Dataset for "Self-assembly of amphiphilic polyoxometalates for the preparation of mesoporous polyoxometalate-titania catalysts"

The dataset contains ASCII files for small-angle neutron scattering (SANS) curves and fits for polyoxometalate-headed surfactant (POM-2Cn, n=12, 14, 16 and 18) solution as a function of surfactant concentrations. Solutions are prepared in two different solvents: deuterium dioxide, 7:3 deuterium dioxide and H2O mixture.

The dataset also contains Igor files for the following:

- the plot of determination of critical micelle concentrations (CMC) of the POM-2Cn H2O system through conductivity measurements;
- the plot of 13C NMR, 31P NMR of POM-2Cn;
- the plot of UV-vis spectra and IR of POM-2Cn;
- the degradation line of RhB by nPOM-TiO2 catalysts and the corresponding rate constants;
- the plot of TGA for POM-2Cn;
- the XRD patterns of nPOM-TiO2 and TiO2.

Subjects:

Cite this dataset as:
Di, A., Edler, K., Hossain, K., Schmitt, J., Alves Da Silva, M., Mahmoudi, N., Errington, R., 2020. Dataset for "Self-assembly of amphiphilic polyoxometalates for the preparation of mesoporous polyoxometalate-titania catalysts". Bath: University of Bath Research Data Archive. Available from: https://doi.org/10.15125/BATH-00931.

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Data

archived data.zip
application/zip (7MB)
Creative Commons: Attribution 4.0

Creators

Andi Di
University of Bath

Karen Edler
University of Bath

Julien Schmitt
University of Bath; Laboratoire de Synthèse et Fonctionnalisation des Céramiques

Najet Mahmoudi
Rutherford Appleton Laboratory

R. John Errington
Newcastle University

Contributors

University of Bath
Rights Holder

Documentation

Data collection method:

Full details of the methodology used may be found in the Experimental section of the associated paper.

Additional information:

The SANS data are recorded in plain text files. The remaining data are provided in Igor Pro Packed Experiment (.pxp) format.

Methodology link:

Di, A., Schmitt, J., da Silva, M. A., Hossain, K. M. Z., Mahmoudi, N., Errington, R. J., and Edler, K. J., 2020. Self-assembly of amphiphilic polyoxometalates for the preparation of mesoporous polyoxometalate-titania catalysts. Nanoscale, 12(43), 22245-22257. Available from: https://doi.org/10.1039/d0nr05967f.

Funders

China Scholarship Council (CSC)
https://doi.org/10.13039/501100004543

PhD Studentship

National Science Foundation (NSF)
https://doi.org/10.13039/100000001

IMR-MIP DANSE - Distributed Data Analysis for Neutron Scattering Experiments - CNST
DMR-0520547

Horizon 2020 Framework Programme (H2020)
https://doi.org/10.13039/100010661

PROJECT SINE2020 World class Science and Innovation with Neutrons in Europe 2020 – SINE2020
654000

Publication details

Publication date: 27 October 2020
by: University of Bath

Version: 1

DOI: https://doi.org/10.15125/BATH-00931

URL for this record: https://researchdata.bath.ac.uk/id/eprint/931

Related papers and books

Di, A., Schmitt, J., da Silva, M. A., Hossain, K. M. Z., Mahmoudi, N., Errington, R. J., and Edler, K. J., 2020. Self-assembly of amphiphilic polyoxometalates for the preparation of mesoporous polyoxometalate-titania catalysts. Nanoscale, 12(43), 22245-22257. Available from: https://doi.org/10.1039/d0nr05967f.

Contact information

Please contact the Research Data Service in the first instance for all matters concerning this item.

Contact person: Karen Edler

Departments:

Faculty of Science
Chemistry

Research Centres & Institutes
Centre for Sustainable and Circular Technologies (CSCT)