Dataset for "Understanding heat driven gelation of anionic cellulose nanofibrils: Combining Saturation Transfer Difference (STD) NMR, Small Angle X-ray Scattering (SAXS) and rheology"

This dataset contains the data underlying the figures in the paper "Understanding heat driven gelation of anionic cellulose nanofibrils: Combining Saturation Transfer Difference (STD) NMR, Small Angle X-ray Scattering (SAXS) and rheology". The data for figure 4 (SAXS) is given as four different data files: Figure 4(a) Oxidised cellulose nanofibrils (OCNF) at 25 °C and OCNF at 25°C after annealing at 80°C and Figure 4(b) cationic cellulose nanofibrils (CCNF) at 25 °C and CCNF at 25°C after annealing at 80°C as explained in the materials and methods of the main manuscript. In a similar fashion, the Fig. ESI3 and Fig. ESI6 files contain the data underlying figures 3 and 6 of the electronic supplementary information.

Subjects:
Biomolecules and biochemistry

Cite this dataset as:
Calabrese, V., Schmitt, J., Edler, K., Alves Da Silva, M., Scott, J., 2018. Dataset for "Understanding heat driven gelation of anionic cellulose nanofibrils: Combining Saturation Transfer Difference (STD) NMR, Small Angle X-ray Scattering (SAXS) and rheology". Bath: University of Bath Research Data Archive. Available from: https://doi.org/10.15125/BATH-00476.

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Data

Fig. 1.txt
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Storage and loss moduli as function of temperature and time.

Fig. 2.txt
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Shear viscosity loop of OCNF and OCNF* (heated) 1.25 wt% dispersions.

Fig. 3.txt
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UV-Vis transmittance spectra of the OCNF and OCNF* dispersions at 0.5 and 1 wt%.

Fig. 4 a)OCNF after 80°C.txt
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SAXS patterns for OCNF at 25°C after annealing at 80°C

Fig. 4 a)OCNF.txt
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SAXS patterns for OCNF at 25°C

Fig. 4 b)CCNF after 80°C.txt
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SAXS patterns for CCNF at 25°C after annealing at 80°C

Fig. 4 b)CCNF.txt
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SAXS patterns for CCNF at 25°C

Fig. ESI3.txt
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Fig. ESI6.txt
text/plain (33kB)
Creative Commons: Attribution 4.0

Creators

Vincenzo Calabrese
University of Bath

Julien Schmitt
University of Bath

Karen Edler
University of Bath

Janet Scott
University of Bath

Contributors

University of Bath
Rights Holder

Coverage

Collection date(s):

From 1 February 2017 to 1 September 2017

Documentation

Data collection method:

Data collection, materials and methods are listed in the associated manuscript.

Funders

Engineering and Physical Sciences Research Council (EPSRC)
https://doi.org/10.13039/501100000266

New Enzymatically Produced Interpenetrating Starch-Cellulose Gels
EP/N033310/1

Publication details

Publication date: 25 September 2018
by: University of Bath

Version: 1

DOI: https://doi.org/10.15125/BATH-00476

URL for this record: https://researchdata.bath.ac.uk/id/eprint/476

Related papers and books

Calabrese, V., Muñoz-García, J. C., Schmitt, J., da Silva, M. A., Scott, J. L., Angulo, J., Khimyak, Y. Z. and Edler, K. J., 2019. Understanding heat driven gelation of anionic cellulose nanofibrils: Combining saturation transfer difference (STD) NMR, small angle X-ray scattering (SAXS) and rheology. Journal of Colloid and Interface Science, 535, pp.205-213. Available from: https://doi.org/10.1016/j.jcis.2018.09.085.

Contact information

Please contact the Research Data Service in the first instance for all matters concerning this item.

Contact person: Vincenzo Calabrese

Departments:

Faculty of Science
Chemistry