8.66 4.17 20 -2 1 1.01 1.54 20 2 1 4.76 2.71 20 2 1 4.43 3.83 20 -2 2 99.31 13.50 20 2 2 69.70 10.74 20 -2 2 99.26 13.60 20 2 2 71.62 11.09 20 2 2 87.10 12.50 20 -2 3 -0.07 2.92 20 -2 3 -0.78 1.91 20 2 3 -0.67 2.28 20 2 3 4.11 3.58 20 2 3 2.61 3.55 20 -2 4 17.11 5.18 20 -2 4 20.48 5.70 20 2 4 13.02 4.91 20 2 4 20.98 5.46 20 2 4 22.26 6.63 20 -2 5 3.83 3.15 20 -2 5 -2.53 2.82 20 2 5 3.66 3.55 20 2 5 0.40 2.90 20 2 5 3.88 3.15 20 -3 0 -2.45 2.92 20 -3 0 5.89 4.82 20 3 0 2.38 2.49 20 3 0 -3.67 3.81 0 0 0 0.00 0.00 TITL 008_240K_SulfamerazineF1_ in Pna2(1) REM Pna2(1) (#33, found as Pbn2(1) in ba-c setting) CELL 0.68890 14.485221 8.201991 21.900222 90.0000 90.0000 90.0000 ZERR 8.00 0.000138 0.000084 0.000301 0.0000 0.0000 0.0000 LATT -1 SYMM -x,-y, z+1/2 SYMM x+1/2,-y+1/2, z SYMM -x+1/2, y+1/2, z+1/2 SFAC C H N O S UNIT 88.00 96.00 32.00 16.00 8.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 92368