Dataset supporting "In situ X-ray reflectivity and GISAXS study of mesoporous silica films grown from sodium silicate solution precursors"
This dataset includes data relating to mesoporous silica films grown from sodium silicate solution precursors: dynamic light scattering (DLS) data for solutions containing cetrimonium bromide and sodium nitrate; small angle X-ray scattering (SAXS) data for films contain cetyltrimethylammonium bromide (CTAB), silica and polyethylenimine (PEI), and silica film; thermogravimetric analysis (TGA) data recording the decomposition of CTAB–PEI–silica in air with temperature; in-situ X-ray reflectivity (XRR) data, surface pressure data, and grazing incidence X-ray scattering (GISAXS) data for the interface between the solution (sodium silicate, CTAB, PEI) and air; and nitrogen sorption data.
Cite this dataset as:
Di, A.,
Schmitt, J.,
Elstone, N.,
Arnold, T.,
Edler, K.,
2022.
Dataset supporting "In situ X-ray reflectivity and GISAXS study of mesoporous silica films grown from sodium silicate solution precursors".
Bath: University of Bath Research Data Archive.
Available from: https://doi.org/10.15125/BATH-01151.
Export
Data
DLS.pxp
application/octet-stream (96kB)
Creative Commons: Attribution 4.0
Dynamic light scattering data
small-angle … lab-based-SAXS.7z
application/x-7z-compressed (551kB)
Creative Commons: Attribution 4.0
Small angle X-ray scattering data (lab-based)
TGA-data.7z
application/x-7z-compressed (125kB)
Creative Commons: Attribution 4.0
Thermogravimetric analysis data
XRR-data.7z
application/x-7z-compressed (161kB)
Creative Commons: Attribution 4.0
In-situ X-ray reflectivity data
surface-pressure-data.7z
application/x-7z-compressed (4MB)
Creative Commons: Attribution 4.0
Surface pressure data
GISAXS-data.7z
application/x-7z-compressed (21MB)
Creative Commons: Attribution 4.0
Grazing incidence X-ray scattering data
N2-isotherm.7z
application/x-7z-compressed (17kB)
Creative Commons: Attribution 4.0
Nitrogen sorption data
Creators
Andi Di
University of Bath
Julien Schmitt
University of Bath; Centre national de la recherche scientifique
Naomi Elstone
University of Bath
Thomas Arnold
Diamond Light Source Ltd; European Spallation Source ERIC
Karen Edler
University of Bath
Contributors
University of Bath
Rights Holder
Documentation
Data collection method:
Full details of the methodology can be found in the Experimental section of the associated paper.
Data processing and preparation activities:
The XRR data were normalised.
Technical details and requirements:
All the data are plotted in Igor Pro software, https://www.wavemetrics.com/.
Additional information:
SAXS data has three columns: Q (x axis), scattering intensity (y axis) and error for scattering intensity. GISAXS data are images. XRR data has three columns: Q as x axis, reflectivity (y axis) and error in y axis. Surface pressure data contains two columns: time and surface pressure.
Methodology link:
Di, A., Schmitt, J., Elstone, N., Arnold, T., and Edler, K. J., 2022. In situ X-ray reflectivity and GISAXS study of mesoporous silica films grown from sodium silicate solution precursors. Microporous and Mesoporous Materials, 341, 112018. Available from: https://doi.org/10.1016/j.micromeso.2022.112018.
Funders
Engineering and Physical Sciences Research Council (EPSRC)
https://doi.org/10.13039/501100000266
EPSRC Centre for Doctoral Training in Sustainable Chemical Technologies
EP/L016354/1
China Scholarship Council (CSC)
https://doi.org/10.13039/501100004543
PhD Studentship
Publication details
Publication date: 25 May 2022
by: University of Bath
Version: 1
DOI: https://doi.org/10.15125/BATH-01151
URL for this record: https://researchdata.bath.ac.uk/id/eprint/1151
Related papers and books
Di, A., Schmitt, J., Elstone, N., Arnold, T., and Edler, K. J., 2022. In situ X-ray reflectivity and GISAXS study of mesoporous silica films grown from sodium silicate solution precursors. Microporous and Mesoporous Materials, 341, 112018. Available from: https://doi.org/10.1016/j.micromeso.2022.112018.
Contact information
Please contact the Research Data Service in the first instance for all matters concerning this item.
Contact person: Karen Edler
Faculty of Science
Chemistry
