Dataset for "Self-assembly of amphiphilic polyoxometalates for the preparation of mesoporous polyoxometalate-titania catalysts"

The dataset contains ASCII files for small-angle neutron scattering (SANS) curves and fits for polyoxometalate-headed surfactant (POM-2Cn, n=12, 14, 16 and 18) solution as a function of surfactant concentrations. Solutions are prepared in two different solvents: deuterium dioxide, 7:3 deuterium dioxide and H2O mixture.

The dataset also contains Igor files for the following:

- the plot of determination of critical micelle concentrations (CMC) of the POM-2Cn H2O system through conductivity measurements;
- the plot of 13C NMR, 31P NMR of POM-2Cn;
- the plot of UV-vis spectra and IR of POM-2Cn;
- the degradation line of RhB by nPOM-TiO2 catalysts and the corresponding rate constants;
- the plot of TGA for POM-2Cn;
- the XRD patterns of nPOM-TiO2 and TiO2.

Subjects:

Catalysis and surfaces

Cite this dataset as:
Di, A., Edler, K., Hossain, K., Schmitt, J., Alves Da Silva, M., Mahmoudi, N., Errington, R., 2020. Dataset for "Self-assembly of amphiphilic polyoxometalates for the preparation of mesoporous polyoxometalate-titania catalysts". Bath: University of Bath Research Data Archive. Available from: https://doi.org/10.15125/BATH-00931.

Export

Data

archived data.zip
application/zip (7MB)
Creative Commons: Attribution 4.0

Creators

Andi Di
University of Bath

0000-0003-4527-2504

Karen Edler
University of Bath

0000-0001-5822-0127

Kazi M. Zakir Hossain
University of Bath

0000-0002-4178-7271

Julien Schmitt
University of Bath; Laboratoire de Synthèse et Fonctionnalisation des Céramiques

0000-0002-3452-6655

Marcelo Alves Da Silva
University of Bath

0000-0002-1413-4021

Najet Mahmoudi
Rutherford Appleton Laboratory

R. John Errington
Newcastle University

Contributors

University of Bath
Rights Holder

Documentation

Data collection method:

Full details of the methodology used may be found in the Experimental section of the associated paper.

Technical details and requirements:

This work benefited from DANSE software developed under NSF award DMR-0520547.

Additional information:

The SANS data are recorded in plain text files. The remaining data are provided in Igor Pro Packed Experiment (.pxp) format.

Methodology link:

Di, A., Schmitt, J., da Silva, M. A., Hossain, K. M. Z., Mahmoudi, N., Errington, R. J., and Edler, K. J., 2020. Self-assembly of amphiphilic polyoxometalates for the preparation of mesoporous polyoxometalate-titania catalysts. Nanoscale, 12(43), 22245-22257. Available from: https://doi.org/10.1039/d0nr05967f.