Dataset for Synthesis of Photocatalytic Pore Size-Tuned ZnO Molecular Foams
Raw data files for XRD, HPLC, UV dosage, ICPMS, Eeo, MicroCT and hydrodynamic calculations associated with manuscript titled "Synthesis of Photocatalytic Pore Size-Tuned ZnO Molecular Foams"
XRD contains raw data of XRD spectra used to analyse crystallinity and crystal phase of ZnO samples.
HPLC contains the raw data used to produce degradation profiles of carbamazepine when exposed to the photocatalyst. UV dosage contains the raw data used to plot degradation against UV irradiation supplied to allow for greater analysis between flow rates of reactor.
ICPMS contains the raw data collected to analyse the concentration of metal in the pollutant stream, allowing for analysis of material stability.
Eeo contains the calculations used to work out the electrical energy efficiency of the system, allowing for analysis of efficiency when operating the reactor under different conditions.
MicroCT is the raw data collected from analysis of the 3D reconstruction of the samples, used to analyse the pore structure (size, sphericity, ect)
Hydrodynamic calculations contains the calculations conducted to understand the reactor system and to calculate key parameters allowing for the discussion of the reactor.
Cite this dataset as:
Warren, Z.,
Tasso Guaraldo, T.,
Wenk, J.,
Mattia, D.,
2022.
Dataset for Synthesis of Photocatalytic Pore Size-Tuned ZnO Molecular Foams.
Bath: University of Bath Research Data Archive.
Available from: https://doi.org/10.15125/BATH-01118.
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Data
ZW MolFoam Dataset Data.zip
application/zip (722kB)
Creative Commons: Attribution 4.0
Zip file containing raw data files for XRD, HPLC, ICPMS, UV dosage, Eeo, MicroCT and hydrodynamic calculations associated with manuscript titled "Synthesis of Photocatalytic Pore Size-Tuned ZnO Molecular Foams"
Creators
Zachary Warren
University of Bath
Thais Tasso Guaraldo
University of Bath
Jannis Wenk
Supervisor
University of Bath
Davide Mattia
Supervisor
University of Bath
Contributors
University of Bath
Rights Holder
Coverage
Collection date(s):
From 9 January 2012 to 31 August 2021
Documentation
Data collection method:
XRD - sampling between 2 Theta of 20 - 90 with Cu K alpha xrays. HPLC - degradation experiments used 1 mL samples taken every 15 or 30 minutes. Analysis was performed on a Thermo Scientific Ultimate 3000 liquid chromatograph with a UV detector. CBZ analysis used a Thermo Scientific Acclaim 120 C18 column (3.0 X 75.0 mm, particle size 3.0 µm) and a Thermo Scientific Acclaim 120 C18 guard column (R) 120 C18 (3.0 X 10.0 mm, particle size 5.0 µm) The mobile phase was made up using 5.0 mM phosphoric acid and acetonitrile 70:30 (v:v) with a flow rate of 0.8 mL min-1, injection volume of 20 µL and detection wavelength of 285 nm. ICPMS - All samples, standards and blanks, were spiked with internal standard elements Be, In, and Re. The Zn concentration was calibrated using six synthetic standards prepared from a 1000 ppm Inorganic Ventures (VA, USA) standard. MicroCT - Data collected using a Nikon XT H 225 ST using a 178 kV x-ray source and 0.708 second exposure time, 3141 projections and 4 frames per projection and analysed using Thermo Scientific Avizo Software 9 3D data visualisation software.
Funders
Engineering and Physical Sciences Research Council
https://doi.org/10.13039/501100000266
Fellowship - Photocatalytic Anodic Membranes for Micropollutant Removal
EP/P031382/1
Publication details
Publication date: 4 May 2022
by: University of Bath
Version: 1
DOI: https://doi.org/10.15125/BATH-01118
URL for this record: https://researchdata.bath.ac.uk/id/eprint/1118
Related papers and books
Warren, Z., Guaraldo, T. T., Wenk, J., and Mattia, D., 2022. Synthesis of photocatalytic pore size-tuned ZnO molecular foams. Journal of Materials Chemistry A, 10(21), 11542-11552. Available from: https://doi.org/10.1039/d2ta02038f.
Contact information
Please contact the Research Data Service in the first instance for all matters concerning this item.
Contact person: Davide Mattia
Faculty of Engineering & Design
Chemical Engineering
Research Centres & Institutes
Water Innovation and Research Centre (WIRC)
