Dataset for "Understanding heat driven gelation of anionic cellulose nanofibrils: Combining Saturation Transfer Difference (STD) NMR, Small Angle X-ray Scattering (SAXS) and rheology"

Dataset for "Understanding heat driven gelation of anionic cellulose nanofibrils: Combining Saturation Transfer Difference (STD) NMR, Small Angle X-ray Scattering (SAXS) and rheology"

This dataset contains the data underlying the figures in the paper "Understanding heat driven gelation of anionic cellulose nanofibrils: Combining Saturation Transfer Difference (STD) NMR, Small Angle X-ray Scattering (SAXS) and rheology". The data for figure 4 (SAXS) is given as four different data files: Figure 4(a) Oxidised cellulose nanofibrils (OCNF) at 25 °C and OCNF at 25°C after annealing at 80°C and Figure 4(b) cationic cellulose nanofibrils (CCNF) at 25 °C and CCNF at 25°C after annealing at 80°C as explained in the materials and methods of the main manuscript. In a similar fashion, the Fig. ESI3 and Fig. ESI6 files contain the data underlying figures 3 and 6 of the electronic supplementary information.

Subjects:
Biomolecules and biochemistry

Cite this dataset as:
Calabrese, V., Schmitt, J., Edler, K., Alves Da Silva, M., Scott, J., 2018. Dataset for "Understanding heat driven gelation of anionic cellulose nanofibrils: Combining Saturation Transfer Difference (STD) NMR, Small Angle X-ray Scattering (SAXS) and rheology". University of Bath Research Data Archive. https://doi.org/10.15125/BATH-00476.

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Data

Fig.%201.txt
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Storage and loss moduli as function of temperature and time.

Fig.%202.txt
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Shear viscosity loop of OCNF and OCNF* (heated) 1.25 wt% dispersions.

Fig.%203.txt
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UV-Vis transmittance spectra of the OCNF and OCNF* dispersions at 0.5 and 1 wt%.

Fig.%204%20a%29 ... 2080%C2%B0C.txt
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SAXS patterns for OCNF at 25°C after annealing at 80°C

Fig.%204%20a%29OCNF.txt
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SAXS patterns for OCNF at 25°C

Fig.%204%20b%29 ... 2080%C2%B0C.txt
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SAXS patterns for CCNF at 25°C after annealing at 80°C

Fig.%204%20b%29CCNF.txt
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SAXS patterns for CCNF at 25°C

Fig.%20ESI3.txt
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Fig.%20ESI6.txt
text/plain (33kB)
Creative Commons: Attribution 4.0

Creators

Vincenzo Calabrese
University of Bath

Julien Schmitt
University of Bath

Karen Edler
University of Bath

Janet Scott
University of Bath

Coverage

Collection date(s):

From 1 February 2017 to 1 September 2017

Documentation

Data collection method:

Data collection, materials and methods are listed in the associated manuscript.

Funders

Engineering and Physical Sciences Research Council (EPSRC)
https://doi.org/10.13039/501100000266

New Enzymatically Produced Interpenetrating Starch-Cellulose Gels
EP/N033310/1

Publication details

Publication date: 25 September 2018
by: University of Bath

Version: 1

DOI: https://doi.org/10.15125/BATH-00476

URL for this record: https://researchdata.bath.ac.uk/id/eprint/476

Related articles

Calabrese, V., Muñoz-García, J. C., Schmitt, J., da Silva, M. A., Scott, J. L., Angulo, J., Khimyak, Y. Z. and Edler, K. J., 2019. Understanding heat driven gelation of anionic cellulose nanofibrils: Combining saturation transfer difference (STD) NMR, small angle X-ray scattering (SAXS) and rheology. Journal of Colloid and Interface Science, 535, pp.205-213. Available from: https://doi.org/10.1016/j.jcis.2018.09.085.

Contact information

Please contact the Research Data Service in the first instance for all matters concerning this item.

Contact person: Vincenzo Calabrese

Departments:

Faculty of Science
Chemistry